CN104186977A - Vitamin D3 beadlet and production method thereof - Google Patents
Vitamin D3 beadlet and production method thereof Download PDFInfo
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- CN104186977A CN104186977A CN201410391636.3A CN201410391636A CN104186977A CN 104186977 A CN104186977 A CN 104186977A CN 201410391636 A CN201410391636 A CN 201410391636A CN 104186977 A CN104186977 A CN 104186977A
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Abstract
The invention relates to the field of vitamin production, and particularly relates to a vitamin D3 beadlet which is long in expiration date and can be dispersed in cold water. The vitamin D3 beadlet comprises vitamin D3 oil, 2,6-ditertiary butyl-4-cresol, starch sodiilm octenylsuccinate, maltodextrin and pure water. A production method of the vitamin D3 beadlet comprises the following steps: firstly weighing, then dissolving the vitamin D3 oil, charging ethoxyquin; and adding the pure water in an emulsifying pot, charging the starch sodiilm octenylsuccinate, charging white sugar, waiting for emulsifying; adding a mixture in an oil dissolving kettle in the emulsifying pot, starting a fluidized bed system and a starch system for processing, and pumping the vitamin D3 beadlet out. The expiration date of the vitamin D3 beadlet produced by adopting the formula can reach 24 months, thus the service life of the vitamin D3 beadlet is prolonged, and the vitamin D3 beadlet can be dispersed in cold water, thus the use limit to the vitamin D3 beadlet can be reduced, and the use range is enlarged; meanwhile, compared with an existing standard formula, the formula and the production method have the advantages that the production cost can be greatly lowered, and the production benefit of enterprises is increased.
Description
Technical field
The present invention relates to vitamin production field, especially a kind of vitamin d3 beadlet and production method thereof.
Background technology
Vitamin d3 beadlet is the conventional product of feed addictive, and its whole use amount is larger.And there is following shortcoming in the vitamin d3 beadlet that existing standard recipe is produced:
1. shelf life of products only has 12 months, from production, completing the multistage dealer's of process running again enters retailer and user's hand again, elder may need to consume six months, therefore consumer only has limit the spendable time, and for enterprise, different period use amounts are indefinite, can cause a large amount of retinyl acetates to cause waste because of expired.
2. product can not disperse in cold water, and this defect causes in use required water environment need to be heated to uniform temperature, just can make it in water, disperse, and has caused unnecessary operation, causes the waste of the energy simultaneously.
3. in standard recipe, use gelatin as raw material, can have the risk that produces heavy metal pollution, the destruction that can cause ecological environment.
Summary of the invention
The object of the invention is provides a kind of long shelf-life, the vitamin d3 beadlet that can disperse in cold water and production method thereof in order to solve the deficiency of above-mentioned technology.
In order to achieve the above object, the vitamin d3 beadlet that the present invention is designed, it is by oleovitamin D3,2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in oleovitamin D3, pure vitamin D3 accounts for 1.2-1.5%, 2, and 6-di-t-butyl-4-cresols accounts for 1-2%, starch sodium octenyl succinate and accounts for that 5-60%, maltodextrin account for 30-80%, pure water accounts for 5-8%.
Wherein: described 2,6-di-t-butyl-4-cresols by ethoxyquin, replaced and shared percentage by weight constant.
Wherein: described maltodextrin by white sugar, replaced and shared percentage by weight constant.
The production method of vitamin d3 beadlet, first according to formula rate, each composition is weighed, then oleovitamin D3 is dropped in molten oily still, start to stir, and be heated to 50-70 ℃, melt to oleovitamin D3, after its clarification, make the temperature of molten oily still remain in the situation of 66-70 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols or ethoxyquin, stir 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is the 80-160% of solid content, be heated to 50-70 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into maltodextrin or the white sugar of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin or white sugar finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 10-30 minute, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 66-70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 400-500m.p.s, open fluidized system and starch systems, first starch systems is blown 5-10 minute starch to spray tower to fluid bed, the temperature of starch is controlled at 50-80 ℃, moisture 10%-13%, fluid bed EAT is controlled at 40-80 ℃, now open sprayer, adjust rotating speed to 40-50HZ, adjust gear pump pressure to 0.4-0.5Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 40-80 ℃, keep fluidized bed drying temperature 40-60 ℃, when the moisture drying to 15% of vitamin d3 beadlet, fluidized-bed temperature can be adjusted into 60-80 ℃ continues dry, when the moisture of vitamin d3 beadlet reaches 5% ± 1%, vitamin d3 beadlet is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
The resulting vitamin d3 beadlet of the present invention and production method thereof, the shelf-life of producing the vitamin d3 beadlet obtaining by this formula can reach 24 months, improves its service time, and it can disperse in cold water simultaneously, thereby can reduce, it is used to restriction, increase the scope of application; And this formula and production method are relative and existing standard formula, can reduce production costs greatly, improve the productivity effect of enterprise.
The specific embodiment
The present invention is further described by the following embodiment.
Embodiment 1:
The vitamin d3 beadlet that the present embodiment is described, it is by oleovitamin D3,2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in oleovitamin D3, pure vitamin D3 accounts for 1.2%, 2, and 6-di-t-butyl-4-cresols accounts for 1%, starch sodium octenyl succinate accounts for 12.8%, maltodextrin accounts for 80%, pure water accounts for 5%.
Embodiment 2:
The vitamin d3 beadlet that the present embodiment is described, it is by oleovitamin D3,2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in oleovitamin D3, pure vitamin D3 accounts for 1.5%, 2, and 6-di-t-butyl-4-cresols accounts for 2%, starch sodium octenyl succinate accounts for 60%, maltodextrin accounts for 30%, pure water accounts for 6.5%.
Embodiment 3:
The vitamin d3 beadlet that the present embodiment is described, it is comprised of oleovitamin D3, ethoxyquin, starch sodium octenyl succinate, maltodextrin and pure water, and wherein the percentage of the shared gross mass of each composition is: in oleovitamin D3, pure vitamin D3 accounts for 1.3%, ethoxyquin accounts for 1.5%, starch sodium octenyl succinate accounts for 41.2%, maltodextrin accounts for 50%, pure water accounts for 6%.
Embodiment 4:
The vitamin d3 beadlet that the present embodiment is described, it is by oleovitamin D3,2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, white sugar and pure water form, wherein the percentage of the shared gross mass of each composition is: in oleovitamin D3, pure vitamin D3 accounts for 1.4%, 2, and 6-di-t-butyl-4-cresols accounts for 1.6%, starch sodium octenyl succinate accounts for 30%, white sugar accounts for 60%, pure water accounts for 7%.
Embodiment 5:
The production method of the vitamin d3 beadlet that the present embodiment is described, first according to formula rate, each composition is weighed, then oleovitamin D3 is dropped in molten oily still, start to stir, and be heated to 50 ℃, melt to oleovitamin D3, after its clarification, make the temperature of molten oily still remain in the situation of 66 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols, stirs 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is 80% of solid content, be heated to 50 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into the maltodextrin of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 10 minutes, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 66 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 400m.p.s, open fluidized system and starch systems, first starch systems is blown 5 minutes starch to spray tower to fluid bed, the temperature of starch is controlled at 50 ℃, moisture 10%-13%, fluid bed EAT is controlled at 40 ℃, now open sprayer, adjust rotating speed to 40HZ, adjust gear pump pressure to 0.4Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 40 ℃, keep 40 ℃ of fluidized bed drying temperature, when the moisture drying to 15% of vitamin d3 beadlet, fluidized-bed temperature can be adjusted into 60 ℃ continues dry, when the moisture of vitamin d3 beadlet reaches 4%, vitamin d3 beadlet is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
Embodiment 6:
The production method of the vitamin d3 beadlet that the present embodiment is described, first according to formula rate, each composition is weighed, then oleovitamin D3 is dropped in molten oily still, start to stir, and be heated to 70 ℃, and melt to oleovitamin D3, after its clarification, make the temperature of molten oily still remain on the ethoxyquin that drops into formula ratio in the situation of 70 ℃, stir 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is 160% of solid content, be heated to 70 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into the maltodextrin of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 30 minutes, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 500m.p.s, open fluidized system and starch systems, first starch systems is blown 10 minutes starch to spray tower to fluid bed, the temperature of starch is controlled at 80 ℃, moisture 13%, fluid bed EAT is controlled at 80 ℃, now open sprayer, adjust rotating speed to 50HZ, adjust gear pump pressure to 0.5Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 80 ℃, keep fluidized bed drying temperature 60 C, when the moisture drying to 15% of vitamin d3 beadlet, fluidized-bed temperature can be adjusted into 80 ℃ continues dry, when the moisture of vitamin d3 beadlet reaches 6%, vitamin d3 beadlet is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
Embodiment 7:
The production method of the vitamin d3 beadlet that the present embodiment is described, first according to formula rate, each composition is weighed, then oleovitamin D3 is dropped in molten oily still, start to stir, and be heated to 60 ℃, melt to oleovitamin D3, after its clarification, make the temperature of molten oily still remain in the situation of 68 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols, stirs 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is 12% of solid content, be heated to 60 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into the white sugar of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing white sugar finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 20 minutes, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 68 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 450m.p.s, open fluidized system and starch systems, first starch systems is blown 5-10 minute starch to spray tower to fluid bed, the temperature of starch is controlled at 60 ℃, moisture 12%, fluid bed EAT is controlled at 60 ℃, now open sprayer, adjust rotating speed to 45HZ, adjust gear pump pressure to 0.45Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 60 ℃, keep fluidized bed drying temperature 50 C, when the moisture drying to 15% of vitamin d3 beadlet, fluidized-bed temperature can be adjusted into 70 ℃ continues dry, when the moisture of vitamin d3 beadlet reaches 5%, vitamin d3 beadlet is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
Claims (4)
1. a vitamin d3 beadlet, it is characterized in that: it is by oleovitamin D3,2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in oleovitamin D3, pure vitamin D3 accounts for 1.2-1.5%, 2, and 6-di-t-butyl-4-cresols accounts for 1-2%, starch sodium octenyl succinate and accounts for that 5-60%, maltodextrin account for 30-80%, pure water accounts for 5-8%.
2. a kind of vitamin d3 beadlet according to claim 1, is characterized in that: described 2,6-di-t-butyl-4-cresols by ethoxyquin, replaced and shared percentage by weight constant.
3. a kind of vitamin d3 beadlet according to claim 1 and 2, is characterized in that: described maltodextrin by white sugar, replaced and shared percentage by weight constant.
4. the production method of a vitamin d3 beadlet, it is characterized in that: first according to formula rate, each composition is weighed, then oleovitamin D3 is dropped in molten oily still, start to stir, and be heated to 50-70 ℃, melt to oleovitamin D3, after its clarification, make the temperature of molten oily still remain in the situation of 66-70 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols or ethoxyquin, stir 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is the 80-160% of solid content, be heated to 50-70 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into maltodextrin or the white sugar of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin or white sugar finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 10-30 minute, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 66-70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 400-500m.p.s, open fluidized system and starch systems, first starch systems is blown 5-10 minute starch to spray tower to fluid bed, the temperature of starch is controlled at 50-80 ℃, moisture 10%-13%, fluid bed EAT is controlled at 40-80 ℃, now open sprayer, adjust rotating speed to 40-50HZ, adjust gear pump pressure to 0.4-0.5Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 40-80 ℃, keep fluidized bed drying temperature 40-60 ℃, when the moisture drying to 15% of vitamin d3 beadlet, fluidized-bed temperature can be adjusted into 60-80 ℃ continues dry, when the moisture of vitamin d3 beadlet reaches 5% ± 1%, vitamin d3 beadlet is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
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| CN201410391636.3A CN104186977A (en) | 2014-08-11 | 2014-08-11 | Vitamin D3 beadlet and production method thereof |
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| CN201410391636.3A CN104186977A (en) | 2014-08-11 | 2014-08-11 | Vitamin D3 beadlet and production method thereof |
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| CN101888788A (en) * | 2007-12-05 | 2010-11-17 | 帝斯曼知识产权资产管理有限公司 | Pulverous formulation of a fat-soluble active ingredient |
| CN102652732A (en) * | 2012-03-23 | 2012-09-05 | 食味添（上海）科技贸易有限公司 | Nano water-soluble emulsion and preparation method thereof |
| CN102716087A (en) * | 2012-05-31 | 2012-10-10 | 浙江中同科技有限公司 | Vitamin powder and preparation method thereof |
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2014
- 2014-08-11 CN CN201410391636.3A patent/CN104186977A/en active Pending
Patent Citations (5)
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| CN101873848A (en) * | 2007-07-19 | 2010-10-27 | 帝斯曼知识产权资产管理有限公司 | Tablettable formulations of lipophilic health ingredients |
| CN101888788A (en) * | 2007-12-05 | 2010-11-17 | 帝斯曼知识产权资产管理有限公司 | Pulverous formulation of a fat-soluble active ingredient |
| CN101564384A (en) * | 2008-07-14 | 2009-10-28 | 烟台绿叶动物保健品有限公司 | Multivitamin aqueous solution preparation |
| CN102652732A (en) * | 2012-03-23 | 2012-09-05 | 食味添（上海）科技贸易有限公司 | Nano water-soluble emulsion and preparation method thereof |
| CN102716087A (en) * | 2012-05-31 | 2012-10-10 | 浙江中同科技有限公司 | Vitamin powder and preparation method thereof |
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Application publication date: 20141210 |