CN104186976A - Vitamin A acetate beadlet and production method thereof - Google Patents
Vitamin A acetate beadlet and production method thereof Download PDFInfo
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- CN104186976A CN104186976A CN201410391635.9A CN201410391635A CN104186976A CN 104186976 A CN104186976 A CN 104186976A CN 201410391635 A CN201410391635 A CN 201410391635A CN 104186976 A CN104186976 A CN 104186976A
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- retinyl acetate
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Abstract
The invention relates to the field of vitamin production and particularly relates to a vitamin A acetate beadlet with long quality guarantee period and capability of dispersing in cold water. The vitamin A acetate beadlet consists of vitamin A acetate, 2, 6-di-tert-butyl-4-cresol, starch sodium octenylsuccinate, maltodextrin and pure water. A production method of the vitamin A acetate beadlet comprises the following steps: (1) firstly weighing, then melting the vitamin A acetate, and adding ethoxyquin for later use; adding pure water into an emulsifying pot, stirring, simultaneously adding the starch sodium octenylsuccinate and white sugar and waiting for emulsification; adding a mixture in an oil melting kettle into the emulsifying pot, starting a fluidized-bed system and a starch system, and after treatment, extracting the vitamin A acetate beadlet. The quality guarantee period of the vitamin A acetate beadlet can reach 24 months, and simultaneously the vitamin A acetate beadlet can be dispersed in cold water, so that the use limitation can be reduced; compared with an existing standard formula, the formula and the production method have the advantages that the production cost can be greatly reduced and the production benefit of an enterprise can be increased.
Description
Technical field
The present invention relates to vitamin production field, especially a kind of retinyl acetate particulate and production method thereof.
Background technology
Retinyl acetate particulate is the conventional product of feed addictive, and its whole use amount is larger.And there is following shortcoming in the retinyl acetate particulate that existing standard recipe is produced:
1. shelf life of products only has 12 months, from production, completing the multistage dealer's of process running again enters retailer and user's hand again, elder may need to consume six months, therefore consumer only has limit the spendable time, and for enterprise, different period use amounts are indefinite, can cause a large amount of retinyl acetates to cause waste because of expired.
2. product can not disperse in cold water, and this defect causes in use required water environment need to be heated to uniform temperature, just can make it in water, disperse, and has caused unnecessary operation, causes the waste of the energy simultaneously.
3. in standard recipe, use gelatin as raw material, can have the risk that produces heavy metal pollution, the destruction that can cause ecological environment.
Summary of the invention
The object of the invention is the retinyl acetate particulate and the production method thereof that in order to solve the deficiency of above-mentioned technology, a kind of long shelf-life are provided, can in cold water, disperse.
In order to achieve the above object, the retinyl acetate particulate that the present invention is designed, it is by retinyl acetate, 2, 6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in retinyl acetate, pure vitamin A acetic acid esters accounts for the 10-20% of each composition gross mass, 2, 6-di-t-butyl-4-cresols accounts for the 1-2% of each composition gross mass, starch sodium octenyl succinate accounts for the 10-60% of each composition gross mass, maltodextrin accounts for the 20-70% of each composition gross mass, pure water accounts for the 5-8% of each composition gross mass.
Wherein: described 2,6-di-t-butyl-4-cresols by ethoxyquin, replaced and shared percentage by weight constant.
Wherein: described maltodextrin by white sugar, replaced and shared percentage by weight constant.
The production method of retinyl acetate particulate, first according to formula rate, each composition is weighed, then retinyl acetate is dropped in molten oily still, start to stir, and be heated to 50-70 ℃, melt to retinyl acetate, after its clarification, make the temperature of molten oily still remain in the situation of 66-70 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols or ethoxyquin, stir 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is the 80-160% of total solid, be heated to 50-70 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into maltodextrin or the white sugar of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin or white sugar finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 10-30 minute, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 66-70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 400-500m.p.s, open fluidized system and starch systems, first starch systems is blown 5-10 minute starch to spray tower to fluid bed, the temperature of starch is controlled at 50-80 ℃, moisture 10%-13%, fluid bed EAT is controlled at 40-80 ℃, now open sprayer, adjust rotating speed to 40-50HZ, adjust gear pump pressure to 0.4-0.5Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 40-80 ℃, keep fluidized bed drying temperature 40-60 ℃, when the moisture drying to 15% of retinyl acetate particulate, fluidized-bed temperature can be adjusted into 60-80 ℃ continues dry, when the moisture of retinyl acetate particulate reaches 5% ± 1%, retinyl acetate particulate is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
The resulting retinyl acetate particulate of the present invention and production method thereof, the shelf-life of producing the retinyl acetate particulate obtaining by this formula can reach 24 months, improves its service time, and it can disperse in cold water simultaneously, thereby can reduce, it is used to restriction, increase the scope of application; And this formula and production method are relative and existing standard formula, can reduce production costs greatly, improve the productivity effect of enterprise.
The specific embodiment
The present invention is further described by the following embodiment.
Embodiment 1:
The retinyl acetate particulate that the present embodiment is described, it is by retinyl acetate, 2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in retinyl acetate, pure vitamin A acetic acid esters accounts for 10%, 2 of each composition gross mass, 6-di-t-butyl-4-cresols account for each composition gross mass 1%, starch sodium octenyl succinate account for each composition gross mass 45%, maltodextrin account for each composition gross mass 39%, pure water accounts for 5% of each composition gross mass.
Embodiment 2:
The retinyl acetate particulate that the present embodiment is described, it is by retinyl acetate, 2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in retinyl acetate, pure vitamin A acetic acid esters accounts for 20%, 2 of each composition gross mass, 6-di-t-butyl-4-cresols account for each composition gross mass 2%, starch sodium octenyl succinate account for each composition gross mass 30%, maltodextrin account for each composition gross mass 40%, pure water accounts for 8% of each composition gross mass.
Embodiment 3:
The retinyl acetate particulate that the present embodiment is described, it is comprised of retinyl acetate, ethoxyquin, starch sodium octenyl succinate, maltodextrin and pure water, and wherein the percentage of the shared gross mass of each composition is: in retinyl acetate pure vitamin A acetic acid esters account for each composition gross mass 15%, ethoxyquin account for each composition gross mass 2%, starch sodium octenyl succinate account for each composition gross mass 26%, maltodextrin account for each composition gross mass 50%, pure water accounts for 7% of each composition gross mass.
Embodiment 4:
The retinyl acetate particulate that the present embodiment is described, it is by retinyl acetate, 2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, white sugar and pure water form, wherein the percentage of the shared gross mass of each composition is: in retinyl acetate, pure vitamin A acetic acid esters accounts for 12%, 2 of each composition gross mass, 6-di-t-butyl-4-cresols account for each composition gross mass 1%, starch sodium octenyl succinate account for each composition gross mass 56%, white sugar account for each composition gross mass 25%, pure water accounts for 6% of each composition gross mass.
Embodiment 5:
The production method of the retinyl acetate particulate that the present embodiment is described, first according to formula rate, each composition is weighed, then retinyl acetate is dropped in molten oily still, start to stir, and be heated to 50 ℃, melt to retinyl acetate, after its clarification, make the temperature of molten oily still remain in the situation of 66 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols, stirs 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is 80% of total solid, be heated to 50 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into the maltodextrin of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 10 minutes, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 66-70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 400m.p.s, open fluidized system and starch systems, first starch systems is blown 5 minutes starch to spray tower to fluid bed, the temperature of starch is controlled at 50 ℃, moisture 10%, fluid bed EAT is controlled at 40 ℃, now open sprayer, adjust rotating speed to 40HZ, adjust gear pump pressure to 0.4Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 40 ℃, keep 40 ℃ of fluidized bed drying temperature, when the moisture drying to 15% of retinyl acetate particulate, fluidized-bed temperature can be adjusted into 60 ℃ continues dry, when the moisture of retinyl acetate particulate reaches 4%, retinyl acetate particulate is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
Embodiment 6:
The production method of the retinyl acetate particulate that the present embodiment is described, first according to formula rate, each composition is weighed, then retinyl acetate is dropped in molten oily still, start to stir, and be heated to 70 ℃, melt to retinyl acetate, after its clarification, make the temperature of molten oily still remain in the situation of 70 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols, stirs 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is 160% of total solid, be heated to 70 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into the white sugar of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing white sugar finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 30 minutes, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 500m.p.s, open fluidized system and starch systems, first starch systems is blown 10 minutes starch to spray tower to fluid bed, the temperature of starch is controlled at 80 ℃, moisture 13%, fluid bed EAT is controlled at 80 ℃, now open sprayer, adjust rotating speed to 50HZ, adjust gear pump pressure to 0.5Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 80 ℃, keep fluidized bed drying temperature 60 C, when the moisture drying to 15% of retinyl acetate particulate, fluidized-bed temperature can be adjusted into 80 ℃ continues dry, when the moisture of retinyl acetate particulate reaches 6%, retinyl acetate particulate is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
Embodiment 7:
The production method of the retinyl acetate particulate that the present embodiment is described, first according to formula rate, each composition is weighed, then retinyl acetate is dropped in molten oily still, start to stir, and be heated to 60 ℃, and melt to retinyl acetate, after its clarification, make the temperature of molten oily still remain on the ethoxyquin that drops into formula ratio in the situation of 68 ℃, stir 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is 120% of total solid, be heated to 60 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into the maltodextrin of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 20 minutes, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 68 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 450m.p.s, open fluidized system and starch systems, first starch systems is blown 7 minutes starch to spray tower to fluid bed, the temperature of starch is controlled at 60 ℃, moisture 12%, fluid bed EAT is controlled at 60 ℃, now open sprayer, adjust rotating speed to 45HZ, adjust gear pump pressure to 0.45Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 60 ℃, keep fluidized bed drying temperature 50 C, when the moisture drying to 15% of retinyl acetate particulate, fluidized-bed temperature can be adjusted into 70 ℃ continues dry, when the moisture of retinyl acetate particulate reaches 5%, retinyl acetate particulate is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
Claims (4)
1. a retinyl acetate particulate, it is characterized in that: it is by retinyl acetate, 2,6-di-t-butyl-4-cresols, starch sodium octenyl succinate, maltodextrin and pure water form, wherein the percentage of the shared gross mass of each composition is: in retinyl acetate, pure vitamin A acetic acid esters accounts for the 10-20%, 2 of each composition gross mass, and 20-70%, the pure water that 10-60%, the maltodextrin that 1-2%, the starch sodium octenyl succinate that 6-di-t-butyl-4-cresols accounts for each composition gross mass accounts for each composition gross mass accounts for each composition gross mass accounts for the 5-8% of each composition gross mass.
2. a kind of retinyl acetate particulate according to claim 1, is characterized in that: described 2,6-di-t-butyl-4-cresols by ethoxyquin, replaced and shared percentage by weight constant.
3. a kind of retinyl acetate particulate according to claim 1 and 2, is characterized in that: described maltodextrin by white sugar, replaced and shared percentage by weight constant.
4. the production method of a retinyl acetate particulate, it is characterized in that: first according to formula rate, each composition is weighed, then retinyl acetate is dropped in molten oily still, start to stir, and be heated to 50-70 ℃, melt to retinyl acetate, after its clarification, make the temperature of molten oily still remain in the situation of 66-70 ℃ and drop into 2 of formula ratio, 6-di-t-butyl-4-cresols or ethoxyquin, stir 5 minutes, standby, in emulsification pot, add pure water, the amount of pure water is the 80-160% of total solid, be heated to 50-70 ℃, the starch sodium octenyl succinate that drops into formula ratio when stirring, and finished in 30 minutes, finish starch sodium octenyl succinate, continue to be stirred to it and melt completely, drop into maltodextrin or the white sugar of formula ratio while making the temperature of emulsification pot remain on 70 ℃, the speed of throwing maltodextrin or white sugar finished in 20 minutes, stir and be cooled to 68 ℃ after 30 minutes, treat emulsification, mixture in molten oily still is added in emulsification pot, add speed to add in 10-30 minute, in adition process, continue to stir, and after having added, stir again 30 minutes, when the temperature of emulsification pot is down to 66-70 ℃, test emulsion viscosity, and by pure water adjusting viscosity until reach 400-500m.p.s, open fluidized system and starch systems, first starch systems is blown 5-10 minute starch to spray tower to fluid bed, the temperature of starch is controlled at 50-80 ℃, moisture 10%-13%, fluid bed EAT is controlled at 40-80 ℃, now open sprayer, adjust rotating speed to 40-50HZ, adjust gear pump pressure to 0.4-0.5Mpa, open spray valve, open steam hammer, carry out mist projection granulating, now control the temperature of fluid bed at 40-80 ℃, keep fluidized bed drying temperature 40-60 ℃, when the moisture drying to 15% of retinyl acetate particulate, fluidized-bed temperature can be adjusted into 60-80 ℃ continues dry, when the moisture of retinyl acetate particulate reaches 5% ± 1%, retinyl acetate particulate is extracted out and prepared to detect, detect after qualified and carry out weighing and bagging, warehouse-in.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410391635.9A CN104186976A (en) | 2014-08-11 | 2014-08-11 | Vitamin A acetate beadlet and production method thereof |
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| CN201410391635.9A CN104186976A (en) | 2014-08-11 | 2014-08-11 | Vitamin A acetate beadlet and production method thereof |
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Cited By (4)
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| CN106580919A (en) * | 2016-12-29 | 2017-04-26 | 无限极（中国）有限公司 | Ganoderma spore oil microcapsule powder and preparing method and application thereof |
| CN111867566A (en) * | 2018-03-15 | 2020-10-30 | 帝斯曼知识产权资产管理有限公司 | Vitamin A-containing extrudate |
| CN114748445A (en) * | 2022-05-12 | 2022-07-15 | 浙江花园营养科技有限公司 | High-content vitamin A acetate particle and preparation method thereof |
| CN114796152A (en) * | 2022-05-12 | 2022-07-29 | 浙江花园生物高科股份有限公司 | Vitamin A acetate particle and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580919A (en) * | 2016-12-29 | 2017-04-26 | 无限极（中国）有限公司 | Ganoderma spore oil microcapsule powder and preparing method and application thereof |
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| CN111867566A (en) * | 2018-03-15 | 2020-10-30 | 帝斯曼知识产权资产管理有限公司 | Vitamin A-containing extrudate |
| CN114748445A (en) * | 2022-05-12 | 2022-07-15 | 浙江花园营养科技有限公司 | High-content vitamin A acetate particle and preparation method thereof |
| CN114796152A (en) * | 2022-05-12 | 2022-07-29 | 浙江花园生物高科股份有限公司 | Vitamin A acetate particle and preparation method thereof |
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| CN114796152B (en) * | 2022-05-12 | 2023-12-12 | 浙江花园生物医药股份有限公司 | Vitamin A acetate particle and preparation method thereof |
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Application publication date: 20141210 |