CN104304335A - Mildew-resistant moisture-absorption double-effect preparation and preparation method thereof - Google Patents
Mildew-resistant moisture-absorption double-effect preparation and preparation method thereof Download PDFInfo
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- CN104304335A CN104304335A CN201410423881.8A CN201410423881A CN104304335A CN 104304335 A CN104304335 A CN 104304335A CN 201410423881 A CN201410423881 A CN 201410423881A CN 104304335 A CN104304335 A CN 104304335A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 33
- 238000010521 absorption reaction Methods 0.000 title claims abstract description 14
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 34
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims abstract description 34
- 244000037364 Cinnamomum aromaticum Species 0.000 claims abstract description 18
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims abstract description 18
- 235000013717 Houttuynia Nutrition 0.000 claims abstract description 18
- 240000000233 Melia azedarach Species 0.000 claims abstract description 18
- 235000015398 thunder god vine Nutrition 0.000 claims abstract description 18
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 17
- 229960005070 ascorbic acid Drugs 0.000 claims abstract description 17
- 235000010323 ascorbic acid Nutrition 0.000 claims abstract description 17
- 239000011668 ascorbic acid Substances 0.000 claims abstract description 17
- 239000001110 calcium chloride Substances 0.000 claims abstract description 17
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 17
- 229910001629 magnesium chloride Inorganic materials 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 240000000691 Houttuynia cordata Species 0.000 claims abstract 4
- 239000000843 powder Substances 0.000 claims description 21
- 241000218691 Cupressaceae Species 0.000 claims description 17
- 240000003377 Shepherdia canadensis Species 0.000 claims description 17
- 235000018324 Shepherdia canadensis Nutrition 0.000 claims description 17
- 239000006071 cream Substances 0.000 claims description 7
- 238000000605 extraction Methods 0.000 claims description 7
- 239000012467 final product Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 238000010992 reflux Methods 0.000 claims description 7
- 238000005516 engineering process Methods 0.000 abstract description 2
- 229920001661 Chitosan Polymers 0.000 abstract 1
- 241000972672 Phellodendron Species 0.000 abstract 1
- 241000580955 Sapindus mukorossi Species 0.000 abstract 1
- 241000830536 Tripterygium wilfordii Species 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 241000758769 Houttuynia Species 0.000 description 14
- 230000000694 effects Effects 0.000 description 5
- 239000003112 inhibitor Substances 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 206010016952 Food poisoning Diseases 0.000 description 1
- 208000019331 Foodborne disease Diseases 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
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Abstract
A disclosed mildew-resistant moisture-absorption double-effect preparation is mainly prepared from the following raw materials in parts by weight: 30 parts of chitosan, 20-30 parts of calcium chloride, 25-35 parts of magnesium chloride, 0.3-0.7 part of ascorbic acid, 14-26 parts of phellodendron, 25-35 parts of cordate houttuynia, 20-30 parts of cassia seed, 10-20 parts of tripterygium wilfordii, 15-25 parts of melia azedarach, and 16-24 parts of sapindus mukorossi. The invention also provides a preparation method of the mildew-resistant moisture-absorption double-effect preparation. Compared with the prior art, the prepared double-effect preparation is low in cost and simple in technology, possesses substantial mildew resistance and water adsorption performance, comprises the main compositions which are traditional Chinese medicine extractives, and is capable of substantially reducing environment pollution.
Description
Technical field
The present invention relates to a kind of preparation and preparation method thereof, be specifically related to a kind of to there is preparation of mildew-resistant and moisture absorption double effects and preparation method thereof.
Background technology
Along with the raising of China's expanding economy and living standards of the people, society increases day by day to the demand of mould inhibitor.Mould inhibitor Main Function suppresses microbial growth and breeding, prevents article from going mouldy, by insect pest, to extend the holding time of article.The article such as food, timber, clothing can be applied to, there is important effect in real life.
At present, existing mould inhibitor, based on chemical anti mildew agent, often contains the material in a large number to human body and bad environmental, such as, may cause cancer, cause deformity or cause food poisoning etc.In addition, most mould inhibitor only has the effect preventing from going mouldy, and effect is single.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the invention provides a kind of mildew-resistant moisture absorption double-effect preparation and preparation method thereof.
Technical scheme: for achieving the above object, the invention provides a kind of mildew-resistant moisture absorption double-effect preparation, and it is mainly made by the raw material of following weight ratio:
Shitosan 30 parts, calcium chloride 20-30 part, magnesium chloride 25-35 part, ascorbic acid 0.3-0.7 part,
Golden cypress 14-26 part, cordate houttuynia 25-35 part, cassia seed 20-30 part, thunder godvine 10-20 part,
Chinaberry 15-25 part, soapberry 16-24 part.
As preferably, described mildew-resistant moisture absorption double-effect preparation is mainly made by the raw material of following weight ratio:
Shitosan 30 parts, calcium chloride 22-28 part, magnesium chloride 28-32 part, ascorbic acid 0.4-0.6 part,
Golden cypress 18-22 part, cordate houttuynia 28-32 part, cassia seed 22-28 part, thunder godvine 12-18 part,
Chinaberry 18-22 part, soapberry 18-22 part.
Preferred as another kind, the molecular weight of described shitosan is 4000-6000.
Present invention also offers the preparation method of described mildew-resistant moisture absorption double-effect preparation, it is mainly made by following steps:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 6-10 times of volume water refluxing extraction 1-3 time, each 1-3 hour, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 60-100 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Beneficial effect: relative to prior art, the double-effect preparation of gained of the present invention, cost is low, and technique is simple, have significant mildew-resistant and water absorbing properties, and main component is Chinese medical extract, significantly can reduce environmental pollution.
Embodiment
Below in conjunction with embodiment, the present invention is further described.
Embodiment 1:
Prescription:
Shitosan 30g, calcium chloride 20g, magnesium chloride 25g, ascorbic acid 0.3g, golden cypress 14g, cordate houttuynia 25g,
Cassia seed 20g, thunder godvine 10g, chinaberry 15g, soapberry 16g.
The molecular weight of described shitosan is 4000.
Preparation method:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 6 times of volume water refluxing extraction 1 time, each 1 hour, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 60 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Embodiment 2:
Shitosan 30g, calcium chloride 30g, magnesium chloride 35g, ascorbic acid 0.7g, golden cypress 26g, cordate houttuynia 35g,
Cassia seed 30g, thunder godvine 20g, chinaberry 25g, soapberry 24g.
The molecular weight of described shitosan is 6000.
Preparation method:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 10 times of volume water refluxing extraction 3 times, each 3 hours, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 100 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Embodiment 3:
Shitosan 30g, calcium chloride 25g, magnesium chloride 30g, ascorbic acid 0.5g, golden cypress 20g, cordate houttuynia 30g,
Cassia seed 25g, thunder godvine 15g, chinaberry 20g, soapberry 20g.
The molecular weight of described shitosan is 5000.
Preparation method:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 8 times of volume water refluxing extraction 2 times, each 2 hours, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 80 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Embodiment 4:
Shitosan 30g, calcium chloride 22g, magnesium chloride 28g, ascorbic acid 0.4g, golden cypress 18g, cordate houttuynia 28g,
Cassia seed 22g, thunder godvine 12g, chinaberry 18g, soapberry 18g.
The molecular weight of described shitosan is 4500.
Preparation method:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 7 times of volume water refluxing extraction 1 time, each 2 hours, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 70 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Embodiment 5:
Shitosan 30g, calcium chloride 28g, magnesium chloride 32g, ascorbic acid 0.6g, golden cypress 22g, cordate houttuynia 32g,
Cassia seed 28g, thunder godvine 18g, chinaberry 22g, soapberry 22g.
The molecular weight of described shitosan is 5500.
Preparation method:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 6-10 times of volume water refluxing extraction 1-3 time, each 1-3 hour, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 60-100 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Experimental example invention formulation mildew-resistant water absorbing properties detects
Contrast 1 group and adopt prescription of the present invention and preparation method, do not comprise the double-effect preparation obtained by golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry;
Contrast 2 groups and adopt prescription of the present invention, each raw material grinds through pulverizing, the double-effect preparation obtained by simple physical mixing;
Invention formulation mildew-resistant water absorbing properties testing result is in table 1
Table 1 gained preparation of the present invention mildew-resistant water absorbing properties testing result (n=3)
Note: compared with control group, * P<0.05
By upper Biao Ke get, compared with two control groups, the embodiment of the present invention 3,4 and 5 gained economic benefits and social benefits are through detecting, and result shows its mildew-resistant preventive effect and after 30 days, water absorption rate is significantly increased, and have significant mildew-resistant and water suction double effects, and environmental sound.
Claims (4)
1. a mildew-resistant moisture absorption double-effect preparation, is characterized in that, it is mainly made by the raw material of following weight ratio:
Shitosan 30 parts, calcium chloride 20-30 part, magnesium chloride 25-35 part, ascorbic acid 0.3-0.7 part, golden cypress 14-26 part,
Cordate houttuynia 25-35 part, cassia seed 20-30 part, thunder godvine 10-20 part, chinaberry 15-25 part, soapberry 16-24 part.
2. mildew-resistant moisture absorption double-effect preparation according to claim 1, is characterized in that, it is mainly made by the raw material of following weight ratio:
Shitosan 30 parts, calcium chloride 22-28 part, magnesium chloride 28-32 part, ascorbic acid 0.4-0.6 part, golden cypress 18-22 part,
Cordate houttuynia 28-32 part, cassia seed 22-28 part, thunder godvine 12-18 part, chinaberry 18-22 part, soapberry 18-22 part.
3. mildew-resistant moisture absorption double-effect preparation according to claim 1, is characterized in that, the molecular weight of described shitosan is 4000-6000.
4. the preparation method of the mildew-resistant moisture absorption double-effect preparation described in any one of claim 1-3, is characterized in that, it is mainly made by following steps:
(1) get golden cypress, cordate houttuynia, cassia seed, thunder godvine, chinaberry and soapberry, add 6-10 times of volume water refluxing extraction 1-3 time, each 1-3 hour, merge extract, concentrated, dry, get dry extract;
(2) step (1) is residue obtained dry, pulverize to 60-100 order powder, obtains dry powder;
(3) shitosan, calcium chloride, magnesium chloride and ascorbic acid are mixed, then add above-mentioned dry cream and dry powder, mix, be ground into particle, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410423881.8A CN104304335B (en) | 2014-08-26 | 2014-08-26 | A kind of mildew-resistant moisture absorption double-effect preparation and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410423881.8A CN104304335B (en) | 2014-08-26 | 2014-08-26 | A kind of mildew-resistant moisture absorption double-effect preparation and preparation method thereof |
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| CN104304335A true CN104304335A (en) | 2015-01-28 |
| CN104304335B CN104304335B (en) | 2016-08-17 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105638757A (en) * | 2016-01-19 | 2016-06-08 | 黄伟洪 | Clothing drying and mold preventing bactericide |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088386A (en) * | 1992-12-25 | 1994-06-29 | 李晓云 | A kind of mildew-resistant, insect-proof agent and compound method thereof |
| US5391779A (en) * | 1992-07-27 | 1995-02-21 | Rohm And Haas Company | Stable extracts from neem seeds |
| CN102310966A (en) * | 2010-07-01 | 2012-01-11 | 郑州大学 | Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof |
| CN102600705A (en) * | 2012-04-10 | 2012-07-25 | 福建省中医药研究院 | Edible plant dryer |
-
2014
- 2014-08-26 CN CN201410423881.8A patent/CN104304335B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5391779A (en) * | 1992-07-27 | 1995-02-21 | Rohm And Haas Company | Stable extracts from neem seeds |
| CN1088386A (en) * | 1992-12-25 | 1994-06-29 | 李晓云 | A kind of mildew-resistant, insect-proof agent and compound method thereof |
| CN102310966A (en) * | 2010-07-01 | 2012-01-11 | 郑州大学 | Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof |
| CN102600705A (en) * | 2012-04-10 | 2012-07-25 | 福建省中医药研究院 | Edible plant dryer |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105638757A (en) * | 2016-01-19 | 2016-06-08 | 黄伟洪 | Clothing drying and mold preventing bactericide |
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| CN104304335B (en) | 2016-08-17 |
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Effective date of registration: 20231220 Address after: 511466 Jinzhou Jingang Avenue, Nansha District, Guangzhou City, Guangdong Province Zhuhai Circuit Biheju Central County 1-1301 Patentee after: He Hai Address before: 325200 20, Lane 1, Fei Yun Road, Fei Yun street, Ruian, Wenzhou, Zhejiang. Patentee before: Zhao Lan |
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