CN104152054B - A kind of preparation method of soft glass polishing fluid of zirconium matrix - Google Patents
A kind of preparation method of soft glass polishing fluid of zirconium matrix Download PDFInfo
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- CN104152054B CN104152054B CN201410175265.5A CN201410175265A CN104152054B CN 104152054 B CN104152054 B CN 104152054B CN 201410175265 A CN201410175265 A CN 201410175265A CN 104152054 B CN104152054 B CN 104152054B
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Abstract
The invention discloses a kind of preparation method of soft glass polishing fluid of zirconium matrix, it is characterized in that, described preparation method comprises the following steps: (1) calcining, the test of (2) specific surface, (3) grinding, (4) screening, the test of (5) solid content, (6) batching.The invention has the beneficial effects as follows: the present invention has good cutting output, have good smooth finish to glazed surface, security is high, mixes iron powder and meets the requirement of user to paste color.
Description
Technical field
The present invention is specifically related to a kind of preparation method of soft glass polishing fluid of zirconium matrix.
Background technology
At present, a kind of preparation method of soft glass polishing fluid of zirconium matrix easily makes polishing soft glass produce scuffing, and cutting output is inadequate, and existing preparation method easily produces precipitation.
Summary of the invention
Object of the present invention: the preparation method that the invention provides a kind of soft glass polishing fluid of zirconium matrix, the present invention has good cutting output, and have good smooth finish to glazed surface, security is high, mixes iron powder and meets the requirement of client to paste color.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme: a kind of preparation method of soft glass polishing fluid of zirconium matrix, is characterized in that, described preparation method comprises the following steps:
(1) calcine: 800-900 DEG C, zirconium carbonate raw material process of passing through tunnel kiln is sintered into zirconium white;
(2) specific surface test: get the zirconium white calcined, by full-automatic specific surface instrument test specific surface, the Eligibility requirements of specific surface is 1-10m
2/ g;
(3) grind: the zirconium white 20KG getting suitable specific surface adds 20KG zirconium carbonate raw material, mixes 0.03% iron powder, adds 50kg deionized water, ball milling 5-7h, test granularity Eligibility requirements 1.5-1.7 μm;
(4) screen: by 150 mesh screen macrobeads, sampling and testing granularity at the end of blowing, qualified for subsequent use, defectively to do over again;
(5) solid content test: get above-mentioned 5 slurry agitation even, get 3 sample test solid contents;
(6) prepare burden: the add-on calculating size mixing total amount and each auxiliary material of product according to solid content, then carry out PH adjustment, add 0.05% ammoniacal liquor, reach PH=6-7, dispersed with stirring 1 hour, finally add 0.02%dispal and stir 1 hour.
The invention has the beneficial effects as follows: the present invention has good cutting output, have good smooth finish to glazed surface, security is high, mixes iron powder and meets the requirement of user to paste color.
Embodiment
The invention will be further described below.
A preparation method for the soft glass polishing fluid of zirconium matrix, is characterized in that, described preparation method comprises the following steps:
(1) calcine: 800-900 DEG C, zirconium carbonate raw material process of passing through tunnel kiln is sintered into zirconium white;
(2) specific surface test: get the zirconium white calcined, by full-automatic specific surface instrument test specific surface, the Eligibility requirements of specific surface is 1-10m
2/ g;
(3) grind: the zirconium white 20KG getting suitable specific surface adds 20KG zirconium carbonate raw material, mixes 0.03% iron powder, adds 50kg deionized water, ball milling 5-7h, test granularity Eligibility requirements 1.5-1.7 μm;
(4) screen: by 150 mesh screen macrobeads, sampling and testing granularity at the end of blowing, qualified for subsequent use, defectively to do over again;
(5) solid content test: get above-mentioned 5 slurry agitation even, get 3 sample test solid contents;
(6) prepare burden: the add-on calculating size mixing total amount and each auxiliary material of product according to solid content, then carry out PH adjustment, add 0.05% ammoniacal liquor, reach PH=6-7, dispersed with stirring 1 hour, finally add 0.02%dispal and stir 1 hour.
Be more than the description of this invention and non-limiting, based on other embodiments of inventive concept, also all among protection scope of the present invention.
Claims (1)
1. a preparation method for the soft glass polishing fluid of zirconium matrix, is characterized in that, described preparation method comprises the following steps:
(1) calcine: 800-900 DEG C, zirconium carbonate raw material process of passing through tunnel kiln is sintered into zirconium white;
(2) specific surface test: get the zirconium white calcined, by full-automatic specific surface instrument test specific surface, the Eligibility requirements of specific surface is 1-10 ㎡/g;
(3) grind: the zirconium white 20kg getting suitable specific surface adds 20kg zirconium carbonate raw material, mixes 0.03% iron powder, adds 50kg deionized water, ball milling 5-7h, test granularity and choose 1.5-1.7 μm qualified for requiring;
(5) screen: by 150 mesh screen macrobeads, sampling and testing granularity at the end of blowing, qualified for subsequent use, defectively to do over again;
(6) solid content test: get above-mentioned slurry agitation even, get 3 sample test solid contents;
(7) prepare burden: the add-on calculating size mixing total amount and each auxiliary material of product according to solid content, then carry out pH regulator, add 0.05% ammoniacal liquor, reach pH=6-7, dispersed with stirring 1 hour, finally add 0.02%dispal and stir 1 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410175265.5A CN104152054B (en) | 2014-04-29 | 2014-04-29 | A kind of preparation method of soft glass polishing fluid of zirconium matrix |
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| CN201410175265.5A CN104152054B (en) | 2014-04-29 | 2014-04-29 | A kind of preparation method of soft glass polishing fluid of zirconium matrix |
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| CN104152054A CN104152054A (en) | 2014-11-19 |
| CN104152054B true CN104152054B (en) | 2016-03-23 |
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| CN201410175265.5A Active CN104152054B (en) | 2014-04-29 | 2014-04-29 | A kind of preparation method of soft glass polishing fluid of zirconium matrix |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106010298A (en) * | 2016-06-29 | 2016-10-12 | 上海华明高纳稀土新材料有限公司 | Zirconium oxide polishing solution and preparation method thereof |
| CN110256969B (en) * | 2019-05-29 | 2020-11-10 | 湖南皓志科技股份有限公司 | Blue glass fine polishing solution and preparation method thereof |
Citations (6)
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|---|---|---|---|---|
| JP2007514856A (en) * | 2003-12-18 | 2007-06-07 | スリーエム イノベイティブ プロパティズ カンパニー | Alumina-yttria particles and method for producing the same |
| CN102250585A (en) * | 2011-08-19 | 2011-11-23 | 永州皓志稀土材料有限公司 | Preparation method of zirconia grinding fluid |
| CN102516880A (en) * | 2011-12-14 | 2012-06-27 | 德米特（苏州）电子环保材料有限公司 | Preparation method of cerium oxide matrix glass lens polishing powder |
| CN102516881A (en) * | 2011-12-14 | 2012-06-27 | 德米特（苏州）电子环保材料有限公司 | Manufacturing method of resin eyeglass polishing powder with alumina matrix |
| CN103402705A (en) * | 2011-01-27 | 2013-11-20 | 福吉米株式会社 | Polishing material and polishing composition |
| CN103450813A (en) * | 2013-01-10 | 2013-12-18 | 湖南皓志新材料股份有限公司 | Preparation method of iron-doped zirconium oxide polishing solution |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101543809B1 (en) * | 2007-03-29 | 2015-08-11 | 도호 티타늄 가부시키가이샤 | Method for production of alkali titanate method for production of hollow powder of alkali titanate alkali titanate and hollow powder thereof produced by the methods and friction material comprising the alkali titanate or the hollow powder thereof |
-
2014
- 2014-04-29 CN CN201410175265.5A patent/CN104152054B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007514856A (en) * | 2003-12-18 | 2007-06-07 | スリーエム イノベイティブ プロパティズ カンパニー | Alumina-yttria particles and method for producing the same |
| CN103402705A (en) * | 2011-01-27 | 2013-11-20 | 福吉米株式会社 | Polishing material and polishing composition |
| CN102250585A (en) * | 2011-08-19 | 2011-11-23 | 永州皓志稀土材料有限公司 | Preparation method of zirconia grinding fluid |
| CN102516880A (en) * | 2011-12-14 | 2012-06-27 | 德米特（苏州）电子环保材料有限公司 | Preparation method of cerium oxide matrix glass lens polishing powder |
| CN102516881A (en) * | 2011-12-14 | 2012-06-27 | 德米特（苏州）电子环保材料有限公司 | Manufacturing method of resin eyeglass polishing powder with alumina matrix |
| CN103450813A (en) * | 2013-01-10 | 2013-12-18 | 湖南皓志新材料股份有限公司 | Preparation method of iron-doped zirconium oxide polishing solution |
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| CN104152054A (en) | 2014-11-19 |
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