CN104178528A - Method for making alcohol from straws - Google Patents

Method for making alcohol from straws Download PDF

Info

Publication number
CN104178528A
CN104178528A CN201410474621.3A CN201410474621A CN104178528A CN 104178528 A CN104178528 A CN 104178528A CN 201410474621 A CN201410474621 A CN 201410474621A CN 104178528 A CN104178528 A CN 104178528A
Authority
CN
China
Prior art keywords
compound
alcohol
make
stalk
maize straw
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410474621.3A
Other languages
Chinese (zh)
Inventor
王玉南
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Environmental Protection Technology Co Ltd Newly Pulls Together In Suzhou
Original Assignee
Environmental Protection Technology Co Ltd Newly Pulls Together In Suzhou
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Environmental Protection Technology Co Ltd Newly Pulls Together In Suzhou filed Critical Environmental Protection Technology Co Ltd Newly Pulls Together In Suzhou
Priority to CN201410474621.3A priority Critical patent/CN104178528A/en
Publication of CN104178528A publication Critical patent/CN104178528A/en
Pending legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel

Landscapes

  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

The invention discloses a method for making alcohol from straws, which comprises the following steps: 1. selecting high-quality corn straws, and cleaning; 2. adding corn cob, rice hull, cottonseed hull and sunflower residue as a composite base material; 3. pulverizing the mixture to 145 meshes; 4. hydrolyzing the mixture with distilled water; 5. boiling the hydrolyzed mixture in an iron pan; 6. cooling; 7. diastatic fermentation: fermenting the cooled mixture in a ceramic cylinder with the diameter of 1.5m; and 8. distilling and extracting. The invention provides a novel method for producing alcohol from corn straws, and has the advantages of short development process, high efficiency and low energy consumption, thereby lowering the alcohol production cost and widening the straw application range.

Description

Utilize stalk to make the method for alcohol
Technical field
The present invention relates to stalk application, particularly relate to a kind of method of utilizing stalk to make alcohol.
Background technology
Alcohol is a kind of important industrial raw material, be widely used in food, chemical industry, medicine and other fields, it is replacing gasoline partly or entirely, there is the advantages such as safety, clean, regeneration, alcohol mainly be take molasses, potato class, cereal as fermenting raw materials production, mainly take corn as raw material, due to population growth and Alcohol Production Cost Problems in China northeast, the corn of take is hard to carry on as raw material production alcohol, and utilizes abundant, cheap maize straw to become inexorable trend for raw material production alcohol.
I am after at present still lower aspect straw utilization rate, general maize straw is except small part is utilized, most of with direct impouring environment of form such as accumulation, waste burnings, causes very big pollution and waste, and the method thermo-efficiency of this direct burning is very low, very large waste stalk resource.Maize straw is mainly Mierocrystalline cellulose, hemicellulose and wooden element, after pre-treatment and hydrolysis, can decompose saccharogenesis, is the favourable resource of making alcohol.
Summary of the invention
The technical problem that the present invention mainly solves is to provide a kind of method of utilizing stalk to make alcohol, thereby have the producing alcohol by using maize straws novel method that the flow process developed is short, efficiency is high, energy consumption is low, reduces Alcohol Production cost, has expanded stalk use range.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is: a kind of method of utilizing stalk to make alcohol is provided, comprises the following steps:
Step 1: choose the maize straw of high-quality, then clear up the impurity such as silt, stone of maize straw the inside; Step 2: add corn cob, rice hulls, cotton seed hulls, Sunflower Receptacle slag as composite base-material;
Step 3: first maize straw is put into iron hammer pulverizer and pulverized, reach 150mu, then the corn cob in composite base-material, rice hulls, cotton seed hulls, Sunflower Receptacle slag are added successively in pulverizer and carry out co-grinding, reach the compound of 145mu;
Step 4: hydrolysis, with distilled water, compound is soaked and is hydrolyzed for 6~7.5 hours;
Step 5: iron pan boiling, the compound after hydrolysis is put into iron pan and carry out boiling, in pot, put into calcium oxide and soften;
Step 6: cold lack, by compound pull out put on cooling table, carry out cooling fast;
Step 7: diastatic fermentation, it is the ceramic cylinder of 1.5 meters that the compound after cold lack is put into diameter, keeps one deck compound to add distiller's yeast one time during placement, until ceramic cylinder is filled out at 4/5ths o'clock, and cylinder body seal is tight, ferment 5~6 days;
Step 8: distillation extraction, take out after waiting the fermentation of compound in ceramic cylinder, put into distiller and distill, 65%~85% the alcohol that can make.
In preferred embodiments of the present invention, in described step 3, compound is set to by weight percentage: corn cob 10%~15%, rice hulls 5%~10%, cotton seed hulls 2.5%~5.5%, Sunflower Receptacle slag 15%~20%, maize straw 65%~75%.
In preferred embodiments of the present invention, the calcium chloride of putting in pot in described step 5 accounts for 5% of compound.
In preferred embodiments of the present invention, described step 6 adopts air-cooledly carries out coolingly, and the described air-cooled time is in 30min clock.
In preferred embodiments of the present invention, in described step 7, the bed thickness of compound is 15cm.
The invention has the beneficial effects as follows: a kind of method of utilizing stalk to make alcohol, reduces Alcohol Production cost, has expanded stalk use range thereby have the producing alcohol by using maize straws novel method that the flow process developed is short, efficiency is high, energy consumption is low.
Embodiment
Below the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only a part of embodiment of the present invention, rather than whole embodiment.Embodiment based in the present invention, those of ordinary skills, not making all other embodiment that obtain under creative work prerequisite, belong to the scope of protection of the invention.
The embodiment of the present invention comprises:
Utilize stalk to make a method for alcohol, comprise the following steps:
Step 1: choose the maize straw of high-quality, then clear up the impurity such as silt, stone of maize straw the inside; Step 2: add corn cob, rice hulls, cotton seed hulls, Sunflower Receptacle slag as composite base-material;
Step 3: first maize straw is put into iron hammer pulverizer and pulverized, reach 150mu, then the corn cob in composite base-material, rice hulls, cotton seed hulls, Sunflower Receptacle slag are added successively in pulverizer and carry out co-grinding, reach the compound of 145mu;
Step 4: hydrolysis, with distilled water, compound is soaked and is hydrolyzed for 6~7.5 hours;
Step 5: iron pan boiling, the compound after hydrolysis is put into iron pan and carry out boiling, in pot, put into calcium oxide and soften;
Step 6: cold lack, by compound pull out put on cooling table, carry out cooling fast;
Step 7: diastatic fermentation, it is the ceramic cylinder of 1.5 meters that the compound after cold lack is put into diameter, keeps one deck compound to add distiller's yeast one time during placement, until ceramic cylinder is filled out at 4/5ths o'clock, and cylinder body seal is tight, ferment 5~6 days;
Step 8: distillation extraction, take out after waiting the fermentation of compound in ceramic cylinder, put into distiller and distill, 65%~85% the alcohol that can make.
Further, in described step 3, compound is set to by weight percentage: corn cob 10%~15%, rice hulls 5%~10%, cotton seed hulls 2.5%~5.5%, Sunflower Receptacle slag 15%~20%, maize straw 65%~75%.
Further, the calcium chloride of putting in pot in described step 5 accounts for 5% of compound.
Further, described step 6 adopts air-cooledly carries out coolingly, and the described air-cooled time is in 30min clock.
Further, in described step 7, the bed thickness of compound is 15cm.
The invention has the beneficial effects as follows: a kind of method of utilizing stalk to make alcohol, reduces Alcohol Production cost, has expanded stalk use range thereby have the producing alcohol by using maize straws novel method that the flow process developed is short, efficiency is high, energy consumption is low.
The foregoing is only embodiments of the invention; not thereby limit the scope of the claims of the present invention; every equivalent structure or conversion of equivalent flow process that utilizes description of the present invention to do; or be directly or indirectly used in other relevant technical field, be all in like manner included in scope of patent protection of the present invention.

Claims (5)

1. utilize stalk to make a method for alcohol, it is characterized in that, comprise the following steps:
Step 1: choose the maize straw of high-quality, then clear up the impurity such as silt, stone of maize straw the inside; Step 2: add corn cob, rice hulls, cotton seed hulls, Sunflower Receptacle slag as composite base-material;
Step 3: first maize straw is put into iron hammer pulverizer and pulverized, reach 150mu, then the corn cob in composite base-material, rice hulls, cotton seed hulls, Sunflower Receptacle slag are added successively in pulverizer and carry out co-grinding, reach the compound of 145mu;
Step 4: hydrolysis, with distilled water, compound is soaked and is hydrolyzed for 6~7.5 hours;
Step 5: iron pan boiling, the compound after hydrolysis is put into iron pan and carry out boiling, in pot, put into calcium oxide and soften;
Step 6: cold lack, by compound pull out put on cooling table, carry out cooling fast;
Step 7: diastatic fermentation, it is the ceramic cylinder of 1.5 meters that the compound after cold lack is put into diameter, keeps one deck compound to add distiller's yeast one time during placement, until ceramic cylinder is filled out at 4/5ths o'clock, and cylinder body seal is tight, ferment 5~6 days;
Step 8: distillation extraction, take out after waiting the fermentation of compound in ceramic cylinder, put into distiller and distill, 65%~85% the alcohol that can make.
2. the method for utilizing stalk to make alcohol according to claim 1, it is characterized in that, in described step 3, compound is set to by weight percentage: corn cob 10%~15%, rice hulls 5%~10%, cotton seed hulls 2.5%~5.5%, Sunflower Receptacle slag 15%~20%, maize straw 65%~75%.
3. the method for utilizing stalk to make alcohol according to claim 1, is characterized in that, the calcium chloride of putting in pot in described step 5 accounts for 5% of compound.
4. the method for utilizing stalk to make alcohol according to claim 1, is characterized in that, described step 6 adopts air-cooledly carries out coolingly, and the described air-cooled time is in 30min clock.
5. utilize according to claim 1 stalk to make the method for alcohol, it is characterized in that, in described step 7, the bed thickness of compound is 15cm.
CN201410474621.3A 2014-09-18 2014-09-18 Method for making alcohol from straws Pending CN104178528A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410474621.3A CN104178528A (en) 2014-09-18 2014-09-18 Method for making alcohol from straws

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410474621.3A CN104178528A (en) 2014-09-18 2014-09-18 Method for making alcohol from straws

Publications (1)

Publication Number Publication Date
CN104178528A true CN104178528A (en) 2014-12-03

Family

ID=51959873

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410474621.3A Pending CN104178528A (en) 2014-09-18 2014-09-18 Method for making alcohol from straws

Country Status (1)

Country Link
CN (1) CN104178528A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105950672A (en) * 2016-06-20 2016-09-21 宁夏紫荆花纸业有限公司 Method for making alcohol by using crop straws

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101225409A (en) * 2007-01-19 2008-07-23 丁长青 Fuel ethanol produced by straw
CN101358218A (en) * 2008-09-22 2009-02-04 王建设 Method for producing xylose coupled cogeneration of propanone, butanol and ethanol using stalk
CN101492700A (en) * 2009-03-05 2009-07-29 王建设 Intensive processing method for stalk articles or agricultural castoff

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101225409A (en) * 2007-01-19 2008-07-23 丁长青 Fuel ethanol produced by straw
CN101358218A (en) * 2008-09-22 2009-02-04 王建设 Method for producing xylose coupled cogeneration of propanone, butanol and ethanol using stalk
CN101492700A (en) * 2009-03-05 2009-07-29 王建设 Intensive processing method for stalk articles or agricultural castoff

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
孙君社等: "秸秆生产乙醇预处理关键技术", 《化学进展》, vol. 19, no. 78, 31 August 2007 (2007-08-31), pages 1122 - 1128 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105950672A (en) * 2016-06-20 2016-09-21 宁夏紫荆花纸业有限公司 Method for making alcohol by using crop straws

Similar Documents

Publication Publication Date Title
Sindhu et al. Water hyacinth a potential source for value addition: an overview
Li et al. An overview of algae bioethanol production
CN101358218B (en) Method for producing xylose coupled cogeneration of propanone, butanol and ethanol using stalk
CN103993042B (en) A kind of lignocellulose material co-producing bio ethanol and the method for pulullan
CN104140907B (en) A kind of tea wine preparation technology
CN103740769A (en) Technology using straw for combined production of ethanol and biogas
CN102703518A (en) Method for producing alcohol and cultivating edible fungus by solid fermentation through mixing manioc waste with treacle
CN101691537A (en) Integrated processing method for byproducts in lignocellulose-refining fuel ethanol
CN101096690B (en) Method for preparing ethanol with turmeric
CN104178528A (en) Method for making alcohol from straws
CN103173500A (en) Method for manufacturing ethanol by using persimmon
CN103947889B (en) Fly-maggot feed and preparation method thereof
CN101024848A (en) Method for producing alcohol using sweet kaoliang straw
CN102220381A (en) Technology for producing edible alcohol by using crushed vermicelli and bean dregs
CN1706928A (en) Sugar cane wine and its production process
CN102465074A (en) Sugarcane wine and production method thereof
CN101298619A (en) Method for preparing ethanol from beet
CN108531516B (en) Comprehensive utilization method of water lettuce
KR101011244B1 (en) Method for preparing bioethanol from watermelon seeds
CN101781587B (en) Method for preparing biodiesel by using animal fat and fresh sweet potato
CN203999586U (en) Novel cassava alcohol production device
CN104313058A (en) Marsh gas power generation method using biomass energy sources
CN102031207B (en) Method for producing soap base by utilizing waste water containing grease
CN102965202B (en) Preparation method of biodiesel by using heterogeneous catalyst
CN102242158A (en) Method for producing ethanol with lotus peel powder as raw material by synchronization of saccharification and fermentation

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20141203