CN108070321A - A kind of preparation method of the soft glass polishing fluid of zirconium matrix - Google Patents
A kind of preparation method of the soft glass polishing fluid of zirconium matrix Download PDFInfo
- Publication number
- CN108070321A CN108070321A CN201610989319.0A CN201610989319A CN108070321A CN 108070321 A CN108070321 A CN 108070321A CN 201610989319 A CN201610989319 A CN 201610989319A CN 108070321 A CN108070321 A CN 108070321A
- Authority
- CN
- China
- Prior art keywords
- specific surface
- preparation
- zirconium
- soft glass
- polishing fluid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a kind of preparation methods of the soft glass polishing fluid of zirconium matrix, which is characterized in that the preparation method comprises the following steps：（1）Calcining,（2）Specific surface test,（3）Grinding,（4）Screening,（5）Solid content test,（6）Dispensing.The beneficial effects of the invention are as follows：The present invention has good cutting output, there is good finish to polished surface, safe, mixes iron powder and meets requirement of the user to paste color.
Description
Technical field
Present invention relates particularly to a kind of preparation methods of the soft glass polishing fluid of zirconium matrix.
Background technology
At present, a kind of preparation method of the soft glass polishing fluid of zirconium matrix easily makes polishing soft glass generate scuffing,
And cutting output is inadequate, and existing preparation method easily generates precipitation.
The content of the invention
The purpose of the present invention：The present invention provides a kind of preparation method of the soft glass polishing fluid of zirconium matrix, the present invention
With good cutting output, there is good finish to polished surface, it is safe, it mixes iron powder and meets client to paste color
Requirement.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that：A kind of soft glass of zirconium matrix is thrown
The preparation method of light liquid, which is characterized in that the preparation method comprises the following steps：
(1) calcine：Zirconium carbonate raw material process of passing through tunnel kiln is sintered into zirconium oxide for 800-900 DEG C；
(2) specific surface is tested：The zirconium oxide that calcining is taken to complete tests specific surface, the conjunction of specific surface by full-automatic specific surface instrument
Lattice requirement is 1-10m2/g；
(3) grind：The zirconium oxide 20KG of suitable specific surface is taken to add 20KG zirconium carbonate raw materials, mixes 0.03% iron powder, adds in 50kg
Deionized water, ball milling 5-7h, 1.5-1.7 μm of test granularity Eligibility requirements；
(4) screen：By 150 mesh screen bulky grains, sampling and testing granularity at the end of blowing is qualified spare, unqualified to do over again；
(5) solid content is tested：It takes above-mentioned 5 slurry agitation uniform, takes 3 sample test solid contents；
(6) dispensing：Size mixing total amount and the addition of each auxiliary material of product are calculated according to solid content, PH adjustings is then carried out, adds
Enter 0.05% ammonium hydroxide, reach PH=6-7, be dispersed with stirring 1 it is small when, be eventually adding 0.02%dispal stirring 1 it is small when.
The beneficial effects of the invention are as follows：The present invention has good cutting output, there is good finish to polished surface, pacifies
Quan Xinggao mixes iron powder and meets requirement of the user to paste color.
Specific embodiment
The invention will be further described below.
A kind of preparation method of the soft glass polishing fluid of zirconium matrix, which is characterized in that the preparation method include with
Lower step：
(1) calcine：Zirconium carbonate raw material process of passing through tunnel kiln is sintered into zirconium oxide for 800-900 DEG C；
(2) specific surface is tested：The zirconium oxide that calcining is taken to complete tests specific surface, the conjunction of specific surface by full-automatic specific surface instrument
Lattice requirement is 1-10m2/g；
(3) grind：The zirconium oxide 20KG of suitable specific surface is taken to add 20KG zirconium carbonate raw materials, mixes 0.03% iron powder, adds in 50kg
Deionized water, ball milling 5-7h, 1.5-1.7 μm of test granularity Eligibility requirements；
(4) screen：By 150 mesh screen bulky grains, sampling and testing granularity at the end of blowing is qualified spare, unqualified to do over again；
(5) solid content is tested：It takes above-mentioned 5 slurry agitation uniform, takes 3 sample test solid contents；
(6) dispensing：Size mixing total amount and the addition of each auxiliary material of product are calculated according to solid content, PH adjustings is then carried out, adds
Enter 0.05% ammonium hydroxide, reach PH=6-7, be dispersed with stirring 1 it is small when, be eventually adding 0.02%dispal stirring 1 it is small when.
It is non-limiting the above are the description of this invention, the other embodiment based on inventive concept, also in the present invention
Protection domain among.
Claims (1)
1. the preparation method of the soft glass polishing fluid of a kind of zirconium matrix, which is characterized in that the preparation method includes following
Step：(1) calcine：Zirconium carbonate raw material process of passing through tunnel kiln is sintered into zirconium oxide for 800-900 DEG C；(2) specific surface is tested：Take calcining
The zirconium oxide of completion tests specific surface by full-automatic specific surface instrument, and the Eligibility requirements of specific surface are 1-10m2/g；(3) grind：
The zirconium oxide 20KG of suitable specific surface is taken to add 20KG zirconium carbonate raw materials, mixes 0.03% iron powder, adds in 50kg deionized waters, ball milling
5-7h, 1.5-1.7 μm of test granularity Eligibility requirements；(4) screen：By 150 mesh screen bulky grains, sample and survey at the end of blowing
Granularity is tried, it is qualified spare, it is unqualified to do over again；(5) solid content is tested：It takes above-mentioned 5 slurry agitation uniform, 3 sample tests is taken to consolidate
Content；(6) dispensing：Size mixing total amount and the addition of each auxiliary material of product are calculated according to solid content, PH adjustings is then carried out, adds
Enter 0.05% ammonium hydroxide, reach PH=6-7, be dispersed with stirring 1 it is small when, be eventually adding 0.02%dispal stirring 1 it is small when.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610989319.0A CN108070321A (en) | 2016-11-10 | 2016-11-10 | A kind of preparation method of the soft glass polishing fluid of zirconium matrix |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610989319.0A CN108070321A (en) | 2016-11-10 | 2016-11-10 | A kind of preparation method of the soft glass polishing fluid of zirconium matrix |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108070321A true CN108070321A (en) | 2018-05-25 |
Family
ID=62154364
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610989319.0A Pending CN108070321A (en) | 2016-11-10 | 2016-11-10 | A kind of preparation method of the soft glass polishing fluid of zirconium matrix |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108070321A (en) |
-
2016
- 2016-11-10 CN CN201610989319.0A patent/CN108070321A/en active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| TWI582055B (en) | Ultra fine milk of lime composition | |
| CN103992743B (en) | Polishing fluid and its preparation process containing cerium dioxide powder Yu colloidal silicon dioxide compound abrasive | |
| CN108430616A (en) | The method for determining the mineralogical characteristic of calcining and flux calcination diatomaceous earth products | |
| CN105731855A (en) | Vertical mill slag grinding aid and preparation method thereof | |
| CN107235649B (en) | A kind of cement grinding aid and preparation method thereof | |
| CN112557429B (en) | Quantitative determination method and sample preparation method for all minerals in graphite ore | |
| CN108956675A (en) | For CO2In-situ comparative analysis method for rock mineral components before and after water-rock reaction | |
| CN105597944A (en) | Fluorite ore flotation method | |
| CN105675636B (en) | A kind of XRD quantitative analysis methods based on gypsoide in cement-based material | |
| CN101936832B (en) | New method for particle size analysis of ferruginous cemented mud rock | |
| CN110698104A (en) | Method for repairing cement-based material cracks by using soybean urease | |
| CN104865185A (en) | Method for analyzing lithofacies of powder samples | |
| CN104152054B (en) | A kind of preparation method of soft glass polishing fluid of zirconium matrix | |
| CN108535297A (en) | The identification method of metal oxide object phase in a kind of vanadium-titanium magnitite sinter | |
| CN108516713B (en) | Pretreatment and application method of phosphogypsum | |
| CN107932348B (en) | A kind of silicon rubber is the viscoplasticity magnetic abrasive tool and preparation method thereof of matrix | |
| CN108070321A (en) | A kind of preparation method of the soft glass polishing fluid of zirconium matrix | |
| CN206325500U (en) | A kind of silica polishing fluid configuration device | |
| CN103952084B (en) | A kind of preparation method of metal-polishing liquid of alumina host | |
| CN104017498A (en) | Preparation method of automobile polishing solution with alumina substrate | |
| Cui et al. | Preparation of CaCO-SiO composite with core-shell structure and its application in silicone rubber | |
| CN104843729B (en) | Process and its application of zeolite are prepared under a kind of normal temperature and pressure | |
| CN110117182A (en) | A kind of fluorite Pellet production method | |
| CN108102428A (en) | The method that ball milling modification prepares ultra-fine powdered whiting | |
| CN108640686A (en) | A kind of europium yttrium is co-doped with calcirm-fluoride scintillating ceramic and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180525 |
|
| WD01 | Invention patent application deemed withdrawn after publication |