CN104356847A - Novel corrosion-resistant laminated floor coating and novel preparation method thereof - Google Patents
Novel corrosion-resistant laminated floor coating and novel preparation method thereof Download PDFInfo
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- CN104356847A CN104356847A CN201410613760.XA CN201410613760A CN104356847A CN 104356847 A CN104356847 A CN 104356847A CN 201410613760 A CN201410613760 A CN 201410613760A CN 104356847 A CN104356847 A CN 104356847A
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- Prior art keywords
- consolidated floor
- floor coating
- corrosion resistant
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/12—Esters; Ether-esters of cyclic polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F15/00—Flooring
- E04F15/02—Flooring or floor layers composed of a number of similar elements
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2206—Oxides; Hydroxides of metals of calcium, strontium or barium
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Architecture (AREA)
- Inorganic Chemistry (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Paints Or Removers (AREA)
Abstract
The invention belongs to the field of floor materials and discloses a corrosion-resistant laminated floor coating and a preparation method thereof. The coating comprises the following components: phenolic resin, calcium oxide, aluminum silicate, dicyclohexyl phthalate and the like. The preparation method comprises the following steps: (1), pulverizing the calcium oxide and the aluminum silicate by a pulverizer respectively; (2), opening a reaction kettle, heating the reaction kettle to be 70 to 75 DEG C, adding 12 to 19 parts by weight of phenolic resin, 5 to 10 parts by weight calcium oxide, 6 to 11 parts by weight of aluminum silicate, 3 to 7 parts by weight of dicyclohexyl phthalate and 5 to 11 parts by weight of 2-methyl-2 butene into the reaction kettle, and stirring until the raw materials are mixed uniformly; (3), increasing the internal temperature of the reaction kettle to be 85 to 90 DEG C, adding 2 to 5 parts by weight of butyl butyrate and 7 to 12 parts by weight of polytetrafluoroethylene resin, and stirring fully and uniformly to obtain the corrosion-resistant laminated floor coating.
Description
Technical field
The invention belongs to flooring material field, relate to a kind of consolidated floor coating and preparation method thereof, particularly relate to a kind of corrosion resistant consolidated floor coating and preparation method thereof.
Background technology
Consolidated floor is generally made up of four layer material compounds, i.e. wearing layer, ornament layer, high-density substrate layer, balance layer.Qualified consolidated floor is with one or more layers special dipping thermosetting aminoresin.Cover the substrate surfaces such as high-density plate, the back side adds balance moisture-proof barrier, front adds ornament layer and wearing layer forms through hot pressing.Consolidated floor top coat is generally divided into aluminium sesquioxide type consolidated floor, melamine-type consolidated floor, piano lacquer painting type consolidated floor.The consolidated floor of melamine surface coating, is generally used for wallboard, desktop etc., is used in the less demanding place of rub proofness.Its wear-resisting revolution only has 300-500 to turn.Working strength is large, two or three months, and the decorative paper on surface, will wear and tear.The resistance to acids and bases of the coating on consolidated floor top layer is also extremely important, the corrosion-resistant intensity of the coat composed consolidated floor of poor acid and alkali-resistance is lower, after touching acid solution or alkali lye, easily larger destruction is produced to consolidated floor, therefore need the acid and alkali-resistance intensity improving consolidated floor coating.
Summary of the invention
The technical problem solved: the coating on consolidated floor top layer has decisive action to wear-resisting, the acid and alkali-resistance of consolidated floor, the performance such as withstand voltage, the poor coating of character can the intensity of direct reduction consolidated floor, affect the use of consolidated floor, the acid and alkali-resistance intensity of conventional consolidated floor coating is lower, therefore needs a kind of corrosion resistant consolidated floor coating and preparation method thereof.
Technical scheme: the consolidated floor coating that the invention discloses a kind of novel corrosion resistant, the consolidated floor coating of described novel corrosion resistant comprises the raw material of following weight parts:
Further, the consolidated floor coating of described a kind of novel corrosion resistant, comprises the raw material of following weight parts:
Further, the consolidated floor coating of described a kind of novel corrosion resistant, comprises the raw material of following weight parts:
A novel preparation method for corrosion resistant consolidated floor coating, preparation method is as follows:
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 100 order-300 orders;
(2) reactor is opened, temperature of reaction kettle is increased to 70-75 DEG C, in reactor, add that resol is 12-19 part, calcium oxide is 5-10 part, pure aluminium silicate is 6-11 part, dicyclohexyl phthalate is 3-7 part, 2-methyl-2-butene is 5-11 part, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly;
(3) again reactor temperature being increased to 85-90 DEG C, then adding that butyl butyrate is 2-5 part, teflon resin is 7-12 part, more fully stirs, is corrosion resistant consolidated floor coating after stirring.
In the preparation method of described a kind of corrosion resistant consolidated floor coating, alr mode is mechanical stirring, and mixing speed is 80-200r/min.
Described a kind of corrosion resistant consolidated floor coating is preparing the purposes in consolidated floor.
Beneficial effect: consolidated floor coating optimum formula of the present invention is 16 parts, resol, 7 parts, calcium oxide, pure aluminium silicate 9 parts, dicyclohexyl phthalate 5 parts, 2-methyl-2-butene 8 parts, butyl butyrate 4 parts, teflon resin 9 parts, the intensity of the acid and alkali-resistance of the consolidated floor coating prepared by above-mentioned formula is the highest, can be used in consolidated floor, improve the acid and alkali-resistance intensity of consolidated floor.
Embodiment
Embodiment 1
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 300 orders; (2) reactor is opened, temperature of reaction kettle is increased to 70 DEG C, in reactor, add that resol is 19Kg, calcium oxide is 5Kg, pure aluminium silicate is 11Kg, dicyclohexyl phthalate be 3Kg, 2-methyl-2-butene is 5Kg, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly; (3) again reactor temperature being increased to 90 DEG C, then adding that butyl butyrate is 5Kg, teflon resin is 12Kg, more fully stirs, is corrosion resistant consolidated floor coating after stirring.
No property and appearance change after consolidated floor coating prepared by embodiment 1 soaks 3h respectively under the acetic acid solution of 20wt% and the sodium hydroxide solution of 20wt%.
Embodiment 2
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 100 orders; (2) reactor is opened, temperature of reaction kettle is increased to 75 DEG C, in reactor, add that resol is 12Kg, calcium oxide is 10Kg, pure aluminium silicate is 6Kg, dicyclohexyl phthalate be 7Kg, 2-methyl-2-butene is 11Kg, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly; (3) again reactor temperature being increased to 85 DEG C, then adding that butyl butyrate is 2Kg, teflon resin is 7Kg, more fully stirs, is corrosion resistant consolidated floor coating after stirring.
No property and appearance change after consolidated floor coating prepared by embodiment 2 soaks 3h respectively under the acetic acid solution of 20wt% and the sodium hydroxide solution of 20wt%.
Embodiment 3
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 300 orders; (2) reactor is opened, temperature of reaction kettle is increased to 70 DEG C, in reactor, add that resol is 14Kg, calcium oxide is 8Kg, pure aluminium silicate is 7Kg, dicyclohexyl phthalate be 6Kg, 2-methyl-2-butene is 10Kg, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly; (3) again reactor temperature being increased to 90 DEG C, then adding that butyl butyrate is 4Kg, teflon resin is 8Kg, more fully stirs, is corrosion resistant consolidated floor coating after stirring.
No property and appearance change after consolidated floor coating prepared by embodiment 3 soaks 5h respectively under the acetic acid solution of 20wt% and the sodium hydroxide solution of 20wt%.
Embodiment 4
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 200 orders; (2) reactor is opened, temperature of reaction kettle is increased to 75 DEG C, in reactor, add that resol is 17Kg, calcium oxide is 6Kg, pure aluminium silicate is 10Kg, dicyclohexyl phthalate be 4Kg, 2-methyl-2-butene is 6Kg, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly; (3) again reactor temperature being increased to 90 DEG C, then adding that butyl butyrate is 3Kg, teflon resin is 10Kg, more fully stirs, is corrosion resistant consolidated floor coating after stirring.
No property and appearance change after consolidated floor coating prepared by embodiment 4 soaks 7h respectively under the acetic acid solution of 20wt% and the sodium hydroxide solution of 20wt%.
Embodiment 5
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 200 orders; (2) reactor is opened, temperature of reaction kettle is increased to 75 DEG C, in reactor, add that resol is 16Kg, calcium oxide is 7Kg, pure aluminium silicate is 9Kg, dicyclohexyl phthalate be 5Kg, 2-methyl-2-butene is 8Kg, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly; (3) again reactor temperature being increased to 85 DEG C, then adding that butyl butyrate is 4Kg, teflon resin is 9Kg, more fully stirs, is corrosion resistant consolidated floor coating after stirring.
No property and appearance change after consolidated floor coating prepared by embodiment 5 soaks 10h respectively under the acetic acid solution of 20wt% and the sodium hydroxide solution of 20wt%.
Claims (6)
1. a consolidated floor coating for novel corrosion resistant, is characterized in that, described corrosion resistant consolidated floor coating comprises the raw material of following weight parts:
2. the consolidated floor coating of a kind of novel corrosion resistant according to claim 1, is characterized in that, described corrosion resistant consolidated floor coating comprises the raw material of following weight parts:
3. the consolidated floor coating of a kind of novel corrosion resistant according to claim 1, is characterized in that, described corrosion resistant consolidated floor coating comprises the raw material of following weight parts:
4. a novel preparation method for the consolidated floor coating of novel corrosion resistant, is characterized in that the preparation method of described consolidated floor coating is as follows:
(1) calcium oxide and pure aluminium silicate pulverizer are pulverized respectively, all pulverize as powder wood number is 100 order-300 orders;
(2) reactor is opened, temperature of reaction kettle is increased to 70-75 DEG C, in reactor, add that resol is 12-19 part, calcium oxide is 5-10 part, pure aluminium silicate is 6-11 part, dicyclohexyl phthalate is 3-7 part, 2-methyl-2-butene is 5-11 part by weight, stir after adding, be stirred to above-mentioned raw materials and be mixed to evenly;
(3) again reactor temperature being increased to 85-90 DEG C, then adding that butyl butyrate is 2-5 part, teflon resin is 7-12 part, more fully stirs by weight, is corrosion resistant consolidated floor coating after stirring.
5. the novel preparation method of a kind of corrosion resistant consolidated floor coating according to claim 4, it is characterized in that alr mode is mechanical stirring, mixing speed is 80-200r/min.
6. the consolidated floor coating of a kind of novel corrosion resistant according to claims 1 to 3 is preparing the purposes in consolidated floor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410613760.XA CN104356847A (en) | 2014-11-04 | 2014-11-04 | Novel corrosion-resistant laminated floor coating and novel preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410613760.XA CN104356847A (en) | 2014-11-04 | 2014-11-04 | Novel corrosion-resistant laminated floor coating and novel preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104356847A true CN104356847A (en) | 2015-02-18 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410613760.XA Pending CN104356847A (en) | 2014-11-04 | 2014-11-04 | Novel corrosion-resistant laminated floor coating and novel preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005118730A1 (en) * | 2004-06-04 | 2005-12-15 | Nihon Parkerizing Co., Ltd. | Aqueous coating material for sliding member and sliding member |
| CN102352167A (en) * | 2011-09-13 | 2012-02-15 | 大连鹏鸿木业有限公司 | Floor paint |
| CN102439102A (en) * | 2009-03-13 | 2012-05-02 | Hi-希尔公司 | Anti-corrosion and low friction coating |
| CN103013271A (en) * | 2012-11-28 | 2013-04-03 | 启东市隆腾电气有限公司 | Skid prevention paint for floors |
-
2014
- 2014-11-04 CN CN201410613760.XA patent/CN104356847A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005118730A1 (en) * | 2004-06-04 | 2005-12-15 | Nihon Parkerizing Co., Ltd. | Aqueous coating material for sliding member and sliding member |
| CN102439102A (en) * | 2009-03-13 | 2012-05-02 | Hi-希尔公司 | Anti-corrosion and low friction coating |
| CN102352167A (en) * | 2011-09-13 | 2012-02-15 | 大连鹏鸿木业有限公司 | Floor paint |
| CN103013271A (en) * | 2012-11-28 | 2013-04-03 | 启东市隆腾电气有限公司 | Skid prevention paint for floors |
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Application publication date: 20150218 |