CN104327263A - Glucose resin preparation method - Google Patents
Glucose resin preparation method Download PDFInfo
- Publication number
- CN104327263A CN104327263A CN201410522481.2A CN201410522481A CN104327263A CN 104327263 A CN104327263 A CN 104327263A CN 201410522481 A CN201410522481 A CN 201410522481A CN 104327263 A CN104327263 A CN 104327263A
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- China
- Prior art keywords
- glucose
- resin
- ammonia water
- concentrated ammonia
- strong aqua
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a glucose resin preparation method, which is characterized in that the raw materials comprise 100-120 parts of glucose and 25-30 parts of 25 DEG concentrated ammonia water, the glucose is dissolved in water to obtain a solution with a concentration of 60-90 wt%, heating is performed under stirring to achieve a temperature of 120-125 DEG C, the concentrated ammonia water is slowly added within a range of 30-40 min, the concentrated ammonia water adding process is maintained at a range of 120+/-5, stirring is performed for 30-40 min after completing the addition of the concentrated ammonia water, and filtration, separation dehydration and drying are sequentially performed to obtain the product. The glucose resin preparation method has advantages of easily available raw materials, low cost and nature and green property. The product can be eaten, can be used as the ion exchange resin, and can be used as the antibiotics carrier in the medicine industry or used for reducing the gastric acid strength.
Description
Technical field
The invention belongs to a kind of technological method of deep processing of farm products.
Background technology
Resin is a kind of from various plants, the particularly secretory product of hydrocarbon (hydrocarbon polymer) class of conifer.Because the chemical structure that it is special, and can use as the material such as emulsion paint and cementing agent, therefore be taken seriously it and be worth.It is the mixture of multiple macromolecular compound.Resin can be divided into natural resin and synthetic resins two kinds.This is a kind of itself to only have natural resin, but with showing the development of chemical industry, having and much being produced by the polymkeric substance of synthetic, and the chemical property of some polymkeric substance central and physical properties can be very similar with natural resin, and therefore, polymkeric substance can be called as synthetic resins.Its generation trees produce resin different reasons, and therefore scientist makes different viewpoints for this reason.More scientist's approval, plant, with resin seal wound, to kill insect and to prevent fungi from invading, and eliminates the too much metabolite of production, but up to the present, goes back neither one answer certainly.In order to extract resin, generally will in bark partial application, and want simple and cut out one and rotate downward pipeline (being called resin canal), make resin flow out Hou, along resin canal flowing, until drip to collection place.If bark is too hard, uses alcohol (as: methyl alcohol and ethanol etc.) softening or dissolving the fibrous tissue of bark possibly, could resin be collected.Hou under drop of resin, meeting and air produce chemical reaction, can continue and gradually harden, and form solid.Its chemical property resin is a kind of liquid of stickiness, and its main ingredient is the terpenoid substance being easier to volatilize, and makes resin have special taste.Also containing the nonvolatile sticky solid be dissolved in terpenes, so when resin exposes in atmosphere, terpenoid substance vapors away, and makes resin viscosity increase, form solid.In the alkene of its composition, based on the ene compound of double-ring; Time of the ene compound of monocycle shape.Use fractionating process can separate the different fraction of molecular weight, to make different purposes.
Retrieve through Chinese publication, do not have to find the scheme identical with the present invention.
Summary of the invention:
The object of the invention is to; A kind of preparation method of edible glucose resin is proposed
The preparation method of glucose resin of the present invention, is characterized in that: raw materials of glucose 100-120 part, 25 degree of strong aqua 25-30 parts, glucose is dissolved in the water, obtain the solution of the 60-90% concentration of weight percent meter, be under agitation heated to 120-125 DEG C, add strong aqua by 30-40 minute scope lentamente, add strong aqua process to protect in 120 native 5 scopes, after adding strong aqua, stir 30-40 minute, filter, separating and dehydrating, is drying to obtain product.
The present invention compared with prior art its beneficial effect is: have raw material and be easy to get, cost is low, natural green, advantage.Product edible, can make ion exchange resin, is applicable to medicine industry and does antibiotic carrier or reduce hydrochloric acid in gastric juice intensity.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but embodiments of the present invention are not limited thereto.
Embodiment
The present invention is raw materials used buys acquisition.
The preparation method of glucose resin of the present invention, is characterized in that: raw materials of glucose 100-120 part, 25 degree of strong aqua 25-30 parts, glucose is dissolved in the water, obtain the solution of the 60-90% concentration of weight percent meter, be under agitation heated to 120-125 DEG C, add strong aqua by 30-40 minute scope lentamente, add strong aqua process to protect in 120 native 5 scopes, after adding strong aqua, stir 30-40 minute, filter, separating and dehydrating, is drying to obtain product.
Precaution: add strong aqua, control to add speed, make that value is unlikely rises to more than neutrality, to keep away the coking of rabbit sugar part.
Quality product: rosin products nitrogenous 6.3%; Absorption sun, ion energy are every gram of 1.6 millinormal sodium; Calcium or barium; The ability of adsorpting anion is every gram of 10 millinormal sulfate radicals or 0.9 millinormal chlorine root.
This rosin products edible, can make ion exchange resin, is applicable to medicine industry and does antibiotic carrier or reduce hydrochloric acid in gastric juice intensity.
Claims (1)
1. a preparation method for glucose resin, is characterized in that: raw materials of glucose 100-120 part, 25 degree of strong aqua 25-30 parts, glucose is dissolved in the water, obtain the solution of the 60-90% concentration of weight percent meter, be under agitation heated to 120-125 DEG C, add strong aqua by 30-40 minute scope lentamente, add strong aqua process to protect in 120 native 5 scopes, after adding strong aqua, stir 30-40 minute, filter, separating and dehydrating, is drying to obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410522481.2A CN104327263A (en) | 2014-09-30 | 2014-09-30 | Glucose resin preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410522481.2A CN104327263A (en) | 2014-09-30 | 2014-09-30 | Glucose resin preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104327263A true CN104327263A (en) | 2015-02-04 |
Family
ID=52402074
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410522481.2A Pending CN104327263A (en) | 2014-09-30 | 2014-09-30 | Glucose resin preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104327263A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110894407A (en) * | 2019-11-26 | 2020-03-20 | 山东柯帷博伟耐火材料有限公司 | Formaldehyde-free binder and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101274948A (en) * | 2008-05-08 | 2008-10-01 | 缪泽年 | D-aminoglucose and preparation thereof |
| CN101463238A (en) * | 2009-01-12 | 2009-06-24 | 西北大学 | Preparation of environment protection type adhesive |
| CN101775045A (en) * | 2009-12-07 | 2010-07-14 | 汪昔奇 | Method for preparing glucosamine hydrochloride |
-
2014
- 2014-09-30 CN CN201410522481.2A patent/CN104327263A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101274948A (en) * | 2008-05-08 | 2008-10-01 | 缪泽年 | D-aminoglucose and preparation thereof |
| CN101463238A (en) * | 2009-01-12 | 2009-06-24 | 西北大学 | Preparation of environment protection type adhesive |
| CN101775045A (en) * | 2009-12-07 | 2010-07-14 | 汪昔奇 | Method for preparing glucosamine hydrochloride |
Non-Patent Citations (1)
| Title |
|---|
| 刘北平等: ""C5H11O5CHO母液制取焦糖色素的研究"", 《常德师范学院学报(自然科学版)》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110894407A (en) * | 2019-11-26 | 2020-03-20 | 山东柯帷博伟耐火材料有限公司 | Formaldehyde-free binder and application thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150204 |