CN104325727A - Preparation method for red-mud expanded perlite decoration and thermal insulation integrated light wall material - Google Patents

Preparation method for red-mud expanded perlite decoration and thermal insulation integrated light wall material Download PDF

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Publication number
CN104325727A
CN104325727A CN201410535335.3A CN201410535335A CN104325727A CN 104325727 A CN104325727 A CN 104325727A CN 201410535335 A CN201410535335 A CN 201410535335A CN 104325727 A CN104325727 A CN 104325727A
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Prior art keywords
red mud
mud
red
decoration
wall material
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CN201410535335.3A
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CN104325727B (en
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唐竹兴
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Shandong University of Technology
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Shandong University of Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B9/00Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
    • B32B9/002Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising natural stone or artificial stone
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B33/00Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B30/00Compositions for artificial stone, not containing binders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2607/00Walls, panels

Abstract

A preparation method for a red-mud expanded perlite decoration and thermal insulation integrated light wall material is characterized in that the red-mud expanded perlite decoration and thermal insulation integrated light wall material is prepared by performing high-temperature sintering on an extrusion-formed red-mud expanded pearl plate and a red-mud coated expanded pearl granule. The prepared red-mud expanded perlite decoration and thermal insulation integrated light wall material is formed by employing one-step sintering, the surface decoration is the red-mud expanded pearl plate prepared through extrusion forming, so that six surfaces of the wall material all have colorful decoration, the integrality is strong; an internal/external wall material with single color, composite color and other various colors and patterns is prepared by adding a ceramic color agent, extra decoration is not needed, the production technology is simple, the cost is low, the building thermal insulation effect is good, energy is saved and environment is protected; and the produced red-mud expanded perlite decoration and thermal insulation integrated light wall material integrates multiple functions such as decoration, warm keeping, water prevention, heat insulation, sound insulation, shock preventing and the like.

Description

The preparation method of the heat insulation integrated light wall material of red mud expanded pearlite decorative
Technical field
The present invention relates to the preparation method of the heat insulation integrated light wall material of red mud expanded pearlite decorative, belong to field of ceramic preparation technology.
Background technology
The heat insulation integrated light wall material of red mud expanded pearlite decorative is collection decoration, heat insulation integrated New Type Light-weight Wall Material, being adopt colored microcrystalline glass decorating wall material, is a kind of novel wall material with decoration, insulation, heat insulation, waterproof, sound insulation and the function integration such as shockproof.Current construction material generally adopts structural clay tile, cement hollow building blocks and air-entrained concrete building block etc., these construction material heat-insulating properties and decorate properties poor, needing when being applied to inner, external wall additionally to add tiling or wallpaper, is the construction material that manufacturing cost is high.
Summary of the invention
The object of this invention is to provide the preparation method of the heat insulation integrated light wall material of red mud expanded pearlite decorative that a kind of serviceability is excellent, production cost is low, its technical scheme is:
the heat insulation integrated light wall material of red mud expanded pearlite decorative is formed through high-temperature firing by extrusion molding red mud expanded pearlite rock beam and the coated expanded perlite granule material of red mud, and concrete preparation method comprises the following steps:
The first step: after red mud and zirconium slag industrial waste are mixed and made into mixed powder with the ratio uniform that weight ratio is 5 ~ 8:2 ~ 5, the water of additional 40 ~ 60% is mixed and made into mud, the ratio uniform of to be the expanded perlite of 2 ~ 5mm again by this mud and particle diameter with weight ratio be 100:20 ~ 50 mixes, and makes the coated expanded perlite granule material of red mud through drying;
Second step: be that mixed powder, kaolin and the ceramic toner prepared in the expanded perlite fine powder of 0.1 ~ 0.5mm, the first step mixes with the ratio uniform that weight ratio is 10 ~ 35:10 ~ 35:77 ~ 20:3 ~ 10 again by granularity, the sodium humate of additional 1 ~ 2wt% and the water Homogeneous phase mixing of 18 ~ 25wt% make plastic mud material again, make thickness is 3 ~ 20mm, width is 100 ~ 500mm red mud expanded pearlite rock beam and dry through vacuum pugging extruder for shaping;
3rd step: first adopt load bearing board left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and will hold burn mould inner surface coat releasing agent, then the red mud expanded pearlite rock beam prepared in second step is distributed in the bottom of holding and burning mould and the medial surface holding burning mould, again by the red mud coated expanded perlite granule material plain cloth prepared in the first step in wherein, and then the red mud expanded pearlite rock beam prepared in second step is covered in top layer, 1 ~ 5 hour is incubated at the temperature of 650 ~ 850 DEG C, crystallization at the temperature of 400 ~ 750 DEG C, anneal 5 ~ 15 hours, through cooling, the heat insulation integrated light wall material of red mud expanded pearlite decorative is made in cutting and surface treatment.
Compared with prior art, its advantage is in the present invention:
1, the heat insulation integrated light wall material of red mud expanded pearlite decorative that prepared by the present invention have employed once-firing, incrustation makes red mud expanded pearlite rock beam by extrusion molding, make the equal chromatic colour decoration in this materials for wall six faces, globality is strong, there is stronger decoration, insulation, waterproof, heat insulation, sound insulation and antiknock quality, production technology is simple, can be mass-produced;
2, the heat insulation integrated light wall material of red mud expanded pearlite decorative that prepared by the present invention can be prepared into the interior and exterior decoration material of the colors such as monochrome, tertiary colour and pattern by adding ceramic toner;
3, the heat insulation integrated light wall material of red mud expanded pearlite decorative prepared of the present invention is owing to have employed once-firing, and without the need to additional decoration, reduces cost significantly, and building heat preservation is effective, energy-saving and environmental protection.
Detailed description of the invention
embodiment 1
The first step: by red mud and zirconium slag industrial waste with weight ratio be after the ratio uniform of 1:1 is mixed and made into mixed powder additional 40% water be mixed and made into mud, the ratio uniform of to be the expanded perlite of 2mm again by this mud and particle diameter with weight ratio be 100:20 mixes, and makes the coated expanded perlite granule material of red mud through drying;
Second step: the ratio uniform mixing by the mixed powder prepared in the expanded perlite fine powder of granularity 0.5mm, the first step, kaolin and ceramic toner with weight ratio being 10:10:77:3 again, the sodium humate of additional 1wt% and the water Homogeneous phase mixing of 18wt% make plastic mud material again, make thickness is 3mm, width is 100mm red mud expanded pearlite rock beam and dry through vacuum pugging extruder for shaping;
3rd step: first adopt load bearing board left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and will hold burn mould inner surface coat releasing agent, then the red mud expanded pearlite rock beam plain cloth prepared in second step is burnt the medial surface of mould in holding the bottom of burning mould and holding, again coated for the red mud prepared in first step expanded perlite granule material is distributed in wherein, and then the red mud expanded pearlite rock beam prepared in second step is covered in top layer, 1 hour is incubated at the temperature of 650 DEG C, crystallization at the temperature of 400 DEG C, anneal 5 hours, through cooling, the heat insulation integrated light wall material of red mud expanded pearlite decorative is made in cutting and surface treatment.
The purity of testing proportion material used is technical pure.
embodiment 2
The first step: by red mud and zirconium slag industrial waste with weight ratio be after the ratio uniform of 6.5:3.5 is mixed and made into mixed powder additional 50% water be mixed and made into mud, the ratio uniform of to be the expanded perlite of 3.5mm again by this mud and particle diameter with weight ratio be 100:35 mixes, and makes the coated expanded perlite granule material of red mud through drying;
Second step: the ratio uniform mixing by the mixed powder prepared in the expanded perlite fine powder of granularity 0.3mm, the first step, kaolin and ceramic toner with weight ratio being 23:23:49:5 again, the sodium humate of additional 1.5wt% and the water Homogeneous phase mixing of 22wt% make plastic mud material again, make thickness is 11mm, width is 300mm red mud expanded pearlite rock beam and dry through vacuum pugging extruder for shaping;
3rd step: first adopt load bearing board left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and will hold burn mould inner surface coat releasing agent, then the red mud expanded pearlite rock beam prepared in second step is distributed in the bottom of holding and burning mould and the medial surface holding burning mould, again by the red mud coated expanded perlite granule material plain cloth prepared in the first step in wherein, and then the red mud expanded pearlite rock beam prepared in second step is covered in top layer, 3 hours are incubated at the temperature of 750 DEG C, crystallization at the temperature of 600 DEG C, anneal 10 hours, through cooling, the heat insulation integrated light wall material of red mud expanded pearlite decorative is made in cutting and surface treatment.
The purity of testing proportion material used is technical pure.
embodiment 3
The first step: by red mud and zirconium slag industrial waste with weight ratio be after the ratio uniform of 8:5 is mixed and made into mixed powder additional 60% water be mixed and made into mud, the ratio uniform of to be the expanded perlite of 5mm again by this mud and particle diameter with weight ratio be 100:50 mixes, and makes the coated expanded perlite granule material of red mud through drying;
Second step: the ratio uniform mixing by the mixed powder prepared in the expanded perlite fine powder of granularity 0.1mm, the first step, kaolin and ceramic toner with weight ratio being 35:35:20:10 again, the sodium humate of additional 2wt% and the water Homogeneous phase mixing of 25wt% make plastic mud material again, make thickness is 20mm, width is 500mm red mud expanded pearlite rock beam and dry through vacuum pugging extruder for shaping;
3rd step: first adopt load bearing board left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and will hold burn mould inner surface coat releasing agent, then the red mud expanded pearlite rock beam prepared in second step is distributed in the bottom of holding and burning mould and the medial surface holding burning mould, again by the red mud coated expanded perlite granule material plain cloth prepared in the first step in wherein, and then the red mud expanded pearlite rock beam prepared in second step is covered in top layer, 5 hours are incubated at the temperature of 850 DEG C, crystallization at the temperature of 750 DEG C, anneal 15 hours, through cooling, the heat insulation integrated light wall material of red mud expanded pearlite decorative is made in cutting and surface treatment.
The purity of testing proportion material used is technical pure.

Claims (1)

1. the preparation method of the heat insulation integrated light wall material of red mud expanded pearlite decorative, it is characterized in that: the heat insulation integrated light wall material of red mud expanded pearlite decorative is formed through high-temperature firing by extrusion molding red mud expanded pearlite rock beam and the coated expanded perlite granule material of red mud, and concrete preparation method comprises the following steps:
The first step: after red mud and zirconium slag industrial waste are mixed and made into mixed powder with the ratio uniform that weight ratio is 5 ~ 8:2 ~ 5, the water of additional 40 ~ 60% is mixed and made into mud, the ratio uniform of to be the expanded perlite of 2 ~ 5mm again by this mud and particle diameter with weight ratio be 100:20 ~ 50 mixes, and makes the coated expanded perlite granule material of red mud through drying;
Second step: be that mixed powder, kaolin and the ceramic toner prepared in the expanded perlite fine powder of 0.1 ~ 0.5mm, the first step mixes with the ratio uniform that weight ratio is 10 ~ 35:10 ~ 35:77 ~ 20:3 ~ 10 again by granularity, the sodium humate of additional 1 ~ 2wt% and the water Homogeneous phase mixing of 18 ~ 25wt% make plastic mud material again, make thickness is 3 ~ 20mm, width is 100 ~ 500mm red mud expanded pearlite rock beam and dry through vacuum pugging extruder for shaping;
3rd step: first adopt load bearing board left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and will hold burn mould inner surface coat releasing agent, then the red mud expanded pearlite rock beam prepared in second step is distributed in the bottom of holding and burning mould and the medial surface holding burning mould, again by the red mud coated expanded perlite granule material plain cloth prepared in the first step in wherein, and then the red mud expanded pearlite rock beam prepared in second step is covered in top layer, 1 ~ 5 hour is incubated at the temperature of 650 ~ 850 DEG C, crystallization at the temperature of 400 ~ 750 DEG C, anneal 5 ~ 15 hours, through cooling, the heat insulation integrated light wall material of red mud expanded pearlite decorative is made in cutting and surface treatment.
CN201410535335.3A 2014-10-13 2014-10-13 The preparation method of the heat insulation integrated light wall material of red mud expanded pearlite decorative Expired - Fee Related CN104325727B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104944914A (en) * 2015-05-25 2015-09-30 绥阳县华夏陶瓷有限责任公司 Red ceramic tile and manufacturing method thereof
CN108162550A (en) * 2018-01-18 2018-06-15 深圳市特斯拉科技实业有限公司 A kind of packaging material containing expanded perlite granule
CN110183132A (en) * 2019-07-15 2019-08-30 贵州大学 The method of red mud modified cement-concrete aggregate
CN111926990A (en) * 2020-08-10 2020-11-13 浩华环境科学有限责任公司 Exterior wall heat insulation building block and manufacturing method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1061935A (en) * 1990-11-26 1992-06-17 重庆建筑工程学院 Expanded perlite-cullet composite veneer
CN1066210A (en) * 1991-04-29 1992-11-18 重庆建筑工程学院 Pearlstone-low-temp ceramics colour glaze composite wall tile
US5558710A (en) * 1994-08-08 1996-09-24 Usg Interiors, Inc. Gypsum/cellulosic fiber acoustical tile composition
CN101560111A (en) * 2009-04-08 2009-10-21 吴汉阳 Foamed ceramics energy saving and heat preservation decorative wall brick and manufacture method thereof
CN102172967A (en) * 2011-03-14 2011-09-07 金同芳 Production equipment of plate material and wall material made of red mud
KR20120021003A (en) * 2010-08-31 2012-03-08 주식회사 디알하이텍 Functional nano element natural stone panel and manufacturing method thereof
CN103922674A (en) * 2014-04-10 2014-07-16 山东建筑大学 Method for producing light-weight wall material by using papermaking white clay

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1061935A (en) * 1990-11-26 1992-06-17 重庆建筑工程学院 Expanded perlite-cullet composite veneer
CN1066210A (en) * 1991-04-29 1992-11-18 重庆建筑工程学院 Pearlstone-low-temp ceramics colour glaze composite wall tile
US5558710A (en) * 1994-08-08 1996-09-24 Usg Interiors, Inc. Gypsum/cellulosic fiber acoustical tile composition
CN101560111A (en) * 2009-04-08 2009-10-21 吴汉阳 Foamed ceramics energy saving and heat preservation decorative wall brick and manufacture method thereof
KR20120021003A (en) * 2010-08-31 2012-03-08 주식회사 디알하이텍 Functional nano element natural stone panel and manufacturing method thereof
CN102172967A (en) * 2011-03-14 2011-09-07 金同芳 Production equipment of plate material and wall material made of red mud
CN103922674A (en) * 2014-04-10 2014-07-16 山东建筑大学 Method for producing light-weight wall material by using papermaking white clay

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104944914A (en) * 2015-05-25 2015-09-30 绥阳县华夏陶瓷有限责任公司 Red ceramic tile and manufacturing method thereof
CN108162550A (en) * 2018-01-18 2018-06-15 深圳市特斯拉科技实业有限公司 A kind of packaging material containing expanded perlite granule
CN110183132A (en) * 2019-07-15 2019-08-30 贵州大学 The method of red mud modified cement-concrete aggregate
CN111926990A (en) * 2020-08-10 2020-11-13 浩华环境科学有限责任公司 Exterior wall heat insulation building block and manufacturing method thereof
CN111926990B (en) * 2020-08-10 2021-07-02 浩华环境科学有限责任公司 Exterior wall heat insulation building block and manufacturing method thereof

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