CN104355550A - Glass with mirror surface pattern effect and preparation method thereof - Google Patents
Glass with mirror surface pattern effect and preparation method thereof Download PDFInfo
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- CN104355550A CN104355550A CN201410606172.3A CN201410606172A CN104355550A CN 104355550 A CN104355550 A CN 104355550A CN 201410606172 A CN201410606172 A CN 201410606172A CN 104355550 A CN104355550 A CN 104355550A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/001—General methods for coating; Devices therefor
- C03C17/002—General methods for coating; Devices therefor for flat glass, e.g. float glass
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
- C03C17/3417—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials all coatings being oxide coatings
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
- C03C17/3429—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials at least one of the coatings being a non-oxide coating
- C03C17/3435—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials at least one of the coatings being a non-oxide coating comprising a nitride, oxynitride, boronitride or carbonitride
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3605—Coatings of the type glass/metal/inorganic compound
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3607—Coatings of the type glass/inorganic compound/metal
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3649—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer made of metals other than silver
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/70—Properties of coatings
- C03C2217/72—Decorative coatings
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/119—Deposition methods from solutions or suspensions by printing
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/154—Deposition methods from the vapour phase by sputtering
- C03C2218/156—Deposition methods from the vapour phase by sputtering by magnetron sputtering
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/30—Aspects of methods for coating glass not covered above
- C03C2218/32—After-treatment
- C03C2218/328—Partly or completely removing a coating
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/30—Aspects of methods for coating glass not covered above
- C03C2218/355—Temporary coating
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
Abstract
The invention provides a preparation method of glass with a mirror surface pattern effect. The preparation method comprises the following steps: (1) manufacturing of a screen: manufacturing the screen with a hollowed pattern which is complementary with the required pattern; (2) printing of the screen: selecting waterborne enameled glass printing ink and utilizing the screen prepared in the step (1) to conduct silk-screen printing to a glass sheet; (3) drying: drying the glass sheet with the required hollowed pattern after printing; (4) sputter coating: according to the requirements of the required mirror surface effect, selecting an appropriate target material, and conducting vacuum magnetron sputtering coating to the surface of the glass sheet printed with the waterborne enameled glass printing ink wholly; (5) cleaning: after coating, cleaning up the waterborne enameled glass printing ink attached on the glass sheet. The preparation method of the glass with the mirror surface pattern effect provided by the invention is simple in technology, good in reliability, and suitable for large-scale industrial production.
Description
Technical field
The invention relates to glass post-processing technical field, particularly a kind of glass with decorative effect and preparation method thereof.
Background technology
In ambetti field, mirror image effect refers to that on glass, the reflected light of pattern has metalluster, this metalluster can in by silvery white to golden yellow not etc.In prior art, there are several means can realize above-mentioned mirror image effect, as the chemical bronzing material etc. in baking vanish glass, low-temperature silver slurry glass and ceramic glaze.
Baking vanish glass, is a kind of ambetti kind, can be made by modes such as spraying, roller coating, silk screen printing or showerings.Baking vanish glass is in the field of business is also back of the body paint glass, point plane baking vanish glass and frosted baking vanish glass, is to be made by the roasting 8-12 hour in the baking box of 30-45 DEG C that sprays paint at the back side of glass.The paint of baking vanish glass has harm to human body, and baking vanish glass lacquer painting poor adhesive force, easily come off in a humidity environment, the poor-performing of resistance to uv irradiating of paint, baking vanish glass is generally used as light tight decorative material for wall surface, is not suitable for building curtain wall glass.
Low-temperature silver slurry glass, is adopt the way of silk screen printing to be printed on glass by this slurry in silver slurry, makes low-temperature silver slurry glass.Silver starches a kind of thick slurry be made up of the particulate of highly purified (99.9%) argent, tackiness agent, solvent, auxiliary agent.The shortcoming of this method is: a. needs to coordinate interlayer to use; B. cost is high, silver slurry price nearly ten thousand yuan of per kilograms, and one kilogram can only printing area be the glass of 6 ~ 9 square meters, when not considering yield rate, every square meter glass cost also up to 1500 yuan ~ 2000 yuan; C. difficulty of processing is large, and efficiency is low, per hour according to a preliminary estimate can only silk screen printing 3-5 sheet glass, production capacity is low.Consider that construction work glass consumption is large, the project cycle is short, so low-temperature silver slurry glass can not meet the various demands to mirror image effect glass.
The gold stamping glaze of chemistry in ceramic glaze, this kind of glaze is applied in ceramic industry.Essence is a kind of chemical polymerization thing, can be combined, present metal-like under the high temperature of 1000 DEG C with glass frit, but temperature required too high, exceedes the softening temperature of engineering glass.
The glass that current magnetron sputtering technology is also applied to mirror image effect makes; mainly by the blocking layer such as paster or protecting glue with pierced pattern is covered on glass; after justifying plated film, blocking layer is peeled off, obtain the glass finally with mirror image effect.The defect of these class methods is, easily makes the edge of plated film pattern and junction, blocking layer be destroyed when peeling off on the one hand blocking layer, plated film pattern be often damaged or pattern edge unintelligible; On the other hand owing to easily causing glass surface local temperature to raise in vacuum magnetic-control sputtering process, often rise to more than 100 DEG C, blocking layer is destroyed, cause blocking layer carbonization to pollute glass, or pattern should do not plated by the place of plated film; Again on the one hand, after blocking layer is peeled off, the position of blocking layer and glass adhesion is not easy to clean, may because of clean improper damage glass surface yet.
Summary of the invention
The invention, for solving the deficiencies in the prior art, provides that a kind of technique is simple, good reliability, is applicable to a kind of of large-scale commercial production and has glass of mirror image effect and preparation method thereof.
Method described in the invention comprises the steps: that (1) makes web plate: make and have the web plate with the pierced pattern of required pattern complementary; (2) screen printing: select water-based colored glazed glass ink, carries out silk screen printing with the web plate that step (1) is made to sheet glass; (3) dry: dry after printing with the sheet glass of required pierced pattern; (4) sputter coating: need to select suitable target to carry out overall vacuum magnetron sputtering plating to the one side that sheet glass is printed with water-based colored glazed glass ink according to specular color; (5) clean: after plated film, the water-based colored glazed glass ink be attached on sheet glass is cleaned up, obtain the glassy product with required mirror image effect.
Before described step (2) is carried out, also comprise sheet glass is cut into slices, the operation such as edging, tempering.
Water-based colored glazed glass ink in above-mentioned steps (2) is preferably rosin water color ink.
The particle fineness of the water-based colored glazed glass ink in above-mentioned steps (2) is 0.5-30 μm.
The thickness of the water-based colored glazed glass ink printing in above-mentioned steps (2) is 10-50 μm, is preferably 30 μm.
Further, in the printing process of described step (2), controlling the temperature of sheet glass when printing is more than 30 DEG C, is preferably 40-45 DEG C.
Drying course described in above-mentioned steps (3), for carry out at 110-160 DEG C, is preferably 120-150 DEG C.
Sputter coating process described in above-mentioned steps (4) makes the openwork part of uncoated water-based colored glazed glass ink in glass sheet surface obtain the coatings with mirror image effect; this coatings comprises reflecting layer and protective layer, and target can be selected as required.Described reflecting layer can be one or more in Cr, CrNx, NiCr, NiCrNx, Ti, TiOx, TiNx, and thickness is 1-30nm; Described protective layer can be one or more in SiNx, SiNxOy, SnOx, and thickness is 1-50nm.
In sputter coating process described in above-mentioned steps (4), vacuum tightness is 1*10
-6bar.
Before above-mentioned steps (5) is carried out, also comprise the sheet glass after to sputter coating and carry out tempering or half tempered process.
Cleaning process described in above-mentioned steps (5) comprises, and soaks more than 24h, and then rinse well in the clear water of the sheet glass after sputter coating more than 40 DEG C with the water-based colored glazed glass ink of high pressure water by glass sheet surface.
The invention additionally provides a kind of glass with mirror image effect, has the mirror effect pattern of any fraction of coverage, and the coatings that this mirror effect pattern is formed by vacuum magnetron sputtering coating film is formed.Described coatings comprises reflecting layer and protective layer, and described reflecting layer can be one or more in Cr, CrNx, NiCr, NiCrNx, Ti, TiOx, TiNx, and thickness is 1-30nm; Described protective layer can be one or more in SiNx, SiNxOy, SnOx, and thickness is 1-50nm.
The described glass with mirror image effect can be common float glass, toughened glass, coated glass etc.; The described structure with the glass of mirror image effect can be single-glass, also can make laminated glass, and described mirror effect pattern can be positioned at any one surface of glass.
The advantage that the invention has and positively effect are: what a, the invention obtained has the glass pattern fraction of coverage variation range of mirror image effect extensively, can obtain the mirror image effect with any fraction of coverage as required; B, the invention can remove water-based colored glazed glass ink easily when not damaging coatings and the glass surface of mirror image, and mirror image edge clear, pattern fidelity or resolving power are controlled, and yield rate is high, can reach more than 99.5%; C, because water-based colored glazed glass ink composition mostly is inorganics, the localized hyperthermia caused in vacuum magnetic-control sputtering process can be born, effectively prevent the non-plated membranous part position of causing because blocking layer is destroyed and pollute; D, the invention technique are simple, with low cost, are applicable to large-scale commercial production, can meet construction work to the heavy demand of glass with mirror image effect.
Accompanying drawing explanation
Fig. 1-2 is the various glass schematic diagram with mirror image effect prepared by the invention.
Fig. 3 is a kind of structural representation with the glass of mirror image effect prepared by the invention.
Wherein, 1 is sheet glass, and 2 is reflecting layer, and 3 is protective layer.
Embodiment
Below by specific embodiment, the invention is further described.
Embodiment 1
The preparation various glass with mirror image effect as illustrated in the accompanying drawings from 1 to 3, in figure, dash area representative has the pattern of mirror reflection effect.First adopt routine techniques to make silk screen printing web plate, make web plate have the pierced pattern of non-shaded portion in figure, for subsequent use.According to desired size, sheet glass is cut, edging and tempering, then with the above-mentioned web plate prepared, silk screen printing is carried out to sheet glass, the non-shaded portion of sheet glass is covered by water-based colored glazed glass ink completely, rosin water color ink selected by described water-based colored glazed glass ink, particle fineness is 5 μm, and print thickness is 30 μm.Sheet glass complete drying at 120 DEG C is made after being completed for printing.Use vacuum magnetic-control sputtering to carry out sputter coating to dried sheet glass, acquisition reflecting layer and protective layer structure are Cr/SiNx (x=1-1.5), and wherein Cr layer thickness is 12-18nm, SiNx layer thickness is 18-25nm, and sputtering condition is as shown in table 1.After plated film completes, clear water sheet glass being put into 40 DEG C soaks 48h, then uses high pressure water flushing wash clean, obtains the sheet glass that various dash area as shown in drawings has silvery white mirror metal gloss.
Table 1
| Reflecting layer | Protective layer | |
| Target | Cr | Si*4 |
| N 2/ Ar flow | 1000Ar | 800/1000 |
| Sputtering power | 20kw | 40kw |
| Glass walking speed | 3m/min | 3m/min |
| Sheet glass temperature | 150℃ | 150℃ |
Embodiment 2
The preparation various glass with mirror image effect as illustrated in the accompanying drawings from 1 to 3, in figure, dash area representative has the pattern of mirror reflection effect.First adopt routine techniques to make silk screen printing web plate, make web plate have the pierced pattern of non-shaded portion in figure, for subsequent use.According to desired size, sheet glass is cut, edging and tempering, then with the above-mentioned web plate prepared, silk screen printing is carried out to sheet glass, when controlling to print, sheet glass temperature is at about 45 DEG C, the non-shaded portion of sheet glass is covered by water-based colored glazed glass ink completely, rosin water color ink selected by described water-based colored glazed glass ink, particle fineness is 10 μm, and print thickness is 30 μm.Sheet glass complete drying at 120 DEG C is made after being completed for printing.Use vacuum magnetic-control sputtering to carry out sputter coating to dried sheet glass, acquisition reflecting layer and protective layer structure are Ti/SiNx (x=1-1.5), and wherein Ti layer thickness is 14-20nm, SiNx layer thickness is 18-25nm, and sputtering condition is as shown in table 2.After plated film completes, clear water sheet glass being put into 40 DEG C soaks 48h, then uses high pressure water flushing wash clean, obtains the sheet glass that various dash area as shown in drawings has silvery white mirror metal gloss.
Table 2
| Reflecting layer | Protective layer | |
| Target | Ti | Si*3 |
| N 2/ Ar flow | 1000Ar | 600/1200 |
| Sputtering power | 20kw | 50kw |
| Glass walking speed | 3m/min | 2.5m/min |
| Sheet glass temperature | 150℃ | 150℃ |
Claims (10)
1. there is a preparation method for the glass of mirror image effect, comprise the steps: that (1) makes web plate: make and there is the web plate with the pierced pattern of required pattern complementary; (2) screen printing: select water-based colored glazed glass ink, carries out silk screen printing with the web plate that step (1) is made to sheet glass; (3) dry: dry after printing with the sheet glass of required pierced pattern; (4) sputter coating: need to select suitable target to carry out overall vacuum magnetron sputtering plating to the one side that sheet glass is printed with water-based colored glazed glass ink according to specular color; (5) clean: after plated film, the water-based colored glazed glass ink be attached on sheet glass is cleaned up.
2. a kind of preparation method with the glass of mirror image effect according to claim 1, is characterized in that: the particle fineness of described water-based colored glazed glass ink is 0.5-30 μm.
3. a kind of preparation method with the glass of mirror image effect according to claim 1, is characterized in that: the thickness of described water-based colored glazed glass ink printing is 10-50 μm, is preferably 30 μm.
4. a kind of preparation method with the glass of mirror image effect according to claim 1, is characterized in that: in the web manufacturing process of described step (2), and controlling the temperature of sheet glass when printing is more than 30 DEG C.
5. a kind of preparation method with the glass of mirror image effect according to claim 1, is characterized in that: the drying course of described step (3) carries out at 110-160 DEG C.
6. a kind of preparation method with the glass of mirror image effect according to claim 1; it is characterized in that: the sputter coating process of described step (4) makes the openwork part of uncoated water-based colored glazed glass ink in glass sheet surface obtain the coatings with mirror image effect, and this coatings comprises reflecting layer and protective layer.
7. a kind of preparation method with the glass of mirror image effect according to claim 6, is characterized in that: described reflecting layer is one or more in Cr, CrNx, NiCr, NiCrNx, Ti, TiOx, TiNx, and thickness is 1-30nm; Described protective layer is one or more in SiNx, SiNxOy, SnOx, and thickness is 1-50nm.
8. a kind of preparation method with the glass of mirror image effect according to claim 1, it is characterized in that: the cleaning process described in described step (5) comprises, soak more than 24h by the clear water of the sheet glass after sputter coating more than 40 DEG C, and then rinse well with the water-based colored glazed glass ink of high pressure water by glass sheet surface.
9. have a glass for mirror image effect, have the mirror effect pattern of any fraction of coverage, the coatings that this mirror effect pattern is formed by vacuum magnetron sputtering coating film is formed.
10. a kind of glass with mirror image effect according to claim 9, it is characterized in that: described coatings comprises reflecting layer and protective layer, described reflecting layer is one or more in Cr, CrNx, NiCr, NiCrNx, Ti, TiOx, TiNx, and thickness is 1-30nm; Described protective layer can be one or more in SiNx, SiNxOy, SnOx, and thickness is 1-50nm.
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| CN201410606172.3A CN104355550A (en) | 2014-10-31 | 2014-10-31 | Glass with mirror surface pattern effect and preparation method thereof |
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| CN201410606172.3A CN104355550A (en) | 2014-10-31 | 2014-10-31 | Glass with mirror surface pattern effect and preparation method thereof |
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Cited By (16)
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| CN106830699A (en) * | 2017-03-31 | 2017-06-13 | 北京海逸风传媒股份有限公司 | A kind of lamp piece and preparation method |
| CN108218244A (en) * | 2018-03-07 | 2018-06-29 | 吴江南玻华东工程玻璃有限公司 | A kind of production method of patterned coated glass |
| CN109423607A (en) * | 2017-09-01 | 2019-03-05 | 福建省辉锐电子技术有限公司 | A method of coated cover-plate is prepared using continuous magnetron sputtering sedimentation |
| CN109422468A (en) * | 2017-09-01 | 2019-03-05 | 福建省辉锐电子技术有限公司 | A method of the coated cover-plate with two or more colors |
| CN109664628A (en) * | 2018-12-21 | 2019-04-23 | 东莞市银泰丰光学科技有限公司 | A kind of production method of novel dumb light anti-dazzle glas |
| CN109719394A (en) * | 2017-10-31 | 2019-05-07 | 蓝思科技（长沙）有限公司 | A kind of processing method of LOGO |
| CN110029918A (en) * | 2018-01-12 | 2019-07-19 | 中国南玻集团股份有限公司 | Hollow glass, glass curtain wall and application |
| CN110357448A (en) * | 2019-07-23 | 2019-10-22 | 嘉善银升玻璃有限公司 | Glass surface high temperature drawing pattern science and engineering skill |
| CN110713348A (en) * | 2019-09-30 | 2020-01-21 | 联想(北京)有限公司 | Electronic device and method for manufacturing glass cover plate |
| CN110819957A (en) * | 2019-11-26 | 2020-02-21 | 天津北玻玻璃工业技术有限公司 | Method for producing coated pattern glass |
| CN110835237A (en) * | 2019-05-14 | 2020-02-25 | 信义玻璃工程（东莞）有限公司 | Method for manufacturing firm color glazed glass and firm color glazed glass |
| CN113320305A (en) * | 2020-02-28 | 2021-08-31 | 深圳市万普拉斯科技有限公司 | Logo making method and terminal |
| CN113747710A (en) * | 2021-08-27 | 2021-12-03 | 维达力实业(深圳)有限公司 | Cover plate, preparation method thereof and electronic equipment |
| CN114737151A (en) * | 2022-03-22 | 2022-07-12 | 东莞市微科光电科技有限公司 | Lens coating process |
| CN115321831A (en) * | 2022-09-13 | 2022-11-11 | 咸宁南玻节能玻璃有限公司 | Method for preparing patterned glass by toughening and coating |
| CN116590656A (en) * | 2023-05-17 | 2023-08-15 | 广州今泰科技股份有限公司 | Surface treatment method for metal surface water-based shielding inter-plating |
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| CN113320305A (en) * | 2020-02-28 | 2021-08-31 | 深圳市万普拉斯科技有限公司 | Logo making method and terminal |
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