CN104357245A - Preparing method and usages of sapindus extract - Google Patents
Preparing method and usages of sapindus extract Download PDFInfo
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- CN104357245A CN104357245A CN201410449761.5A CN201410449761A CN104357245A CN 104357245 A CN104357245 A CN 104357245A CN 201410449761 A CN201410449761 A CN 201410449761A CN 104357245 A CN104357245 A CN 104357245A
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Abstract
The invention provides a preparing method, usages and a product of a sapindus extract. The extracted sapindus extract has excellent clearing, decontaminating and washing capability, can be used in washing products and cleaning products and is green and environment-friendly, so that the sapindus extract can be applied in washing industry and has great industrial prospects and market values.
Description
Technical field
The present invention relates to a Plant Extracts, relate more specifically to a kind of preparation method and its usage of soapberry extract, belong to field of natural product extraction.
Background technology
Seed of Chinese Soapberry (Sapindus), is also called wood and suffers from sub, oily trouble, bitter trouble tree, yellow order, You Luoshu, wash one's hands fruit, soap fruit tree etc.The pericarp of its thick meat shape contains saponin, just can produce foam as long as crumple a little with water, and can be used for cleaning, is one of the main sanitising agent in ancient times.
Seed of Chinese Soapberry has multiple medicinal function, as spot, skin care etc. are removed in antibacterial, anti-dandruff, anticreep, whitening, tea-polyphenol is wherein water-soluble substances, the grease of face, convergence pore can be disposed, energy sterilization, sterilizing, resisting age of skin, can reduce the radiation of daylight middle-ultraviolet lamp to the damage of skin.In addition, wherein contained forulic acid is the cosmetic factor that scientific circles generally acknowledge, can improve skin quality, make its exquisiteness, gloss, high resilience, the effect such as antibacterial, anti-inflammatory in addition simultaneously, anti-oxidant, scavenging free radicals, anticoagulation.And tartaric acid wherein can help skin removed to be deposited in outer field aging cutin, accelerate skin renewal, help improve skin comedo, blackspot, wrinkle, xerosis cutis, the skin problem such as coarse.
At present, large quantifier elimination concentrates in clean, the washing of Seed of Chinese Soapberry, soil removability, and has this type of technical literatures many.
Such as, Chinese patent application CN102517177A just discloses washing liquid, wherein just includes Seed of Chinese Soapberry soap breast 5-15 part of certain mass number.
But in current all prior aries, for the extraction of Seed of Chinese Soapberry, still need to continue to improve, seek better extracting method.Thus suitability for industrialized production can be realized simply.
Summary of the invention
In order to develop the preparation method of new soapberry extract, the present inventor, through a large amount of further investigations, after having paid sufficient creative work, has completed the present invention.
The present invention relates generally to two aspects.
First aspect, the present invention relates to a kind of preparation method of soapberry extract, and described preparation method comprises:
(1) get dry Seed of Chinese Soapberry fruit, ground, obtain 100-200 object raw material powder;
(2) raw material powder being added mass percent concentration is in the aqueous ethanolic solution of 60-80%, temperature programming under room temperature, microwave extraction, and wherein microwave power is 400-600W, and extraction time is 40-60 minute, then filters, and obtains filtrate and filter residue;
(3) filter residue is carried out soxhlet type, extraction solvent is acetone and ethyl acetate mixed solvent, and temperature is 60-80 DEG C, and the time is 1-2 hour, then leaves standstill, and filters and obtains extract;
(4) filtrate of combining step (2) and the extract of step (3), revolves and steams except desolventizing, obtain sticky shape paste, be soapberry extract of the present invention.
In the preparation method of soapberry extract of the present invention, the raw material powder in described step (2) and the mass ratio of aqueous ethanolic solution are 1:10-20, such as, can be 1:10,1:15 or 1:20.
In the preparation method of soapberry extract of the present invention, the temperature programming in described step (2) is 2-5 DEG C/min, is preferably 3 DEG C/min.
In the preparation method of soapberry extract of the present invention, the microwave power in described step (2) is preferably 500W, and extraction time is preferably 50 minutes.
In the preparation method of soapberry extract of the present invention, in the acetone and ethyl acetate mixed solvent in described step (3), the mass ratio of acetone and ethyl acetate is 1:1-3, such as, can be 1:1,1:2 or 1:3, is preferably 1:1`.
In the preparation method of soapberry extract of the present invention, the filter residue in described step (3) and the mass ratio of acetone and ethyl acetate mixed solvent are 1:10-20, such as, can be 1:10,1:15 or 1:20.
Second aspect, the present invention relates to soapberry extract that aforesaid method extracts for washing, clean in purposes.
The soapberry extract extracted due to the inventive method has excellent washing and soil removability, thus can be used for Cleaning preparations, as in washing powder, washing liquid, soap, industrial scrubbing powder etc.
The third aspect, the invention still further relates to any goods comprising the soapberry extract that aforesaid method extracts.
Embodiment
Below by specific embodiment, the present invention is described in detail; but the purposes of these exemplary embodiments and object are only used for exemplifying the present invention; not any type of any restriction is formed to real protection scope of the present invention, more non-protection scope of the present invention is confined to this.
Embodiment 1
(1) get dry Seed of Chinese Soapberry fruit, ground, obtain 100 object raw material powders;
(2) mass percent concentration raw material powder being added 10 times of quality is in the aqueous ethanolic solution of 60%, heats up under room temperature with the speed program of 3 DEG C/min, microwave extraction, wherein microwave power is 400W, extraction time is 40 minutes, then filters, and obtains filtrate and filter residue;
(3) filter residue is carried out soxhlet type, the acetone and ethyl acetate mixed solvent of extraction solvent to be mass ratio be 1:1, wherein the mass ratio of filter residue and mixed solvent is 1:10, and extraction temperature is 60 DEG C, and the time is 1 hour, then leaves standstill, and filters and obtains extract;
(4) filtrate of combining step (2) and the extract of step (3), revolves and steams except desolventizing, obtain sticky shape paste, be soapberry extract of the present invention.
Embodiment 2
(1) get dry Seed of Chinese Soapberry fruit, ground, obtain 150 object raw material powders;
(2) mass percent concentration raw material powder being added 15 times of quality is in the aqueous ethanolic solution of 70%, heats up under room temperature with the speed program of 3 DEG C/min, microwave extraction, wherein microwave power is 500W, extraction time is 50 minutes, then filters, and obtains filtrate and filter residue;
(3) filter residue is carried out soxhlet type, the acetone and ethyl acetate mixed solvent of extraction solvent to be mass ratio be 1:2, extraction temperature is 70 DEG C, and the time is 1.5 hours, then leaves standstill, and filters and obtains extract;
(4) filtrate of combining step (2) and the extract of step (3), revolves and steams except desolventizing, obtain sticky shape paste, be soapberry extract of the present invention.
Embodiment 3
(1) get dry Seed of Chinese Soapberry fruit, ground, obtain 200 object raw material powders;
(2) mass percent concentration raw material powder being added 20 times of quality is in the aqueous ethanolic solution of 80%, heats up under room temperature with the speed program of 3 DEG C/min, microwave extraction, wherein microwave power is 600W, extraction time is 60 minutes, then filters, and obtains filtrate and filter residue;
(3) filter residue is carried out soxhlet type, the acetone and ethyl acetate mixed solvent of extraction solvent to be mass ratio be 1:3, extraction temperature is 80 DEG C, and the time is 2 hours, then leaves standstill, and filters and obtains extract;
(4) filtrate of combining step (2) and the extract of step (3), revolves and steams except desolventizing, obtain sticky shape paste, be soapberry extract of the present invention.
Embodiment 4
(1) get dry Seed of Chinese Soapberry fruit, ground, obtain 100 object raw material powders;
(2) mass percent concentration raw material powder being added 10 times of quality is in the aqueous ethanolic solution of 80%, heats up under room temperature with the speed program of 3 DEG C/min, microwave extraction, wherein microwave power is 500W, extraction time is 40 minutes, then filters, and obtains filtrate and filter residue;
(3) filter residue is carried out soxhlet type, the acetone and ethyl acetate mixed solvent of extraction solvent to be mass ratio be 1:1, extraction temperature is 70 DEG C, and the time is 2 hours, then leaves standstill, and filters and obtains extract;
(4) filtrate of combining step (2) and the extract of step (3), revolves and steams except desolventizing, obtain sticky shape paste, be soapberry extract of the present invention.
Soil removability is tested
By polluting the band having even spot, cutting into equal-sized multiple cloth, being then positioned in washing machine, the soapberry extract of the embodiment 1-4 of equivalent weight is dissolved in water, then adding in washing machine.After the washing same long time, estimate its washability.
After washing, by band hang airing, under high light, then estimate original spot whether wash away, and in order to reduce range estimation error, compare with unpolluted similar band.Found that, the pollution cloth through embodiment 1-4 washing is all cleaned completely, and noresidue spot or blackening, this demonstrate that the soapberry extract that the inventive method is extracted has excellent washability.
Should be appreciated that the purposes of these embodiments is only not intended to for illustration of the present invention limit the scope of the invention.In addition; also should understand; after having read technology contents of the present invention, those skilled in the art can make various change, amendment and/or modification to the present invention, and these all equivalent form of values fall within the protection domain that the application's appended claims limits equally.
Claims (8)
1. a preparation method for soapberry extract, described preparation method comprises:
(1) get dry Seed of Chinese Soapberry fruit, ground, obtain 100-200 object raw material powder;
(2) raw material powder being added mass percent concentration is in the aqueous ethanolic solution of 60-80%, temperature programming under room temperature, microwave extraction, and wherein microwave power is 400-600W, and extraction time is 40-60 minute, then filters, and obtains filtrate and filter residue;
(3) filter residue is carried out soxhlet type, extraction solvent is acetone and ethyl acetate mixed solvent, and temperature is 60-80 DEG C, and the time is 1-2 hour, then leaves standstill, and filters and obtains extract;
(4) filtrate of combining step (2) and the extract of step (3), revolves and steams except desolventizing, obtain sticky shape paste, be described soapberry extract.
2. the preparation method of soapberry extract as claimed in claim 1, is characterized in that: the raw material powder in described step (2) and the mass ratio of aqueous ethanolic solution are 1:10-20.
3. the preparation method of soapberry extract as claimed in claim 1 or 2, is characterized in that: the temperature programming in described step (2) is 2-5 DEG C/min.
4. the preparation method of the soapberry extract as described in any one of claim 1-3, is characterized in that: the microwave power in described step (2) is 500W, and extraction time is 50 minutes.
5. the preparation method of soapberry extract as claimed in claim 4, it is characterized in that: in the acetone and ethyl acetate mixed solvent in described step (3), the mass ratio of acetone and ethyl acetate is 1:1-3.
6. the preparation method of the soapberry extract as described in any one of claim 1-5, is characterized in that: the filter residue in described step (3) and the mass ratio of acetone and ethyl acetate mixed solvent are 1:10-20.
7. the soapberry extract extracted of method described in any one of claim 1-6 for washing, clean in purposes.
8. comprise the goods of the soapberry extract that method described in any one of claim 1-6 is extracted.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410449761.5A CN104357245A (en) | 2014-09-04 | 2014-09-04 | Preparing method and usages of sapindus extract |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410449761.5A CN104357245A (en) | 2014-09-04 | 2014-09-04 | Preparing method and usages of sapindus extract |
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| CN104357245A true CN104357245A (en) | 2015-02-18 |
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| CN201410449761.5A Pending CN104357245A (en) | 2014-09-04 | 2014-09-04 | Preparing method and usages of sapindus extract |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104840387A (en) * | 2015-04-28 | 2015-08-19 | 百朗德生物化学海门有限公司 | Low-irritation-smell soapberry fruit extract production method |
| CN106637900A (en) * | 2016-12-26 | 2017-05-10 | 广西江缘茧丝绸有限公司 | Production method of natural silk cotton quilt |
| CN107090374A (en) * | 2017-05-19 | 2017-08-25 | 北京泰克美高新技术有限公司 | Tea set cleaning fluid and preparation method thereof |
| CN108373953A (en) * | 2018-03-15 | 2018-08-07 | 东华理工大学 | A kind of soapberry ferment handmade soap and preparation method thereof |
| CN114540131A (en) * | 2022-02-25 | 2022-05-27 | 南阳理工学院 | Chemical cleaning agent and preparation method thereof |
-
2014
- 2014-09-04 CN CN201410449761.5A patent/CN104357245A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104840387A (en) * | 2015-04-28 | 2015-08-19 | 百朗德生物化学海门有限公司 | Low-irritation-smell soapberry fruit extract production method |
| CN106637900A (en) * | 2016-12-26 | 2017-05-10 | 广西江缘茧丝绸有限公司 | Production method of natural silk cotton quilt |
| CN107090374A (en) * | 2017-05-19 | 2017-08-25 | 北京泰克美高新技术有限公司 | Tea set cleaning fluid and preparation method thereof |
| CN108373953A (en) * | 2018-03-15 | 2018-08-07 | 东华理工大学 | A kind of soapberry ferment handmade soap and preparation method thereof |
| CN108373953B (en) * | 2018-03-15 | 2020-04-07 | 东华理工大学 | Soapberry enzyme handmade soap and preparation method thereof |
| CN114540131A (en) * | 2022-02-25 | 2022-05-27 | 南阳理工学院 | Chemical cleaning agent and preparation method thereof |
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Application publication date: 20150218 |
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