CN104098992A - Wipe-wash-resisting wall paint and preparation method thereof - Google Patents
Wipe-wash-resisting wall paint and preparation method thereof Download PDFInfo
- Publication number
- CN104098992A CN104098992A CN201410361739.5A CN201410361739A CN104098992A CN 104098992 A CN104098992 A CN 104098992A CN 201410361739 A CN201410361739 A CN 201410361739A CN 104098992 A CN104098992 A CN 104098992A
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- CN
- China
- Prior art keywords
- parts
- wall paint
- revs
- wipe
- wash
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003973 paint Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000012188 paraffin wax Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 6
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims abstract description 6
- 239000005543 nano-size silicon particle Substances 0.000 claims abstract description 6
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229920000180 alkyd Polymers 0.000 claims abstract description 5
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 238000005201 scrubbing Methods 0.000 claims description 15
- 239000005083 Zinc sulfide Substances 0.000 claims description 13
- 229910052984 zinc sulfide Inorganic materials 0.000 claims description 13
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 9
- 229920000126 latex Polymers 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 235000010985 glycerol esters of wood rosin Nutrition 0.000 claims description 4
- 239000004816 latex Substances 0.000 claims description 3
- -1 2 parts~2.5 parts Substances 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 4
- 239000000839 emulsion Substances 0.000 abstract 2
- 235000011187 glycerol Nutrition 0.000 abstract 2
- 235000012239 silicon dioxide Nutrition 0.000 abstract 2
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 125000005456 glyceride group Chemical group 0.000 abstract 1
- 239000000945 filler Substances 0.000 description 3
- 239000000049 pigment Substances 0.000 description 2
- 239000011118 polyvinyl acetate Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses a wipe-wash-resisting wall paint, which is prepared from the following raw materials in parts by weight: 20 to 30 parts of water, 2 to 2.5 parts of paraffin wax, 1 to 2 parts of glycerine, 3 to 5 parts of nano silicon dioxide, 5 to 7 parts of silicone-acrylic emulsion, 3 to 5 parts of lithopone and 30 to 40 parts of film forming matter, wherein the film forming matter is composed of 35% of maleic anhydride modified rosin glyceride and 65% of rosin modified alkyd resin. The preparation method comprises the following steps: adding water, paraffin wax, glycerine and grinded lithopone into a high-speed dispersion machine to be dispersed uniformly; adding nano silicon dioxide, silicone-acrylic emulsion and the film forming matter in a mixture to be mixed uniformly; filtering the mixture when the viscosity is measured 93 KU to 100 KU to obtain the wipe-wash-resisting wall paint. The wipe-wash-resisting wall paint is excellent in wipe-wash-resisting performance, low in cost, and high in price performance ratio.
Description
Technical field
The present invention relates to building coating technical field, especially a kind of scrubbing resistance wall paint and preparation method thereof.
Background technology
At present, commercially available wall paint adopts polyvinyl acetate (PVA) as filmogen conventionally, in order to improve the performance of product, has added more pigment and ultra-fine, relatively large filler, oil number and the specific surface area of these fillers are large, make product paint film light, good hand touch.But because the addition of pigment and filler is too high, the particle diameter of polyvinyl acetate (PVA) is larger, is unfavorable for film forming, cause that paint film is fine and close, weathering resistance is poor, scrub resistance is poor.
Summary of the invention
The object of this invention is to provide a kind of scrubbing resistance wall paint and preparation method thereof, this scrubbing resistance wall paint and preparation method thereof can solve the poor problem of scrub performance.
In order to address the above problem, the technical solution used in the present invention is: a kind of preparation method of scrubbing resistance wall paint, adopt the raw material of following parts by weight to be prepared from: 20 parts～30 parts, water, 2 parts～2.5 parts, paraffin, 1 part～2 parts of glycerol, 3 parts～5 parts of nano silicons, 5 parts～7 parts of organosilicon crylic acid latexs, 3 parts～5 parts, zinc sulfide white, 30 parts～40 parts of filmogens; Wherein said filmogen consists of 35% maleic anhydride modified ester gum and 65% rosin modified alkyd resin.
Preparation method comprises the following steps:
A, zinc sulfide white is proceeded to shredder be ground to granularity and be less than 50 microns;
B, Jiang Shui, paraffin, the zinc sulfide white after glycerol and grinding proceeds in high speed dispersor, under the rotating speed of 1500 revs/min～2000 revs/min, disperses 45 minutes～60 minutes;
C, step B gained material is proceeded to stirrer, add successively while stirring nano silicon, organosilicon crylic acid latex and filmogen, mix; Wherein, stirring velocity is 500 revs/min～600 revs/min;
D, when the viscosity of above-mentioned mixing solutions is 93KU～100 KU, filter, obtain scrubbing resistance wall paint.
Owing to having adopted technique scheme, the present invention compared with prior art has following beneficial effect:
1, this wall paint adopts mixture containing the rosin modified alkyd resin of 35% maleic anhydride modified ester gum and 65% as filmogen, has significantly improved the scuff resistance of wall paint.
2, this wall paint has added nano silicon, makes product property stable, paint film smooth, and resistance to acids and bases, resistance to yellow, ageing-resistant performance are good.
3, the component of this wall paint is simple and easy to get, and cost is low, is the scrubbing resistance wall paint that a kind of novel cost performance is higher.
Embodiment
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
Zinc sulfide white is proceeded to shredder and be ground to granularity and be less than 50 microns, by 2.5 kg water, 0.2 kilogram of paraffin, the zinc sulfide white after 0.15 kilogram of glycerol and 0.4 kilogram of grinding proceeds in high speed dispersor, under the rotating speed of 1800 revs/min, disperses 50 minutes; Gained material is proceeded to stirrer, add successively while stirring 0.5 kilogram of nano silicon, 0.7 kilogram of organosilicon crylic acid latex and 4 kilograms of filmogens, controlling stirring velocity is 550 revs/min, mixes; Detect the viscosity of solution, when the viscosity of solution to be mixed is 96KU, filter, obtain scrubbing resistance wall paint.
Embodiment 2
Zinc sulfide white is proceeded to shredder and be ground to granularity and be less than 50 microns, by 30 kg water, 2.5 kilograms of paraffin, the zinc sulfide white after 2 kilograms of glycerol and 3 kilograms of grindings proceeds in high speed dispersor, under the rotating speed of 1500 revs/min, disperses 45 minutes; Gained material is proceeded to stirrer, add successively while stirring 4 kilograms of nano silicons, 5 kilograms of organosilicon crylic acid latexs and 30 kilograms of filmogens, controlling stirring velocity is 600 revs/min, mixes; Detect the viscosity of solution, when the viscosity of solution to be mixed is 93KU, filter, obtain scrubbing resistance wall paint.
Embodiment 3
Zinc sulfide white is proceeded to shredder and be ground to granularity and be less than 50 microns, by 200 kg water, 22.5 kilograms of paraffin, the zinc sulfide white after 10 kilograms of glycerol and 50 kilograms of grindings proceeds in high speed dispersor, under the rotating speed of 1500 revs/min, disperses 60 minutes; Gained material is proceeded to stirrer, add successively while stirring 30 kilograms of nano silicons, 60 kilograms of organosilicon crylic acid latexs and 350 kilograms of filmogens, controlling stirring velocity is 500 revs/min, mixes; Detect the viscosity of solution, when the viscosity of solution to be mixed is 100KU, filter, obtain scrubbing resistance wall paint.
To embodiment 1, the main performance index of the scrubbing resistance wall paint of embodiment 2 and embodiment 3 preparations is measured respectively, and measurement result is in Table 1:
Table 1 scrubbing resistance wall paint performance index
Claims (3)
1. a scrubbing resistance wall paint, is characterized in that, is prepared from: 20 parts～30 parts, water by the raw material of following parts by weight, 2 parts～2.5 parts, paraffin, 1 part～2 parts of glycerol, 3 parts～5 parts of nano silicons, 5 parts～7 parts of organosilicon crylic acid latexs, 3 parts～5 parts, zinc sulfide white, 30 parts～40 parts of filmogens; Wherein said filmogen consists of 35% maleic anhydride modified ester gum and 65% rosin modified alkyd resin.
2. the preparation method of a scrubbing resistance wall paint, it is characterized in that, adopt the raw material of following parts by weight to be prepared from: 20 parts～30 parts, water, 2 parts～2.5 parts, paraffin, 1 part～2 parts of glycerol, 3 parts～5 parts of nano silicons, 5 parts～7 parts of organosilicon crylic acid latexs, 3 parts～5 parts, zinc sulfide white, 30 parts～40 parts of filmogens; Wherein said filmogen consists of 35% maleic anhydride modified ester gum and 65% rosin modified alkyd resin.
3. preparation method comprises the following steps:
A, zinc sulfide white is proceeded to shredder be ground to granularity and be less than 50 microns;
B, Jiang Shui, paraffin, the zinc sulfide white after glycerol and grinding proceeds in high speed dispersor, under the rotating speed of 1500 revs/min～2000 revs/min, disperses 45 minutes～60 minutes;
C, step B gained material is proceeded to stirrer, add successively while stirring nano silicon, organosilicon crylic acid latex and filmogen, mix; Wherein, stirring velocity is 500 revs/min～600 revs/min;
D, when the viscosity of above-mentioned mixing solutions is 93KU～100 KU, filter, obtain scrubbing resistance wall paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410361739.5A CN104098992B (en) | 2014-07-28 | 2014-07-28 | Scrubbing resistance wall paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410361739.5A CN104098992B (en) | 2014-07-28 | 2014-07-28 | Scrubbing resistance wall paint and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104098992A true CN104098992A (en) | 2014-10-15 |
| CN104098992B CN104098992B (en) | 2016-04-27 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410361739.5A Active CN104098992B (en) | 2014-07-28 | 2014-07-28 | Scrubbing resistance wall paint and preparation method thereof |
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| CN (1) | CN104098992B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105017894A (en) * | 2015-07-29 | 2015-11-04 | 广西梧州龙鱼漆业有限公司 | Nano composite material wall paint |
| CN106893376A (en) * | 2017-03-29 | 2017-06-27 | 广西宏业能源科技有限公司 | A kind of water-fast washable interior wall coating |
| CN107353789A (en) * | 2017-07-18 | 2017-11-17 | 太仓市双凤镇薄彩工艺品厂 | A kind of transparent anti-scratch washcoat for outdoor coloured glaze post |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004115685A (en) * | 2002-09-27 | 2004-04-15 | Pentel Corp | Water-based ink for cloth |
| CN101597447A (en) * | 2009-07-13 | 2009-12-09 | 赵青山 | A kind of nano paint |
| CN102786851A (en) * | 2011-05-16 | 2012-11-21 | 李长山 | Preparation method for external wall nanometer emulsion paint |
| CN103467829A (en) * | 2013-09-25 | 2013-12-25 | 南京天诗新材料科技有限公司 | Nano-silicon dioxide loaded wax water-based dispersion, and preparation method and use thereof |
-
2014
- 2014-07-28 CN CN201410361739.5A patent/CN104098992B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004115685A (en) * | 2002-09-27 | 2004-04-15 | Pentel Corp | Water-based ink for cloth |
| CN101597447A (en) * | 2009-07-13 | 2009-12-09 | 赵青山 | A kind of nano paint |
| CN102786851A (en) * | 2011-05-16 | 2012-11-21 | 李长山 | Preparation method for external wall nanometer emulsion paint |
| CN103467829A (en) * | 2013-09-25 | 2013-12-25 | 南京天诗新材料科技有限公司 | Nano-silicon dioxide loaded wax water-based dispersion, and preparation method and use thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105017894A (en) * | 2015-07-29 | 2015-11-04 | 广西梧州龙鱼漆业有限公司 | Nano composite material wall paint |
| CN106893376A (en) * | 2017-03-29 | 2017-06-27 | 广西宏业能源科技有限公司 | A kind of water-fast washable interior wall coating |
| CN107353789A (en) * | 2017-07-18 | 2017-11-17 | 太仓市双凤镇薄彩工艺品厂 | A kind of transparent anti-scratch washcoat for outdoor coloured glaze post |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104098992B (en) | 2016-04-27 |
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