CN104327720B - A kind of wear-resisting grease proofing coatings - Google Patents

A kind of wear-resisting grease proofing coatings Download PDF

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Publication number
CN104327720B
CN104327720B CN201410613169.4A CN201410613169A CN104327720B CN 104327720 B CN104327720 B CN 104327720B CN 201410613169 A CN201410613169 A CN 201410613169A CN 104327720 B CN104327720 B CN 104327720B
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parts
wear
agent
ultrasonic disperse
grease proofing
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CN104327720A (en
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田野
张晓�
魏珍
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Yangzhou Lubao artificial turf Co. Ltd.
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田野
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Priority to CN201610413363.7A priority patent/CN105860834B/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C09D183/04—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of wear-resisting grease proofing coatings, its raw material includes by weight: silica white 40 44 parts, acrylic resin 26 29 parts, nitrile rubber 18 21 parts, ethanedioic acid polyester 10 15 parts, modified graphene 22 25 parts, zinc oxide 6 10 parts, defoamer 1.6 2 parts, levelling agent 1.5 1.8 parts, dispersant 1.1 1.4 parts, coalescents 1.6 1.8 parts, antioxidant 4020 1 1.3 parts, drier 36 parts, antifungus agent 1.2 1.5 parts, antisettling agent 1.5 1.8 parts, antirust agent 0.6 1 parts.The present invention has high-wear resistance and good oil preventing performance.

Description

A kind of wear-resisting grease proofing coatings
Technology neighborhood
The present invention relates to coatings technology neighborhood, particularly relate to a kind of wear-resisting anti-oil-insulation and be coated with Material.
Background technology
Coatings is charged or indispensable the processing raw material of the hardware of static electrification, coatings It is coated on hardware, it is possible to prevent the electric spark owing to contacting with each other, colliding generation, keep away Exempt from that security incident occurs, but, the anti-wear performance of this coating is not strong, easily due to component Mutually rub and be peeling, thus safety in production is brought serious hidden danger, it addition, Some industries such as PETROLEUM PROCESSING industry, oil stain also can produce erosion, destroy, lead coatings Cause the destruction of coatings.
Summary of the invention
The technical problem that basic background technology exists, the present invention proposes a kind of wear-resisting anti-oil-insulation Coating, has high-wear resistance and good oil preventing performance.
The wear-resisting grease proofing coatings of one that the present invention proposes, its raw material includes by weight: silicon Rubber powder 40-44 part, acrylic resin 26-29 part, nitrile rubber 18-21 part, ethanedioic acid gathers Ester 10-15 part, modified graphene 22-25 part, zinc oxide 6-10 part, defoamer 1.6-2 Part, levelling agent 1.5-1.8 part, dispersant 1.1-1.4 part, coalescents 1.6-1.8 part, Antioxidant 4020 1-1.3 part, drier 3-6 part, antifungus agent 1.2-1.5 part, anti-precipitation Agent 1.5-1.8 part, antirust agent 0.6-1 part；
In the preparation process of modified graphene, by weight by 7-9 part Graphene, 11-13 part Concentration be the sodium nitrite solution of 1.2-1.5mmol/L and 16-18 part hexanol to put into first anti- Answer container, stir 1.2-1.6h with the mixing speed of 110-120rpm, add 1.2-1.5 part Concentration is the sulfuric acid solution of 96-98wt%, and the first reaction vessel is warming up to 63-66 DEG C, with After the mixing speed stirring 1-1.5h of 110-130rpm, it is cooled to 22-26 DEG C, centrifugation After be dried to obtain material A, the speed of centrifugation is 3500-3700rpm；By material A, 3-6 Part acetone, 4-8 part vitamin C, 6-9 part ortho-nitraniline add the second reaction vessel, quiet After putting 20-22h, ultrasonic disperse 1.4-1.8h obtains material B, and the frequency of ultrasonic disperse is 36-40KHz, the power of ultrasonic disperse is 1100-1300W, filters, is dried to obtain modified stone Ink alkene.
Preferably, the mesh number of silica white is 200-400 mesh.
Preferably, in nitrile rubber, acrylonitrile content is 31-35wt%.
Preferably, silica white, acrylic resin, the weight ratio of nitrile rubber are 41-42:27-28: 19-20。
Preferably, its raw material includes by weight: silica white 41-42, acrylic resin 27-28 Part, nitrile rubber 19-20 part, ethanedioic acid polyester 12-13 part, modified graphene 23-24 part, Zinc oxide 7-9 part, defoamer 1.7-1.8 part, levelling agent 1.6-1.7 part, dispersant 1.2-1.3 Part, coalescents 1.7-1.8 part, antioxidant 4020 1.1-1.2 part, drier 4-5 part, Antifungus agent 1.3-1.4 part, antisettling agent 1.6-1.7 part, antirust agent 0.8-0.9 part.
Preferably, in the preparation process of modified graphene, by weight by 7.5-8 part Graphene, 11.5-12 part concentration be the sodium nitrite solution of 1.3-1.4mmol/L and 16.5-17 part just oneself The first reaction vessel put into by alcohol, stirs 1.3-1.5h with the mixing speed of 116-119rpm, adds Entering 1.3-1.4 part concentration is the sulfuric acid solution of 96-98wt%, is warming up to by the first reaction vessel 64-65 DEG C, after stirring 1.3-1.4h with the mixing speed of 115-120rpm, it is cooled to 23-24 DEG C, being dried to obtain material A after centrifugation, the speed of centrifugation is 3580-3600rpm；By material A, 4-5 part acetone, 5-7 part vitamin C, 7-8 part neighbour's nitre Base aniline adds the second reaction vessel, and after standing 21-21.5h, ultrasonic disperse 1.6-1.7h obtains Material B, the frequency of ultrasonic disperse is 38-39KHz, and the power of ultrasonic disperse is 1200-1230W, Filter, be dried to obtain modified graphene.
The present invention using silica white, acrylic resin, nitrile rubber and ethanedioic acid polyester coordinate as Film forming matter, makes the present invention possess good insulating properties and wear-resisting, oil preventing performance, selection 200-400 mesh silica white has abundant microcellular structure, high-specific surface area, high activity, it is possible to and Other film forming matters together, constitute a tridimensional network, improve the insulating properties of the present invention, Fully adsorb simultaneously, accommodate various auxiliary agent, make the film forming of the present invention, curing rate fast and storage Stability is high, and the nitrile rubber that alkene nitrile content is 31-35wt% has good oil resistance And insulating properties, further increase the insulation of the present invention, oil resistance；Modified graphene and Zinc oxide with the use of, substantially increase the anti-wear performance of the present invention, wherein modified graphene is It is made up through ortho-nitraniline modification of Graphene, in modifying process, graphenic surface and adjacent nitre Amido link is formed so that ortho-nitraniline is firmly grafted on Graphene table between base aniline molecule Face, on the one hand improves Graphene dispersibility in the present invention, on the other hand, is grafted The modified graphene of ortho-nitrophenyl amine molecule, the amino that can be contained by its surface and film forming matter In itrile group polar interaction, enhance the interface interaction of modified graphene and film forming matter, Make both the most compatible, it addition, the alkyl bond in modified graphene can divide with film forming matter Son is fully wound around, and further improves stablizing of " film forming matter-modified graphene " structure Property so that the present invention is when by External Force Acting, it is possible to effectively by load transfer to physical mechanical On the modified graphene that performance is extremely strong, thus substantially increase the anti-wear performance of the present invention.
Detailed description of the invention
Below, by specific embodiment, technical scheme is described in detail.
Embodiment 1
The wear-resisting grease proofing coatings of one that the present invention proposes, its raw material includes by weight: silicon Rubber powder 44 parts, acrylic resin 26 parts, nitrile rubber 21 parts, ethanedioic acid polyester 10 parts, Modified graphene 25 parts, zinc oxide 6 parts, defoamer 2 parts, levelling agent 1.5 parts, dispersion Agent 1.4 parts, coalescents 1.6 parts, antioxidant 4020 1.3 parts, drier 3 parts, mildew-resistant Agent 1.5 parts, antisettling agent 1.5 parts, antirust agent 1 part；Wherein, silica white is 200 mesh, In nitrile rubber, acrylonitrile content is 35wt%；
In the preparation process of modified graphene, by weight by 7 parts of Graphenes, 13 parts of concentration The first reaction vessel put into for sodium nitrite solution and 18 parts of hexanol of 1.2mmol/L, Stir 1.6h with the mixing speed of 110rpm, add the sulphuric acid that 1.2 parts of concentration is 98wt% molten Liquid, is warming up to 63 DEG C by the first reaction vessel, after stirring 1h with the mixing speed of 130rpm, Being cooled to 26 DEG C, be dried to obtain material A after centrifugation, the speed of centrifugation is 3500rpm；Material A, 6 parts of acetone, 4 parts of vitamin Cs, 9 parts of ortho-nitranilines are added Second reaction vessel, after standing 20h, ultrasonic disperse 1.8h obtains material B, ultrasonic disperse Frequency is 36KHz, and the power of ultrasonic disperse is 1300W, filters, is dried to obtain modified graphite Alkene.
Embodiment 2
The wear-resisting grease proofing coatings of one that the present invention proposes, its raw material includes by weight: silicon Rubber powder 40 parts, acrylic resin 29 parts, nitrile rubber 18 parts, ethanedioic acid polyester 15 parts, Modified graphene 22 parts, zinc oxide 10 parts, defoamer 1.6 parts, levelling agent 1.8 parts, point Powder 1.1 parts, coalescents 1.8 parts, antioxidant 4020 1 part, drier 6 parts, anti- Mould dose 1.2 parts, antisettling agent 1.8 parts, antirust agent 0.6 part；Wherein, silica white is 400 Mesh, in nitrile rubber, acrylonitrile content is 31wt%；
In the preparation process of modified graphene, by weight by 9 parts of Graphenes, 11 parts of concentration The first reaction vessel put into for sodium nitrite solution and 16 parts of hexanol of 1.5mmol/L, Stir 1.2h with the mixing speed of 120rpm, add the sulphuric acid that 1.5 parts of concentration is 96wt% molten Liquid, is warming up to 66 DEG C by the first reaction vessel, stirs 1.5h with the mixing speed of 110rpm After, it being cooled to 22 DEG C, after centrifugation, be dried to obtain material A, the speed of centrifugation is 3700rpm；Material A, 3 parts of acetone, 8 parts of vitamin Cs, 6 parts of ortho-nitranilines are added Second reaction vessel, after standing 22h, ultrasonic disperse 1.4h obtains material B, ultrasonic disperse Frequency is 40KHz, and the power of ultrasonic disperse is 1100W, filters, is dried to obtain modified graphite Alkene.
Embodiment 3
The wear-resisting grease proofing coatings of one that the present invention proposes, its raw material includes by weight: silicon Rubber powder 42, acrylic resin 27 parts, nitrile rubber 20 parts, ethanedioic acid polyester 12 parts, change Property Graphene 24 parts, zinc oxide 7 parts, defoamer 1.8 parts, levelling agent 1.6 parts, dispersion Agent 1.3 parts, coalescents 1.7 parts, antioxidant 4020 1.2 parts, drier 4 parts, anti- Mould dose 1.4 parts, antisettling agent 1.6 parts, antirust agent 0.9 part；Wherein, silica white is 280 Mesh, in nitrile rubber, acrylonitrile content is 33wt%；
In the preparation process of modified graphene, by weight by 7.5 parts of Graphenes, 12 parts dense The first reaction vessel that sodium nitrite solution and the 17 parts of hexanol that degree is 1.3mmol/L is put into, Stir 1.5h with the mixing speed of 116rpm, add the sulphuric acid that 1.3 parts of concentration is 98wt% molten Liquid, is warming up to 64 DEG C by the first reaction vessel, stirs 1.3h with the mixing speed of 120rpm After, it being cooled to 24 DEG C, after centrifugation, be dried to obtain material A, the speed of centrifugation is 3580rpm；Material A, 5 parts of acetone, 5 vitamin Cs, 8 parts of ortho-nitranilines are added the Two reaction vessels, after standing 21h, ultrasonic disperse 1.7h obtains material B, the frequency of ultrasonic disperse Rate is 38KHz, and the power of ultrasonic disperse is 1230W, filters, is dried to obtain modified graphene.
Embodiment 4
The wear-resisting grease proofing coatings of one that the present invention proposes, its raw material includes by weight: silicon Rubber powder 41, acrylic resin 28 parts, nitrile rubber 19 parts, ethanedioic acid polyester 13 parts, change Property Graphene 23 parts, zinc oxide 9 parts, defoamer 1.7 parts, levelling agent 1.7 parts, dispersion Agent 1.2 parts, coalescents 1.8 parts, antioxidant 4020 1.1 parts, drier 5 parts, anti- Mould dose 1.3 parts, antisettling agent 1.7 parts, antirust agent 0.8 part；Wherein, silica white is 300 Mesh, in nitrile rubber, acrylonitrile content is 32wt%；
In the preparation process of modified graphene, by weight by 8 parts of Graphenes, 11.5 parts dense Sodium nitrite solution that degree is 1.4mmol/L and the first reaction that 16.5 parts of hexanol are put into are held Device, stirs 1.3h with the mixing speed of 119rpm, and adding 1.4 parts of concentration is the sulfur of 96wt% Acid solution, is warming up to 65 DEG C by the first reaction vessel, stirs 1.4h with the mixing speed of 115rpm After, it being cooled to 23 DEG C, after centrifugation, be dried to obtain material A, the speed of centrifugation is 3600rpm；Material A, 4 parts of acetone, 7 parts of vitamin Cs, 7 parts of ortho-nitranilines are added Second reaction vessel, after standing 21.5h, ultrasonic disperse 1.6h obtains material B, ultrasonic disperse Frequency be 39KHz, the power of ultrasonic disperse is 1200W, filters, is dried to obtain modified stone Ink alkene.
The above, the only present invention preferably detailed description of the invention, but the protection model of the present invention Enclose and be not limited thereto, any be familiar with the technical staff of this technology neighborhood in the skill that the invention discloses In the range of art, according to technical scheme and inventive concept equivalent in addition thereof or change Become, all should contain within protection scope of the present invention.

Claims (6)

1. a wear-resisting grease proofing coatings, it is characterised in that its raw material includes by weight: Silica white 40-44 part, acrylic resin 26-29 part, nitrile rubber 18-21 part, ethanedioic acid Polyester 10-15 part, modified graphene 22-25 part, zinc oxide 6-10 part, defoamer 1.6-2 Part, levelling agent 1.5-1.8 part, dispersant 1.1-1.4 part, coalescents 1.6-1.8 part, Antioxidant 4020 1-1.3 part, drier 3-6 part, antifungus agent 1.2-1.5 part, anti-precipitation Agent 1.5-1.8 part, antirust agent 0.6-1 part；
In the preparation process of modified graphene, by weight by 7-9 part Graphene, 11-13 part Concentration be the sodium nitrite solution of 1.2-1.5mmol/L and 16-18 part hexanol to put into first anti- Answer container, stir 1.2-1.6h with the mixing speed of 110-120rpm, add 1.2-1.5 part Concentration is the sulfuric acid solution of 96-98wt%, and the first reaction vessel is warming up to 63-66 DEG C, with After the mixing speed stirring 1-1.5h of 110-130rpm, it is cooled to 22-26 DEG C, centrifugation After be dried to obtain material A, the speed of centrifugation is 3500-3700rpm；By material A, 3-6 Part acetone, 4-8 part vitamin C, 6-9 part ortho-nitraniline add the second reaction vessel, quiet After putting 20-22h, ultrasonic disperse 1.4-1.8h obtains material B, and the frequency of ultrasonic disperse is 36-40KHz, the power of ultrasonic disperse is 1100-1300W, filters, is dried to obtain modified stone Ink alkene.
The most wear-resisting grease proofing coatings, it is characterised in that silica gel The mesh number of powder is 200-400 mesh.
Wear-resisting grease proofing coatings the most according to claim 1 or claim 2, it is characterised in that In nitrile rubber, acrylonitrile content is 31-35wt%.
The most wear-resisting grease proofing coatings, it is characterised in that silica gel Powder, acrylic resin, the weight ratio of nitrile rubber are 41-42:27-28:19-20.
The most wear-resisting grease proofing coatings, it is characterised in that it is former Material includes by weight: silica white 41-42, acrylic resin 27-28 part, nitrile rubber 19-20 Part, ethanedioic acid polyester 12-13 part, modified graphene 23-24 part, zinc oxide 7-9 part, disappear Infusion 1.7-1.8 part, levelling agent 1.6-1.7 part, dispersant 1.2-1.3 part, coalescents 1.7-1.8 part, antioxidant 4020 1.1-1.2 part, drier 4-5 part, antifungus agent 1.3-1.4 Part, antisettling agent 1.6-1.7 part, antirust agent 0.8-0.9 part.
The most wear-resisting grease proofing coatings, it is characterised in that modified In the preparation process of Graphene, by weight by 7.5-8 part Graphene, 11.5-12 part concentration Sodium nitrite solution and 16.5-17 part hexanol for 1.3-1.4mmol/L put into the first reaction Container, stirs 1.3-1.5h with the mixing speed of 116-119rpm, adds 1.3-1.4 part dense Degree is the sulfuric acid solution of 96-98wt%, and the first reaction vessel is warming up to 64-65 DEG C, with After the mixing speed stirring 1.3-1.4h of 115-120rpm, it is cooled to 23-24 DEG C, centrifugal point Being dried to obtain material A after from, the speed of centrifugation is 3580-3600rpm；By material A, 4-5 part acetone, 5-7 part vitamin C, 7-8 part ortho-nitraniline add the second reaction vessel, After standing 21-21.5h, ultrasonic disperse 1.6-1.7h obtains material B, and the frequency of ultrasonic disperse is 38-39KHz, the power of ultrasonic disperse is 1200-1230W, filters, is dried to obtain modified stone Ink alkene.
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CN201610413363.7A CN105860834B (en) 2014-11-05 2014-11-05 A kind of wear-resisting grease proofing coatings

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CN104817894A (en) * 2015-05-05 2015-08-05 广西高农机械有限公司 Composite fireproof coating used for agriculture machinery
CN104861856A (en) * 2015-05-29 2015-08-26 王俐帧 Modified wear-resistance paint for casts
CN105754474A (en) * 2016-03-28 2016-07-13 无锡锡能锅炉有限公司 High-temperature-resistant coating material for biomass fuel boiler wall
CN106497165A (en) * 2016-11-21 2017-03-15 郑州源冉生物技术有限公司 A kind of electronic equipment heat-conductive coating and preparation method thereof
CN106519757A (en) * 2016-11-21 2017-03-22 郑州源冉生物技术有限公司 Thermal conductive coating for heat dissipation of electronic device
CN107384063A (en) * 2017-08-17 2017-11-24 安徽卓越电力设备有限公司 Lithium battery surface antirust paint and preparation method thereof
CN108864936A (en) * 2018-07-26 2018-11-23 合肥广民建材有限公司 A kind of external wall waterproof insulation coating and preparation method thereof
CN109378948B (en) * 2018-09-28 2020-07-14 温岭市钢锋冲件有限公司 Production process of silicon steel stamped steel

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CN102453419B (en) * 2010-10-26 2014-08-27 福建瑞森化工有限公司 External insulation cleaning protective agent and preparation method thereof
US9085710B2 (en) * 2011-08-30 2015-07-21 Illinois Tool Works Inc. Toughened epoxy system for abrasion resistant coatings
KR102016474B1 (en) * 2012-04-20 2019-09-02 삼성전기주식회사 Insulating composition for substrate, prepreg and substrate using the same
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CN104327720A (en) 2015-02-04

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