CN104293186A - Heat-resistant and flame-retardant soundproof oil paint and preparation method thereof - Google Patents
Heat-resistant and flame-retardant soundproof oil paint and preparation method thereof Download PDFInfo
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- CN104293186A CN104293186A CN201410469127.8A CN201410469127A CN104293186A CN 104293186 A CN104293186 A CN 104293186A CN 201410469127 A CN201410469127 A CN 201410469127A CN 104293186 A CN104293186 A CN 104293186A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a heat-resistant and flame-retardant soundproof oil paint. The heat-resistant and flame-retardant soundproof oil paint is characterized by being prepared from the following raw materials in parts by weight: 13-16 parts of vinyl ester resin, 3-5 parts of diamino diphenyl sulfone, 1-2 parts of aluminum isopropoxide, 1-3 parts of calcium stearate, 1-2 parts of glass beads, 1-3 parts of hollow microspheres, 2-3 parts of a nano wood fiber, 2-3 parts of a nano bamboo fiber, 2-4 parts of a carbon nanofiber, 42-47 parts of modified asphalt, 5-8 parts of modified waste resin sand, 0.5-1.0 part of pyrocatechin, 1-2 parts of tetrabutyl titanate, 2-3 parts of cassia oil, 1-2 parts of titanium dioxide, 2-3 parts of glass powder, 6-8 parts of methyl acrylate, 6-8 parts of n-butyl acetate, 8-11 parts of methylbenzene and 4-6 parts of hexamethyl phosphinous triamine. The glass beads added to the heat-resistant and flame-retardant soundproof oil paint disclosed by the invention have the characteristics of heat insulation property, sound insulation property, insulativity and low water absorption rate; the hollow microspheres have the characteristics of good sound insulation property, fire resistance and electrical insulating property and high strength; and the added titanium dioxide has strong heat resistance, weather fastness and chemical stability. A plurality of fibers are also added, so that the heat-resistant and flame-retardant soundproof oil paint is safe, environmentally friendly, and free of radiation, and has heat-conducting, antibacterial and bacteriostatic action; and modified waste resin sand is also added to the heat-resistant and flame-retardant soundproof oil paint, so that the problem of environmental pollution is solved, and the fire retardancy and the fire resistance of the oil paint are improved.
Description
Technical field
The present invention relates to a kind of paint and preparation method thereof, particularly a kind of heat-proof combustion-resistant silent paint and preparation method thereof.
Background technology
Boats and ships are among ocean environment for a long time, ocean and land natural condition difference are very large, and dying in ocean has salt fog and band slight alkalinity, has strong ultraviolet etc. simultaneously, and the etching condition that each position of boats and ships suffers varies, thus the requirement of paint is also had nothing in common with each other.Due to the larger psychology to human body of noise during vessel motion and health bringing all harm, for ensureing that the hearing of people is without prejudice, sleep quality is guaranteed, and the paint with deadening also more and more receives the concern of people.Always fire is the multiple accident of boats and ships, so in order to stop the harm that fire brings, ensures the safety of people's life and property, and flame retardant type paint is the emphasis of current urgent research.
Resin sand is formed by mixed preparing such as silica sand, resin and stiffening agents.The various organic resin contained inside the waste resin sand of bulk deposition or organic-inorganic compound, decomposition rate is slow, serious harm is brought to soil, and can acidified soil soil property, some compounds can along with the inflow rivers that drench with rain, polluted source, people, once drink, bring serious infringement can to the health of people.For this situation, waste resin sand is carried out modification by the present invention, not only solves environmental pollution, and adds in paint the effects such as the dirt-resisting dustproof that improve paint, ageing-resistant and fire prevention to.
Summary of the invention
The object of this invention is to provide a kind of heat-proof combustion-resistant silent paint and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of heat-proof combustion-resistant silent paint, is made up of the raw material of following weight part: vinyl ester resin 13-16, diamino diphenyl sulfone 3-5, aluminum isopropylate 1-2, calcium stearate 1-3, glass microballon 1-2, cenosphere 1-3, nanometer wood fibre 2-3, nano bamboo fiber 2-3, carbon nano fiber 2-4, modifying asphalt 42-47, modified abandoned resin sand 5-8, catechol 0.5-1.0, tetrabutyl titanate 1-2, oil of bay 2-3, titanium dioxide 1-2, glass powder 2-3, methyl acrylate 6-8, N-BUTYL ACETATE 6-8, toluene 8-11, hexamethyl sub-phosphono triamine 4-6;
Described modifying asphalt is made up of the raw material of following weight part: pitch 78-84, sulphur 0.4-1.0, Poly Propylene Wax 0.4-0.8, nano diatomite 0.5-1.0, diaminodiphenylmethane 0.3-0.7, gac 1-2, vinyl chloride-vinyl acetate resin 8-12, maleic anhydride 4-6, Potassium aluminum sulfate dodecahydrate 0.3-0.6, tetrahydrofuran (THF) 7-9, zirconium iso-octoate 0.2-0.4, dibenzoyl peroxide 0.05-0.12, sodium lignosulfonate 0.4-0.8, nano-glass scale 0.4-0.7; Preparation method is to melting by asphalt heating; maleic anhydride and dibenzoyl peroxide is slowly added under the protection of nitrogen; temperature is controlled at 170-180 ° of C; modifying asphalt is obtained stir 0.5-1 hour under 600-800 rev/min after; vinyl chloride-vinyl acetate resin, tetrahydrofuran (THF), zirconium iso-octoate, diaminodiphenylmethane, Poly Propylene Wax are mixed and heated to 130-150 ° of C; then will mix with modifying asphalt, then add all the other surplus materialss and with 800-1200 rev/min of lower agitation grinding 1-1.5 hour.
A kind of heat-proof combustion-resistant silent paint of the present invention, be made up of following concrete steps:
(1) modifying asphalt, vinyl ester resin, diamino diphenyl sulfone, N-BUTYL ACETATE, methyl acrylate, toluene, the sub-phosphono triamine of hexamethyl are added in reactor and are heated to 200-250 ° of C, after being uniformly mixed by mixture, under 600-800 rev/min, stir 2-3 hour;
(2) under identical rotating speed, add modified abandoned resin sand, glass microballon, cenosphere, nanometer wood fibre, nano bamboo fiber, carbon nano fiber, titanium dioxide, glass powder stirring 30-50 minute, temperature is reduced to 60-70 ° of C, add all the other remaining compositions again, stir in reactor, disperse, material after dispersion is added to grinding distribution in sand mill even, and stirs 20-30 minute under 1200-1400 rev/min;
(3) finely dispersed material is added in filter filters, after filtration, obtain the material that fineness is 20-40 μm, by the material package after filtering.
Discarded resin sand is added in shakeout to carry out knockout by modified abandoned resin sand preparation method of the present invention, the metal sundries on removing surface and dirt settling, again by the effect of waste resin sand by oscillator, whizzer, the binding agent on removing surface, again antiquated sand is worn into 400-600 order fine powder by ball mill, add the nano-attapulgite of antiquated sand weight 12%, 5% nano zine oxide, 0.4% Sodium hexametaphosphate 99, the alkylphenol polyoxyethylene of 0.2%, the silicon sol of 8% and 0.5-1% silane coupling agent KH560 mixed grinding evenly.
Advantage of the present invention is: the glass microballon that heat-proof combustion-resistant silent paint of the present invention adds has heat insulation, sound insulation, insulation, the feature that water-intake rate is low, cenosphere has sound-proofing, flame retardant resistance, electrical insulating property is good, and the feature that intensity is high, the titanium dioxide added has very strong thermotolerance, weathering resistance and chemical stability, the present invention also adds multiple fiber safety and environmental protection, radiationless, and there is heat conduction, the effect of antibacterial bacteriostatic, the present invention also adds the waste resin sand of modification, solve a difficult problem for environmental pollution, and improve fire line and the resistivity against fire of paint.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of heat-proof combustion-resistant silent paint, is made up of the raw material of following weight part (kilogram): the sub-phosphono triamine 4 of vinyl ester resin 15, diamino diphenyl sulfone 3, aluminum isopropylate 1, calcium stearate 1, glass microballon 1, cenosphere 2, nanometer wood fibre 2, nano bamboo fiber 2, carbon nano fiber 3, modifying asphalt 42, modified abandoned resin sand 6, catechol 0.7, tetrabutyl titanate 1, oil of bay 2, titanium dioxide 1, glass powder 2, methyl acrylate 8, N-BUTYL ACETATE 8, toluene 10, hexamethyl;
Described modifying asphalt is made up of the raw material of following weight part (kilogram): pitch 82, sulphur 0.6, Poly Propylene Wax 0.5, nano diatomite 0.8, diaminodiphenylmethane 0.4, gac 1, vinyl chloride-vinyl acetate resin 9, maleic anhydride 4, Potassium aluminum sulfate dodecahydrate 0.4, tetrahydrofuran (THF) 8, zirconium iso-octoate 0.2, dibenzoyl peroxide 0.07, sodium lignosulfonate 0.5, nano-glass scale 0.5; Preparation method is to melting by asphalt heating; maleic anhydride and dibenzoyl peroxide is slowly added under the protection of nitrogen; temperature is controlled at 170-180 ° of C; modifying asphalt is obtained stir 0.5-1 hour under 600-800 rev/min after; vinyl chloride-vinyl acetate resin, tetrahydrofuran (THF), zirconium iso-octoate, diaminodiphenylmethane, Poly Propylene Wax are mixed and heated to 130-150 ° of C; then will mix with modifying asphalt, then add all the other surplus materialss and with 800-1200 rev/min of lower agitation grinding 1-1.5 hour.
A kind of heat-proof combustion-resistant silent paint of the present invention, be made up of following concrete steps:
(1) modifying asphalt, vinyl ester resin, diamino diphenyl sulfone, N-BUTYL ACETATE, methyl acrylate, toluene, the sub-phosphono triamine of hexamethyl are added in reactor and are heated to 200-250 ° of C, after being uniformly mixed by mixture, under 600-800 rev/min, stir 2-3 hour;
(2) under identical rotating speed, add modified abandoned resin sand, glass microballon, cenosphere, nanometer wood fibre, nano bamboo fiber, carbon nano fiber, titanium dioxide, glass powder stirring 30-50 minute, temperature is reduced to 60-70 ° of C, add all the other remaining compositions again, stir in reactor, disperse, material after dispersion is added to grinding distribution in sand mill even, and stirs 20-30 minute under 1200-1400 rev/min;
(3) finely dispersed material is added in filter filters, after filtration, obtain the material that fineness is 20-40 μm, by the material package after filtering.
Discarded resin sand is added in shakeout to carry out knockout by modified abandoned resin sand preparation method of the present invention, the metal sundries on removing surface and dirt settling, again by the effect of waste resin sand by oscillator, whizzer, the binding agent on removing surface, again antiquated sand is worn into 400-600 order fine powder by ball mill, add the nano-attapulgite of antiquated sand weight 12%, 5% nano zine oxide, 0.4% Sodium hexametaphosphate 99, the alkylphenol polyoxyethylene of 0.2%, the silicon sol of 8% and 0.5-1% silane coupling agent KH560 mixed grinding evenly.
Paint paint film appearance flat smooth of the present invention, sticking power experiment (GB/T5210-2006) 5.4Mpa, salt water resistance (NaCl of 3%, 27 ° of C ± 6 ° C, 24h) paint film is non-foaming, do not come off, non-corrosive, water tolerance (27 ° of C ± 6 ° C, 240h) is non-foaming, do not come off, thermotolerance (130 ° of C) at least 600h, salt spray resistance (500h) paint film is non-foaming, do not come off, non-corrosive, artificial accelerated aging performance (500h) paint film without efflorescence, without variable color, flawless, abrasion-resistant (750g, 500 turns)/mg 14.
Claims (3)
1. a heat-proof combustion-resistant silent paint, it is characterized in that, be made up of the raw material of following weight part: vinyl ester resin 13-16, diamino diphenyl sulfone 3-5, aluminum isopropylate 1-2, calcium stearate 1-3, glass microballon 1-2, cenosphere 1-3, nanometer wood fibre 2-3, nano bamboo fiber 2-3, carbon nano fiber 2-4, modifying asphalt 42-47, modified abandoned resin sand 5-8, catechol 0.5-1.0, tetrabutyl titanate 1-2, oil of bay 2-3, titanium dioxide 1-2, glass powder 2-3, methyl acrylate 6-8, N-BUTYL ACETATE 6-8, toluene 8-11, hexamethyl sub-phosphono triamine 4-6,
Described modifying asphalt is made up of the raw material of following weight part: pitch 78-84, sulphur 0.4-1.0, Poly Propylene Wax 0.4-0.8, nano diatomite 0.5-1.0, diaminodiphenylmethane 0.3-0.7, gac 1-2, vinyl chloride-vinyl acetate resin 8-12, maleic anhydride 4-6, Potassium aluminum sulfate dodecahydrate 0.3-0.6, tetrahydrofuran (THF) 7-9, zirconium iso-octoate 0.2-0.4, dibenzoyl peroxide 0.05-0.12, sodium lignosulfonate 0.4-0.8, nano-glass scale 0.4-0.7; Preparation method is to melting by asphalt heating; maleic anhydride and dibenzoyl peroxide is slowly added under the protection of nitrogen; temperature is controlled at 170-180 ° of C; modifying asphalt is obtained stir 0.5-1 hour under 600-800 rev/min after; vinyl chloride-vinyl acetate resin, tetrahydrofuran (THF), zirconium iso-octoate, diaminodiphenylmethane, Poly Propylene Wax are mixed and heated to 130-150 ° of C; then will mix with modifying asphalt, then add all the other surplus materialss and with 800-1200 rev/min of lower agitation grinding 1-1.5 hour.
2. a kind of heat-proof combustion-resistant silent paint according to claim 1, is characterized in that, be made up of following concrete steps:
(1) modifying asphalt, vinyl ester resin, diamino diphenyl sulfone, N-BUTYL ACETATE, methyl acrylate, toluene, the sub-phosphono triamine of hexamethyl are added in reactor and are heated to 200-250 ° of C, after being uniformly mixed by mixture, under 600-800 rev/min, stir 2-3 hour;
(2) under identical rotating speed, add modified abandoned resin sand, glass microballon, cenosphere, nanometer wood fibre, nano bamboo fiber, carbon nano fiber, titanium dioxide, glass powder stirring 30-50 minute, temperature is reduced to 60-70 ° of C, add all the other remaining compositions again, stir in reactor, disperse, material after dispersion is added to grinding distribution in sand mill even, and stirs 20-30 minute under 1200-1400 rev/min;
(3) finely dispersed material is added in filter filters, after filtration, obtain the material that fineness is 20-40 μm, by the material package after filtering.
3. modified abandoned resin sand according to claim 1, it is characterized in that, discarded resin sand is added in shakeout to carry out knockout by preparation method, the metal sundries on removing surface and dirt settling, again waste resin sand is passed through oscillator, the effect of whizzer, the binding agent on removing surface, again antiquated sand is worn into 400-600 order fine powder by ball mill, add the nano-attapulgite of antiquated sand weight 12%, the nano zine oxide of 5%, the Sodium hexametaphosphate 99 of 0.4%, the alkylphenol polyoxyethylene of 0.2%, the silicon sol of 8% and the silane coupling agent KH560 mixed grinding of 0.5-1% are evenly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410469127.8A CN104293186A (en) | 2014-09-16 | 2014-09-16 | Heat-resistant and flame-retardant soundproof oil paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410469127.8A CN104293186A (en) | 2014-09-16 | 2014-09-16 | Heat-resistant and flame-retardant soundproof oil paint and preparation method thereof |
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| CN104293186A true CN104293186A (en) | 2015-01-21 |
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| CN201410469127.8A Pending CN104293186A (en) | 2014-09-16 | 2014-09-16 | Heat-resistant and flame-retardant soundproof oil paint and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106083011A (en) * | 2016-06-23 | 2016-11-09 | 合肥奇腾农业科技有限公司 | A kind of antibacterial and mouldproof insulation material and preparation method thereof |
| CN111621204A (en) * | 2020-04-16 | 2020-09-04 | 西卡(上海)管理有限公司 | Liquid sound insulation coating |
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| JPH08259850A (en) * | 1995-03-24 | 1996-10-08 | Shinto Paint Co Ltd | Undercoating composition |
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| CN102417783A (en) * | 2011-10-10 | 2012-04-18 | 漳州市奈特新型建材有限责任公司 | Waterproof/sealing paint with aqueous resin as main body |
| CN103013334A (en) * | 2012-11-28 | 2013-04-03 | 天长市开林化工有限公司 | Asphalt anticorrosive paint applied to hull bottoms |
| CN104004442A (en) * | 2013-02-27 | 2014-08-27 | 江苏时空涂料有限公司 | Preparation of non-toxic drinking water tank coating |
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2014
- 2014-09-16 CN CN201410469127.8A patent/CN104293186A/en active Pending
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| CN1072436A (en) * | 1992-10-16 | 1993-05-26 | 重庆建筑工程学院昆明分院 | Natural rubber breast modified waterproof asphalt material and preparation method thereof |
| JPH08259850A (en) * | 1995-03-24 | 1996-10-08 | Shinto Paint Co Ltd | Undercoating composition |
| CN1861719A (en) * | 2006-06-01 | 2006-11-15 | 江苏兰陵化工集团有限公司 | Anticorrosive ethenyl ester resin glass flake surface coating paint forwet flue desulfating equipment |
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| CN103013334A (en) * | 2012-11-28 | 2013-04-03 | 天长市开林化工有限公司 | Asphalt anticorrosive paint applied to hull bottoms |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106083011A (en) * | 2016-06-23 | 2016-11-09 | 合肥奇腾农业科技有限公司 | A kind of antibacterial and mouldproof insulation material and preparation method thereof |
| CN106083011B (en) * | 2016-06-23 | 2019-02-26 | 三博生化科技（上海）有限公司 | A kind of antibacterial and mouldproof thermal insulation material and preparation method thereof |
| CN111621204A (en) * | 2020-04-16 | 2020-09-04 | 西卡(上海)管理有限公司 | Liquid sound insulation coating |
| CN111621204B (en) * | 2020-04-16 | 2021-11-09 | 西卡(上海)管理有限公司 | Liquid sound insulation coating |
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Application publication date: 20150121 |
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