CN104297434A - Odor evaluation method for automotive interior parts - Google Patents

Odor evaluation method for automotive interior parts Download PDF

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Publication number
CN104297434A
CN104297434A CN201410597446.7A CN201410597446A CN104297434A CN 104297434 A CN104297434 A CN 104297434A CN 201410597446 A CN201410597446 A CN 201410597446A CN 104297434 A CN104297434 A CN 104297434A
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bag
odor evaluations
odor
parts
smell
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CN201410597446.7A
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CN104297434B (en
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王晓
钟加义
王志白
杨旭俭
傅强
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Chongqing Changan Automobile Co Ltd
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Chongqing Changan Automobile Co Ltd
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Abstract

The invention discloses an odor evaluation method for automotive interior parts. Through larger sample sizes and higher test requirements, discrimination of an odor source is increased, so that contribution of a part assembly to the odor of the whole automobile can be investigated more visually. Compared to odor evaluation on material types, the method can quickly locate the whole automobile odor contribution source and achieve odor change, so that the problem of misjudgment caused by poor local homogeneity of constituent materials of the parts is effectively solved, and detection missing of a small number of the constituent materials or auxiliary materials of the complicated part assembly is prevented.

Description

A kind of Odor Evaluations method of automotive trim parts
Technical field
The present invention relates to vehicle air quality management and control field, more specifically to a kind of Odor Evaluations method of automotive trim parts.
Background technology
In-car air quality problem more and more receives the concern of user, and people experience smell in car.Country at 2008 and successively issue in 2011 testing method and limits of in-vehicle air pollution, but in non-regulation car smell ranking method with accept standard.
Present most of automobile main frame maker, for improving air quality in vehicle, is all using or with reference to the Odor Evaluations method of German VDA270, is adopting 1L or 3L glass odor bottle to carry out smell subjective assessment test.As shown in Figure 3, this odor bottle 1 adopts glass material to make bottle 3, and can the bottle cap 2 of airtight odor bottle with one, this bottle cap 2 can use the resistant to elevated temperatures sealing strip composition of the making of the material of glass tape frosted or glass cover and free from extraneous odour, quantitative standard model 4 is loaded in bottle 3, then at three temperature (23 DEG C, 40 DEG C, 80 DEG C), odor evaluation test is carried out respectively, the odor dispersion situation of simulated automotive under indoor temperature, outdoor temperature and high-temperature condition.Because the method only intercepts quantitative standard model 4 to automotive trim parts/material, in the good situation of material homogeneity of interior trim parts/material, the method can well the raw-material odor dispersion situation of across comparison unlike material or different manufacturers, but if test sample material homogeneity is bad just there will be larger erroneous judgement.When current domestic technology is low and cost control is strict, the homogeneity that material is good also cannot be accomplished.In addition, because the method is material level test evaluation, if the smell source of certain car load need be investigated, then need to investigate one by one the hundreds of kind composition starting material of parts all in car, experimental project amount is huge, add the reason that material homogeneity is bad, adopt the method to bring larger difficulty to the smell investigation of car load and rectification.
Summary of the invention
The object of this invention is to provide a kind of Odor Evaluations method of automotive trim parts, to solve car interior trim parts because material homogeneity is bad, parts material composition is complicated, existing material level Odor Evaluations method is adopted to be difficult to investigate the problem in car load smell source.
The Odor Evaluations method of automotive trim parts of the present invention, comprises the following steps:
The preparation of step one, Odor Evaluations bag
1. Odor Evaluations bag only has one end open, and this opening is sealed by sealing strip, and is provided with gas-filled switching tube on Odor Evaluations bag, described Odor Evaluations bag, sealing strip and gas-filled switching tube by free from extraneous odour and the material of resistance to more than 150 DEG C temperature make.
2. guarantee that the impermeability of Odor Evaluations bag is good;
3. be the burin-in process of under the condition of 80 DEG C, Odor Evaluations bag being carried out at least 24h in temperature.
The preparation of step 2, parts to be measured
Load in the polybag of free from extraneous odour by surveying parts, after sealing, the constant temperature and humidity being placed into clean free from extraneous odour is indoor, temperature be 23 ± 2 DEG C, relative humidity places 24h under being the condition of 50% ± 5%.
Step 3: parts pack to be measured
1., at clean free from extraneous odour and in draughty laboratory, parts to be measured are loaded in Odor Evaluations bag, avoids parts to be measured to be polluted;
2. with reference to form one, the size according to parts to be measured is filled with quantitative pure air in Odor Evaluations bag.
Form one
Smell bag type Class1 Type 2 Type 3 Type 4 Type 5
Smell bag size (long × wide) 35×35cm 70×60cm 120×120cm 190×110cm 200×128cm
Filled volume 3L 15L 60L 150L 300L
Step 4: constant temperature smell discharges
The Odor Evaluations bag that parts to be measured are housed is put into free from extraneous odour and with the constant temperature oven of air filtering system, be 60 ± 1 DEG C in temperature, 4h ± 0.2h carries out constant temperature process.
Step 5: smell subjective assessment
Under taking-up Odor Evaluations bag is placed on room temperature environment, when parts temperature is down to 50 ± 1 DEG C, slipper seal bar opens the opening of 10 ± 1cm width by one of Odor Evaluations bag jiao, evaluation personnel nose is from this extended distance 5 ± 1cm, outwards push Odor Evaluations bag, gas is overflowed, and evaluation personnel make oder levels and pass judgment in 10s.
Odor Evaluations requires:
1. Odor Evaluations personnel need through specialty smell the person of debating training and examine qualified.
2. an Odor Evaluations at least needs 3 evaluation personnel, if the evaluation result difference of the personnel of evaluation is greater than 1 grade, needs to substitute and reappraises, until the evaluation result difference of the personnel of evaluation is less than or equal to 1 grade.
Step 6: result evaluation
1. be final Appreciation gist with Odor Evaluations grade, level value shows that more greatly smell is larger, otherwise then less;
2. evaluation conclusion, is shown in form two; If final opinion rating is different, then take the principle that the minority is subordinate to the majority, get the grade that majority select.
Form two
Grade Feature interpretation
1 Smell is not discernable
2 Discernable, but very slight
3 Obviously discover, but can accept
4 Irritant smell, can not accept
5 There is intense stimulus smell, cannot stand
Further, Odor Evaluations bag, sealing strip and gas-filled switching tube are made by teflon.
Further, in step 3, for sticking or have sharp-pointed parts to be measured, then pack again after carrying out parcel process with PTFE film or clean aluminium foil, PE gloves or other clean free from extraneous odour gloves during pack, must be worn.
The Odor Evaluations method of automotive trim parts of the present invention, the composition material efficiently solving parts causes the problem judged by accident because local homogeneity is bad, also prevent minority's composition material of complex parts assembly or the undetected problem of auxiliary material simultaneously.What add smell source by adopting the testing requirements of larger sample volume and Geng Gao distinguishes limit, can investigate the smell percentage contribution of parts assembly to car load more intuitively.Relative to the Odor Evaluations of material type, this method can quick lock in car load smell contribution source go forward side by side promoting the circulation of qi taste rectification.
Accompanying drawing explanation
Fig. 1 is process flow diagram of the present invention;
The structural representation of Fig. 2 when to be that in the present invention, Odor Evaluations is packed have parts to be measured;
Fig. 3 is the schematic diagram of the Odor Evaluations method glass odor bottle used of existing German VDA270.
Embodiment
In order to explain technical scheme of the present invention further, below in conjunction with accompanying drawing, the present invention will be described in detail.
Shown in Fig. 1 and Fig. 2, the Odor Evaluations method of automotive trim parts, comprises the following steps:
The preparation of step one, Odor Evaluations bag
1. Odor Evaluations bag 5 only has one end open, this opening is sealed by sealing strip 6, and gas-filled switching tube 7 is provided with on Odor Evaluations bag, described Odor Evaluations bag 5, sealing strip 6 and gas-filled switching tube 7 are made by teflon, meet material free from extraneous odour and the requirement of ability more than 150 DEG C temperature.
2. adopt and vacuumize the impermeability that mode checks Odor Evaluations bag 5, guarantee that the impermeability of Odor Evaluations bag 5 is good.
3., before using, Odor Evaluations bag 5 is carried out to the burin-in process of at least 24h under the condition of temperature 80 DEG C.
The preparation of step 2, parts to be measured
Survey parts 8 are loaded in the polybag of free from extraneous odour, after sealing, the constant temperature and humidity being placed into clean free from extraneous odour is indoor, temperature be 21 DEG C (also or be 23 DEG C, 25 DEG C), relative humidity be 45% (also or be 50%, 60%) condition under place 24h.
Step 3: parts pack to be measured
1. at clean free from extraneous odour and in draughty laboratory, parts 8 to be measured are loaded in Odor Evaluations bag, parts to be measured are avoided to be polluted, for sticking or have sharp-pointed parts to be measured, pack again after then carrying out parcel process with PTFE film or clean aluminium foil, PE gloves or other clean free from extraneous odour gloves during pack, must be worn.
2. with reference to form one, the size according to parts to be measured is filled with quantitative pure air in Odor Evaluations bag.
Form one
Smell bag type Class1 Type 2 Type 3 Type 4 Type 5
Smell bag size (long × wide) 35×35cm 70×60cm 120×120cm 190×110cm 200×128cm
Filled volume 3L 15L 60L 150L 300L
Step 4: constant temperature smell discharges
The Odor Evaluations bag that parts to be measured are housed is put into free from extraneous odour and with the constant temperature oven of air filtering system, temperature be 59 DEG C (also or be 60 DEG C, 61 DEG C), 3.8h (also or be 4h, 4.2h) carries out constant temperature process.Due to when opening constant temperature oven, temperature can be caused to decline, during operation, thermostatic process at least 3.5h in specified for temperature ranges need be ensured.
Step 5: smell subjective assessment
General about 1min under taking-up Odor Evaluations bag is placed on room temperature environment, parts temperature will be down to about 50 DEG C, now, the opening that slipper seal bar is opened width be about 10cm by one of Odor Evaluations bag jiao, evaluation personnel nose is from extended distance about 5cm, outwards push Odor Evaluations bag 5 gently, gas is overflowed, evaluation personnel make level evaluation in 10s;
Odor Evaluations requires:
1. Odor Evaluations personnel need through specialty smell the person of debating training and examine qualified.
2. an Odor Evaluations at least needs 3 evaluation personnel, if the evaluation result difference of the personnel of evaluation is greater than 1 grade, needs to substitute and reappraises, until the evaluation result difference of the personnel of evaluation is less than or equal to 1 grade.
Step 6: result evaluation
1. be final Appreciation gist with Odor Evaluations grade, level value shows that more greatly smell is larger, otherwise then less;
2. evaluation conclusion, is shown in form two; If the opinion rating of three people is different, then take the principle that the minority is subordinate to the majority, get the grade that majority select.During evaluation procedure, allow to occur the situation between two kinds of evaluation ranks, such as three people are evaluated as 2.5 grades, 2.5 grades, 3 grades and then get 2.5 grades.
Form two
Grade Feature interpretation
1 Smell is not discernable
2 Discernable, but very slight
3 Obviously discover, but can accept
4 Irritant smell, can not accept
5 There is intense stimulus smell, cannot stand

Claims (3)

1. an Odor Evaluations method for automotive trim parts, is characterized in that: comprise the following steps:
The preparation of step one, Odor Evaluations bag
1. Odor Evaluations bag (5) only has one end open, this opening is sealed by sealing strip (6), and on Odor Evaluations bag, be provided with gas-filled switching tube (7), described Odor Evaluations bag, sealing strip and gas-filled switching tube by free from extraneous odour and the material of resistance to more than 150 DEG C temperature make;
2. guarantee that the impermeability of Odor Evaluations bag is good;
3. be the burin-in process of under the condition of 80 DEG C, Odor Evaluations bag being carried out at least 24h in temperature;
The preparation of step 2, parts to be measured
Load in the polybag of free from extraneous odour by surveying parts, after sealing, the constant temperature and humidity being placed into clean free from extraneous odour is indoor, temperature be 23 ± 2 DEG C, relative humidity places 24h under being the condition of 50% ± 5%;
Step 3, parts to be measured pack
1., at clean free from extraneous odour and in draughty laboratory, parts to be measured are loaded in Odor Evaluations bag, avoids parts to be measured to be polluted;
2. with reference to form one, the size according to parts to be measured is filled with quantitative pure air in Odor Evaluations bag;
Form one
Smell bag type Class1 Type 2 Type 3 Type 4 Type 5 Smell bag size (long × wide) 35×35cm 70×60cm 120×120cm 190×110cm 200×128cm Filled volume 3L 15L 60L 150L 300L
Step 4: constant temperature smell discharges
The Odor Evaluations bag that parts to be measured are housed is put into free from extraneous odour and with the constant temperature oven of air filtering system, be 60 ± 1 DEG C in temperature, 4h ± 0.2h carries out constant temperature process;
Step 5: smell subjective assessment
Under taking-up Odor Evaluations bag is placed on room temperature environment, when parts temperature is down to 50 ± 1 DEG C, slipper seal bar opens the opening of 10 ± 1cm width by one of Odor Evaluations bag jiao, evaluation personnel nose is from this extended distance 5 ± 1cm, outwards push Odor Evaluations bag, gas is overflowed, and evaluation personnel make oder levels and pass judgment in 10s;
Odor Evaluations requires:
1. Odor Evaluations personnel need through specialty smell the person of debating training and examine qualified;
2. an Odor Evaluations at least needs 3 evaluation personnel, if the evaluation result difference of the personnel of evaluation is greater than 1 grade, needs to substitute and reappraises, until the evaluation result difference of the personnel of evaluation is less than or equal to 1 grade;
Step 6: result evaluation
1. be final Appreciation gist with Odor Evaluations grade, level value shows that more greatly smell is larger, otherwise then less;
2. evaluation conclusion, is shown in form two; If final opinion rating is different, then take the principle that the minority is subordinate to the majority, get the grade that majority select;
Form two
Grade Feature interpretation 1 Smell is not discernable 2 Discernable, but very slight 3 Obviously discover, but can accept 4 Irritant smell, can not accept 5 There is intense stimulus smell, cannot stand
2. the Odor Evaluations method of automotive trim parts according to claim 1, is characterized in that: described Odor Evaluations bag, sealing strip and gas-filled switching tube are made by teflon.
3. the Odor Evaluations method of automotive trim parts according to claim 1 or 2, it is characterized in that: in step 3, for sticking or have sharp-pointed parts to be measured, pack again after then carrying out parcel process with PTFE film or clean aluminium foil, PE gloves or other clean free from extraneous odour gloves during pack, must be worn.
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Cited By (16)

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CN104764858A (en) * 2015-04-10 2015-07-08 北京汽车股份有限公司 Peculiar smell source detection cabin and vehicle peculiar smell source detection method
CN104807904A (en) * 2015-05-01 2015-07-29 长春富维—江森自控汽车饰件系统有限公司 Method for detecting smell of volatile matter monomer in non-metal material of automotive trim
CN105203706A (en) * 2015-09-15 2015-12-30 广州广电计量检测股份有限公司 Smell testing method
CN105223320A (en) * 2015-10-27 2016-01-06 神龙汽车有限公司 A kind of auto parts and components Odor Evaluations device and using method thereof
CN105842428A (en) * 2016-05-09 2016-08-10 紫荆花涂料(上海)有限公司 Method for evaluating odor of odorless paint or coatings
CN108889149A (en) * 2018-07-04 2018-11-27 中国汽车技术研究中心有限公司 A kind of calibrating gas configuration method for Odor Evaluations staff training
CN108918691A (en) * 2018-03-21 2018-11-30 北京卡达克数据有限公司 A kind of in-car smell substance determines method and in-car smell substance source tracing method
CN109521127A (en) * 2018-12-25 2019-03-26 广州广电计量检测股份有限公司 A kind of qualitative and quantitative analysis method carrying out Odor Evaluations to single odoring substance
CN110865147A (en) * 2019-09-25 2020-03-06 上海瀚海检测技术股份有限公司 Odor test and evaluation method for air conditioner evaporator
CN110927345A (en) * 2019-12-24 2020-03-27 奇瑞新能源汽车股份有限公司 Odor testing method for automotive interior trim part
CN111397996A (en) * 2020-06-08 2020-07-10 中汽研汽车零部件检验中心(宁波)有限公司 Odor standard gas preparation method based on odor intensity concentration relation
CN111693649A (en) * 2020-06-08 2020-09-22 中汽研汽车零部件检验中心(宁波)有限公司 Odor evaluation method for automobile part material by threshold method
CN112285296A (en) * 2020-11-11 2021-01-29 重庆长安汽车股份有限公司 Automobile interior part smell evaluation method based on electronic nose
CN112444617A (en) * 2019-09-04 2021-03-05 中国石油化工股份有限公司 Method for evaluating odor of polyolefin resin and use thereof
CN112740033A (en) * 2020-02-10 2021-04-30 华测检测认证集团股份有限公司 Preparation and use method of odor evaluation reference sample block of automotive interior part material
CN113588819A (en) * 2021-07-27 2021-11-02 重庆长安汽车股份有限公司 Quantitative evaluation method for odor of automobile interior part

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Cited By (24)

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CN104764858B (en) * 2015-04-10 2016-08-24 北京汽车股份有限公司 Sources of odor detection cabin and automobile sources of odor detection method
CN104764858A (en) * 2015-04-10 2015-07-08 北京汽车股份有限公司 Peculiar smell source detection cabin and vehicle peculiar smell source detection method
CN104807904A (en) * 2015-05-01 2015-07-29 长春富维—江森自控汽车饰件系统有限公司 Method for detecting smell of volatile matter monomer in non-metal material of automotive trim
CN105203706A (en) * 2015-09-15 2015-12-30 广州广电计量检测股份有限公司 Smell testing method
CN105223320A (en) * 2015-10-27 2016-01-06 神龙汽车有限公司 A kind of auto parts and components Odor Evaluations device and using method thereof
CN105842428A (en) * 2016-05-09 2016-08-10 紫荆花涂料(上海)有限公司 Method for evaluating odor of odorless paint or coatings
CN108918691A (en) * 2018-03-21 2018-11-30 北京卡达克数据有限公司 A kind of in-car smell substance determines method and in-car smell substance source tracing method
CN108918691B (en) * 2018-03-21 2021-06-22 中汽数据有限公司 Method for determining odor substances in vehicle and method for tracing odor substances in vehicle
CN108889149B (en) * 2018-07-04 2020-04-21 中国汽车技术研究中心有限公司 Standard gas configuration method for training odor evaluation personnel
CN108889149A (en) * 2018-07-04 2018-11-27 中国汽车技术研究中心有限公司 A kind of calibrating gas configuration method for Odor Evaluations staff training
CN109521127A (en) * 2018-12-25 2019-03-26 广州广电计量检测股份有限公司 A kind of qualitative and quantitative analysis method carrying out Odor Evaluations to single odoring substance
CN109521127B (en) * 2018-12-25 2021-11-26 广州广电计量检测股份有限公司 Qualitative and quantitative analysis method for evaluating odor of single odor substance
CN112444617B (en) * 2019-09-04 2023-05-23 中国石油化工股份有限公司 Odor evaluation method of polyolefin resin and application thereof
CN112444617A (en) * 2019-09-04 2021-03-05 中国石油化工股份有限公司 Method for evaluating odor of polyolefin resin and use thereof
CN110865147A (en) * 2019-09-25 2020-03-06 上海瀚海检测技术股份有限公司 Odor test and evaluation method for air conditioner evaporator
CN110927345A (en) * 2019-12-24 2020-03-27 奇瑞新能源汽车股份有限公司 Odor testing method for automotive interior trim part
CN110927345B (en) * 2019-12-24 2023-02-21 奇瑞新能源汽车股份有限公司 Odor testing method for automotive interior trim part
WO2021159255A1 (en) * 2020-02-10 2021-08-19 华测检测认证集团股份有限公司 Vehicle interior component material odor assessment reference sample preparation and use methods
CN112740033A (en) * 2020-02-10 2021-04-30 华测检测认证集团股份有限公司 Preparation and use method of odor evaluation reference sample block of automotive interior part material
CN112740033B (en) * 2020-02-10 2022-10-14 华测检测认证集团股份有限公司 Preparation and use method of odor evaluation reference sample block of automotive interior part material
CN111693649A (en) * 2020-06-08 2020-09-22 中汽研汽车零部件检验中心(宁波)有限公司 Odor evaluation method for automobile part material by threshold method
CN111397996A (en) * 2020-06-08 2020-07-10 中汽研汽车零部件检验中心(宁波)有限公司 Odor standard gas preparation method based on odor intensity concentration relation
CN112285296A (en) * 2020-11-11 2021-01-29 重庆长安汽车股份有限公司 Automobile interior part smell evaluation method based on electronic nose
CN113588819A (en) * 2021-07-27 2021-11-02 重庆长安汽车股份有限公司 Quantitative evaluation method for odor of automobile interior part

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