CN104091515B - Chemical equipment checking maintenance instructional device and chemical process flow - Google Patents

Chemical equipment checking maintenance instructional device and chemical process flow Download PDF

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Publication number
CN104091515B
CN104091515B CN201410362576.2A CN201410362576A CN104091515B CN 104091515 B CN104091515 B CN 104091515B CN 201410362576 A CN201410362576 A CN 201410362576A CN 104091515 B CN104091515 B CN 104091515B
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chemical
tower
plate column
pump
equipment
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CN104091515A (en
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郑根武
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Nanjing College of Chemical Technology
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Nanjing College of Chemical Technology
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Abstract

The invention discloses a kind of chemical equipment checking maintenance instructional device and chemical process flow, this device includes chemical industry equipment, chemical instruments, device frame and chemical pipeline, chemical industry equipment includes storage tank, dynamic equipment, reactor, tower and heat exchanger, chemical industry equipment and chemical instruments are placed on the position adapted and coordinate chemical pipeline to form a complete chemical process flow.The chemical equipment checking maintenance instructional device that the present invention provides; chemical industry equipment, chemical instruments are placed on the position adapted and coordinate chemical pipeline to collectively constitute a complete chemical process flow; it is easy to student get information about the running status of device in each step in chemical process flow and perform the operation of the checking maintenance to each device; the skilled technical ability grasping dismantling device, meets each universities and colleges chemical equipment class personnel training needs and the vocational training for the workers and staff needs of enterprise.

Description

Chemical equipment checking maintenance instructional device and chemical process flow
Technical field
The invention belongs to education, chemical equipment and chemical process technical field, be specifically related to a kind of change managing real integration Frock, for checking maintenance instructional device and chemical process flow, is used for carrying out all kinds of universities and colleges chemical equipment class and relevant speciality thereof Teaching combining theory with practice and Special Technique Training.
Background technology
Chemical equipment is the important support of Chemical Manufacture, and to ensure that producing long period runs continuously, and its important leverage is Need large quantities of to be engaged in chemical machinery equipment maintenance, the application-directed specialty talent overhauling, manufacturing.According to chemical industry in China Association adds up, and chemical equipment installs, overhaul, manage, manufacture post supply and demand ratio is about 1:4, far from meeting chemical industry row The industry demand to chemical equipment professional, chemical equipment one line operator the most do not adapt to modern chemical industry industry with existing For the development of chemical enterprise, in the urgent need to cultivate large quantities of high-quality senior Skill and method chemical equipment manufactures, install, overhaul, Managerial talent.Situated teaching is the effective way improving Talent-cultivating Quality, and each universities and colleges have successively built large quantities of changes Frock is for coach concourse, but there is a certain distance with the checking maintenance of true factory, it is difficult to meet each universities and colleges chemical industry dress Standby class personnel training needs and the vocational training for the workers and staff of enterprise.
The prevailing scenario of chemical plant installations class professional teaching substantially has following several at present: the first chemical pipeline attaching/detaching apparatus, This device is to build number in the classroom of a spaciousness to overlap duplicate pipeline attaching/detaching apparatus, can meet array simultaneously Member carries out pipeline checking maintenance real training;The second is heat exchanger attaching/detaching apparatus, and this device is built-in in the classroom of a spaciousness If number overlaps the duplicate movable tube sheets heat exchanger being arranged on certain altitude, array student can be met simultaneously and carry out heat exchanger Checking maintenance real training;The third is tower class actual training device, and such device is the height according to classroom, builds number set completely The same tower equipment, can meet array student simultaneously and carry out the checking maintenance real training of tower kind equipment.Above actual training device is altogether Being all to build in spacious, spacious classroom with feature, the object of building is all equipment that is single and that repeat, and true The checking maintenance operation of real chemical enterprise is all carried out on chemical production device or at periphery, is at a solid space Operate under state, relate to various device, it is clear that the checking maintenance actual training device of school and true chemical plant installations at present Differ greatly, it is impossible to implement in full the purpose cultivating the checking maintenance talent.
Summary of the invention
For solving the deficiencies in the prior art, the invention provides a kind of chemical equipment checking maintenance instructional device, chemical industry is set Standby, chemical instruments are placed on the position adapted and coordinate chemical pipeline to collectively constitute a complete chemical process flow, It is easy to student get information about the running status of device in each step in chemical process flow and perform the inspection to each device The operation of maintenance, the skilled technical ability grasping dismantling device, meet each universities and colleges chemical equipment class personnel training needs and enterprise Vocational training for the workers and staff need.
To achieve these goals, the technical solution adopted in the present invention is:
Chemical equipment checking maintenance instructional device, it is characterised in that: include chemical industry equipment, chemical instruments, device frame and Chemical pipeline, described chemical industry equipment is arranged on device frame, described chemical instruments be installed on corresponding chemical industry equipment or On chemical pipeline, described chemical industry equipment is connected as an entirety by chemical pipeline, and described chemical industry equipment includes storage tank, moves Equipment, reactor, tower and heat exchanger, described chemical industry equipment and chemical instruments are placed on the position adapted and coordinate Chemical pipeline forms a complete chemical process flow;
Described storage tank includes head tank V6101 and return tank, and wherein head tank V6101 is arranged at the inspection of whole chemical equipment Maintenance instructional device foremost, described head tank V6101 be aided with flange by chemical pipeline between upstream device and be connected Connecing, described return tank includes the first return tank V6201, the second return tank V6301 and the 3rd return tank V6501, institute State return tank to be aided with flange with upstream and downstream equipment by chemical pipeline and be connected;
Described dynamic equipment includes expecting pump and vacuum pump set C6501, described material pump include raw material pump P6101, elevator pump and Reflux pump, described elevator pump includes the first elevator pump P6102, the second elevator pump P6201, the 3rd elevator pump P6301, Described reflux pump includes the first reflux pump P6202, the second reflux pump P6302 and the 3rd reflux pump P6501, described former Material pump P6101 is installed on the downstream of head tank V6101, and described elevator pump and reflux pump are aided with by chemical pipeline respectively Flange is connected with the equipment of upstream and downstream, and described vacuum pump set C6501 is arranged on the 3rd follow-up cooler E6502 Outlet gas line on, be connected with vapor delivery line by flange;
Described reactor includes two reactors, and described reactor includes the first reactor R6101 and the second reactor R6102, described first reactor R6101 is internal coil-tube type reactor, and described second reactor R6102 is jacket type Reactor, the upstream extremity of described reactor is connected with head tank V6101 by chemical pipeline, and described reactor is with former Being provided with raw material pump P6101 between batch can V6101, the downstream of described reactor is aided with by chemical pipeline with upstream device Flange is connected, and is provided with the first elevator pump P6102 between described reactor and corresponding upstream device;
Described tower includes at least two plate column and a packed tower T6301, and described plate column includes the first plate column T6201 and the second plate column T6501, the upstream extremity of described first plate column T6201 passes through chemical pipeline and reactor phase Connect, between described first plate column T6201 and reactor, be provided with the first elevator pump P6102, described first plate column The downstream of T6201 is aided with flange with the upstream extremity of packed tower T6301 by chemical pipeline and is connected, described first plate Be provided with the second elevator pump P6201 between formula tower T6201 and packed tower T6301, the downstream of described packed tower T6301 with The upstream extremity of the second plate column T6501 is aided with flange by chemical pipeline and is connected, described packed tower T6301 and second Being provided with the 3rd elevator pump P6301, described first plate column T6201 between plate column T6501 is that sectional type four saves tower tray, Often joint tower tray is followed successively by bubble-cap type, sieve-board type, float-valve type and tongue shape formula, described second plate column T6501 from top to bottom For made of one piece tower tray, being set to upper and lower two-layer, every layer of tower tray is designed as float-valve type and sieve-board type tower tray the most successively, Described packed tower T6301 is set to the upper and lower, and the upper strata of described packed tower T6301 is gauze structured packing, described The lower floor of packed tower T6301 is Pall ring random packing;
Described heat exchanger includes that reboiler E6201, condenser and cooler, described condenser include the first condenser E6202, the second condenser E6301 and the 3rd condenser E6501, described cooler include the first cooler E6203, Second cooler E6302 and the 3rd cooler E6502, described reboiler E6201 and the first plate column T6201 are connected Connect and be located at the side-lower of the first plate column T6201, described first plate column T6201, the first condenser E6202, One cooler E6203 and the first return tank V6201 the most end to end formation loop, described first plate column T6201 And be provided with between the first return tank V6201 the first reflux pump P6202, described packed tower T6301, the second condenser E6301, Second cooler E6302 and the second return tank V6301 the most end to end formation loop, described packed tower T6301 And it is provided with the second reflux pump P6302, described second plate column T6501, the 3rd condenser between the second return tank V6301 E6501, the 3rd cooler E6502 and the 3rd return tank V6501 the most end to end formation loop, described second The 3rd reflux pump P6501, described reboiler E6201, cold it is provided with between plate column T6501 and the 3rd return tank V6501 Condenser and cooler are respectively adopted fixed tube sheet type, floating head type and U-shaped pipe heat exchanger.
Aforesaid chemical equipment checking maintenance instructional device, it is characterised in that: the diameter of described tower with for checking maintenance, dress The manhole unloading tower tray and filler is suitable.
Aforesaid chemical equipment checking maintenance instructional device, it is characterised in that: described chemical instruments include thermometer, pressure Table, flow meter, content gauge, Field adjustment valve and in-situ transducer.
Aforesaid chemical equipment checking maintenance instructional device, it is characterised in that: described device frame is set to two-layer.
Aforesaid chemical equipment checking maintenance instructional device, it is characterised in that: described chemical industry equipment is arranged over twin beams lifting Machine.
Chemical process flow based on aforesaid chemical equipment checking maintenance instructional device, it is characterised in that:
1) in head tank V6101, the raw material outside battery limit (BL) is put into, the head tank V6101 storage of raw materials;
2) being got by the raw material in head tank V6101 by raw material pump P6101 and enter in reactor, raw material is in reaction Still carries out reacting until having reacted by stirring;
3) material after having reacted is got from reactor through the first elevator pump P6102 and is entered into the first plate column In T6201, the light component in material is discharged from the tower top of the first plate column T6201, and sequentially passes through the first condenser E6202, the first cooler E6203 carry out condensing cooling down operation, flow into afterwards in the first return tank V6201, pass through First reflux pump P6202 gets from the first return tank V6201, and a part returns to the first plate as overhead reflux liquid In formula tower T6201, remainder is then as the extraction of light component product 1, and the heavy constituent in material is at the first plate column T6201 Tower bottom through reboiler E6201 heat to evaporate light component further, be deposited at the bottom of the first plate column T6201 tower The tower bottoms in portion is in the second elevator pump P6201 gets entrance packed tower T6301;
4), after the tower bottoms of the first plate column T6201 enters in packed tower T6301, light component is from packed tower T6301 Tower top discharge, sequentially pass through the second condenser E6301, the second cooler E6302 carry out condense cooling down operation, it In rear inflow the second return tank V6301, got from the second return tank V6301 by the second reflux pump P6302, one Part returns in packed tower T6301 as overhead reflux liquid, and remainder is as the extraction of light component product 2, deposition Tower bottoms bottom packed tower T6301 is in the 3rd elevator pump P6301 gets entrance the second plate column T6501;
5), after during the tower bottoms of packed tower T6301 enters into the second plate column T6501, carry at vacuum pump set C6501 Under the vacuum condition of confession, light component is discharged from the tower top of the second plate column T6501, sequentially pass through the 3rd condenser E6501, 3rd cooler E6502 carries out condensing cooling down operation, flows into afterwards in the 3rd return tank V6501, by the 3rd backflow Pump P6501 gets from the 3rd return tank V6501, and a part returns to the second plate column T6501 as overhead reflux liquid In, remainder, as the extraction of light component product 4, is deposited on the tower bottoms conduct of the second plate column T6501 tower bottom Final component product 3 is discharged from tower bottom.
Aforesaid chemical process flow, it is characterised in that: step 2) in, the first reactor R6101 in reactor, Second reactor R6102 blocked operation, raw material carries out reacting required heat in a kettle. to be provided by adding vapours, Reaction temperature is by adding the amount of vapours to regulate control.
Aforesaid chemical process flow, it is characterised in that: step 5) in, it is cold that vacuum pump set C6501 is arranged on the 3rd But, on the outlet gas line of device E6502, it is connected with vapor delivery line by flange.
The invention have the benefit that a kind of chemical equipment checking maintenance instructional device that the present invention provides, set including chemical industry Standby, chemical instruments, device frame and chemical pipeline, wherein chemical industry equipment includes storage tank, dynamic equipment, reactor, tower And heat exchanger, device frame is used for supporting whole chemical equipment checking maintenance instructional device, maintains the stability of device, And chemical industry equipment, chemical instruments are placed on the position adapted and coordinate chemical pipeline to collectively constitute a complete chemical industry work Process flow, overcome in the past simple and machinery repeat same device so that cannot the drawback of practical in production process, It is easy to student get information about the running status of device in each step in chemical process flow and perform the inspection to each device The operation of maintenance, and the device owing to using in each step is different, the model of same device is different, whipped form or Heat transfer type is different, it is simple to the device of the various model of student's the cognition and comprehension, and the skilled technical ability grasping dismantling device, to various Chemical industry equipment has understanding directly perceived and deep and grasp, comprehensively implements to cultivate the plan of the checking maintenance talent.
Accompanying drawing explanation
Fig. 1 is the process chart of the chemical equipment checking maintenance instructional device of the present invention;
Fig. 2 is the equipment site plan of the chemical equipment technology checking maintenance device of the present invention;
Fig. 3 is the equipment facade layout drawing of the chemical equipment technology checking maintenance device of the present invention;
Fig. 4 is the structural representation of first plate column of the present invention;
Fig. 5 is the structural representation of second plate column of the present invention;
Fig. 6 is the structural representation of the packed tower of the present invention;
The structural representation of Fig. 7 device frame.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the present invention made concrete introduction.
As shown in Figures 1 to 7, chemical equipment checking maintenance instructional device, including chemical industry equipment, chemical instruments, device Framework and chemical pipeline, described chemical industry equipment is arranged on device frame, and described chemical instruments are installed on corresponding chemical industry On equipment or chemical pipeline, described chemical industry equipment is connected as an entirety by chemical pipeline, and described chemical industry equipment includes storage Tank, dynamic equipment, reactor, tower and heat exchanger, described chemical industry equipment and chemical instruments are placed on the position adapted And coordinate chemical pipeline to form a complete chemical process flow, the construction place of this chemical equipment checking maintenance instructional device Length be respectively 24m, 16m, 9m.
Described storage tank includes head tank V6101 and return tank, and wherein head tank V6101 is arranged at the inspection of whole chemical equipment Maintenance instructional device foremost, described head tank V6101 be aided with flange by chemical pipeline between upstream device and be connected Connecing, described return tank includes the first return tank V6201, the second return tank V6301 and the 3rd return tank V6501, institute State return tank to be aided with flange with upstream and downstream equipment by chemical pipeline and be connected.
Described dynamic equipment includes expecting pump and vacuum pump set C6501, described material pump include raw material pump P6101, elevator pump and Reflux pump, described elevator pump includes the first elevator pump P6102, the second elevator pump P6201, the 3rd elevator pump P6301, Described reflux pump includes the first reflux pump P6202, the second reflux pump P6302 and the 3rd reflux pump P6501, described former Material pump P6101 is installed on the downstream of head tank V6101, and described elevator pump and reflux pump are aided with by chemical pipeline respectively Flange is connected with the equipment of upstream and downstream, and described vacuum pump set C6501 is connected with vapor delivery line by flange.
Described reactor includes two reactors, and described reactor includes the first reactor R6101 and the second reactor R6102, described first reactor R6101 is internal coil-tube type reactor, and described second reactor R6102 is jacket type Reactor, the upstream extremity of described reactor is connected with head tank V6101 by chemical pipeline, and described reactor is with former Be provided with raw material pump P6101 between batch can V6101, also measuring tank can be set in the front end of reactor, it is simple to accurately metering from The material quantity that head tank V6101 gets, it is ensured that effectively carrying out of reaction, the downstream of described reactor and upstream device It is aided with flange by chemical pipeline to be connected, is provided with first between described reactor and corresponding upstream device and carries Rising pump P6102, the motor of reactor is connected with shaft by shaft joint after reductor slows down, shaft and upper envelope Head uses mechanical seal form, upper cover and kettle to use Flange joint, and kettle uses with low head and is welded to connect.
Described tower includes at least two plate column and a packed tower T6301, and described plate column includes the first plate column T6201 and the second plate column T6501, the upstream extremity of described first plate column T6201 passes through chemical pipeline and reactor phase Connect, between described first plate column T6201 and reactor, be provided with the first elevator pump P6102, described first plate column The downstream of T6201 is aided with flange with the upstream extremity of packed tower T6301 by chemical pipeline and is connected, described first plate Be provided with the second elevator pump P6201 between formula tower T6201 and packed tower T6301, the downstream of described packed tower T6301 with The upstream extremity of the second plate column T6501 is aided with flange by chemical pipeline and is connected, described packed tower T6301 and second Being provided with the 3rd elevator pump P6301, described first plate column T6201 between plate column T6501 is that sectional type four saves tower tray, Often joint tower tray is followed successively by bubble-cap type, sieve-board type, float-valve type and tongue shape formula, described second plate column T6501 from top to bottom For made of one piece tower tray, being set to upper and lower two-layer, every layer of tower tray is designed as float-valve type and sieve-board type tower tray the most successively, Described packed tower T6301 is set to the upper and lower, and the upper strata of described packed tower T6301 is gauze structured packing, described The lower floor of packed tower T6301 is Pall ring random packing;The diameter of tower is used with for checking maintenance, handling tower tray and filler Manhole suitable.
Described heat exchanger includes that reboiler E6201, condenser and cooler, described condenser include the first condenser E6202, the second condenser E6301 and the 3rd condenser E6501, described cooler include the first cooler E6203, Second cooler E6302 and the 3rd cooler E6502, described reboiler E6201 and the first plate column T6201 are connected Connect and be located at the side-lower of the first plate column T6201, described first plate column T6201, the first condenser E6202, One cooler E6203 and the first return tank V6201 the most end to end formation loop, described first plate column T6201 And be provided with between the first return tank V6201 the first reflux pump P6202, described packed tower T6301, the second condenser E6301, Second cooler E6302 and the second return tank V6301 the most end to end formation loop, described packed tower T6301 And it is provided with the second reflux pump P6302, described second plate column T6501, the 3rd condenser between the second return tank V6301 E6501, the 3rd cooler E6502 and the 3rd return tank V6501 the most end to end formation loop, described second The 3rd reflux pump P6501, described reboiler E6201, cold it is provided with between plate column T6501 and the 3rd return tank V6501 Condenser and cooler are respectively adopted fixed tube sheet type, floating head type and U-shaped pipe heat exchanger, exchanger head and main body Using Flange joint, exchanger tubes and tubesheets uses and is welded to connect.
Chemical instruments include thermometer, Pressure gauge, flow meter, content gauge, Field adjustment valve and in-situ transducer, On the one hand each Major understanding to different instrument and meters can be met, on the other hand also for chemical equipment inspection dimension The training during repairing protected instrument and meter, arranges and the needs of checking maintenance according to chemical production device equipment, by institute Having chemical equipment to be arranged on the device frame with two-layer working place, chemical industry equipment is arranged over double girder crane, This chemical equipment checking maintenance instructional device can be made closer in real checking maintenance workshop, chemical industry equipment can be met again Being actually needed of checking maintenance.
Considering the needs of nationwide Skill Competition at different levels, the chemical equipment checking maintenance instructional device of the present invention sets During standby layout, from technological process, have selected the raw material pump of applicable Skill Competition especially, be designed with before and after pump and the whole nation The pipeline dismounting flow process that Skill Competition is identical, in order to take into account whole nation Skill Competition and select the needs of player and training.
The step building this chemical equipment checking maintenance instructional device is:
The first step, chooses the chemical equipment needing to carry out checking maintenance operation, and the concrete condition according to building place determines respectively The overall dimensions of chemical industry equipment, is listed as follows:
Sequence number Device name Specification Quantity Material
1 Head tank Φ1300*2000 1 304
2 Return tank Φ1000*1200 3 304
3 Reactor Φ1500*1500 2 304
4 Condenser Φ800*2000 3 304
5 Cooler Φ500*1500 3 304
6 Reboiler Φ400*1000 1 304
7 First plate column Φ1200*6000 1 304
8 Second plate column Φ600*5000 1 304
9 Packed tower Φ700*5500 1 304
10 Material pump EG50/200-0.75/4 7 304
11 Vacuum pump set 2.2m3/min 1 304
Second step, determines the Flow Diagram for Chemical Process of this chemical equipment checking maintenance instructional device, as shown in Figure 1.
According to Fig. 1, the chemical process flow of this chemical equipment checking maintenance instructional device is:
1) in head tank V6101, the raw material outside battery limit (BL) is put into;
2) getting after being measured by the raw material in head tank V6101 by raw material pump P6101 enters in reactor, raw material Carry out reacting until having reacted by stirring in a kettle., the first reactor R6101 in reactor, second anti- Answering still R6102 blocked operation, raw material carries out reacting required heat in a kettle. to be provided by adding vapours, reaction temperature Degree is by adding the amount of vapours to regulate control;
3) material after having reacted is got from reactor through the first elevator pump P6102 and is entered into the first plate column In T6201, the light component in material is discharged from the tower top of the first plate column T6201, and sequentially passes through the first condenser E6202, the first cooler E6203 carry out condensing cooling down operation, flow into afterwards in the first return tank V6201, pass through First reflux pump P6202 gets from the first return tank V6201, and a part returns to the first plate as overhead reflux liquid In formula tower T6201, remainder is then as the extraction of light component product 1, and the heavy constituent in material is at the first plate column T6201 Tower bottom through reboiler E6201 heat to evaporate light component further, heat is provided simultaneously, is deposited on the first plate The tower bottoms of formula tower T6201 tower bottom is in the second elevator pump P6201 gets entrance packed tower T6301;
4), after entering in packed tower T6301 after the tower bottoms metering of T6201, the relatively low light component of boiling point is from filling out The tower top of material tower T6301 is discharged, and sequentially passes through the second condenser E6301, the second cooler E6302 carries out condensing cold But operate, flow in the second return tank V6301 afterwards, by the second reflux pump P6302 from the second return tank V6301 In get, a part return in packed tower T6301 as overhead reflux liquid, remainder is relatively low as boiling point Light component product 2 extraction, be deposited on the of a relatively high tower bottoms of the boiling point bottom packed tower T6301 through the 3rd lifting Pump P6301 gets in entrance the second plate column T6501;
5) after entering in the second plate column T6501 after the tower bottoms metering that boiling point is of a relatively high, at vacuum pump set C6501 Under the vacuum condition provided, light component is discharged from the tower top of the second plate column T6501, sequentially passes through the 3rd condenser E6501, the 3rd cooler E6502 carry out condensing cooling down operation, flow in the 3rd return tank V6501 afterwards, pass through 3rd reflux pump P6501 gets from the 3rd return tank V6501, and a part returns to the second plate as overhead reflux liquid In formula tower T6501, remainder, as the extraction of light component product 4, is deposited on the second plate column T6501 tower bottom Tower bottoms is discharged from tower bottom as final component product 3.
3rd step, designs equipment site plan and the equipment facade layout drawing of this chemical equipment technology checking maintenance device, As shown in Figure 2 and Figure 3.
4th step, according to the structural representation of tower chemical industry equipment as Figure 4-Figure 6, improves into and meets what chemical process required Information drawing.
5th step, designs device frame platform, as shown in Figure 7.
The installation of the 6th step, craft piping and field instrument.Will be each according to the Flow Diagram for Chemical Process of design in second step Connect into perfect technological process with chemical pipeline between chemical industry equipment, between chemical pipeline and chemical industry equipment, use flange even Connecing, the pipe fitting in pipeline such as elbow, threeway etc. use and are welded to connect, and the valve in pipeline is according to selected valve kind Class is respectively adopted welding or threaded, and the instrument in pipeline is respectively adopted welding according to selected different types of instrument Or it is threaded;Work progress should strictly be carried out by the various job specfications of chemical plant installations, it is ensured that device and actualization Work process units is as good as.
In this technological process, divided by the first plate column T6201, packed tower T6301 and the second plate column T6501 For the Light ends obtained is in accordance with the relative height of boiling point with heavy constituent, tower bottoms i.e. boiling point is of a relatively high Heavy constituent, the tower bottoms in the first plate column T6201 is separable into packed tower T6301 after entering packed tower T6301 Tower bottoms at the bottom of the light component of tower top and packed tower T6301 tower, the tower bottoms in packed tower T6301 is entering the second plate The restructuring at the bottom of the light component of the second plate column T6501 tower top and packed tower T6301 tower it is separable into again after formula tower T6501 Point, therefore, the light component in the first plate column T6201, packed tower T6301 and the second plate column T6501, weight Component is all comparatively speaking;And due to the simulation that this technological process is actual process flow process, do not specify concrete product Product, are therefore not limited to the height of concrete boiling point, it is simple to be adjusted according to actual, closer in actual process flow process, To be suitable for all kinds of teaching, it is simple to student intuitively understands the operation of each parts and the operation of checking maintenance, for student ability Train highly beneficial.
The ultimate principle of the present invention, principal character and advantage have more than been shown and described.The technical staff of the industry should Understanding, above-described embodiment limits the present invention the most in any form, and the mode of all employing equivalents or equivalent transformation is obtained The technical scheme obtained, all falls within protection scope of the present invention.

Claims (8)

1. chemical equipment checking maintenance instructional device, it is characterized in that: include chemical industry equipment, chemical instruments, device frame and chemical pipeline, described chemical industry equipment is arranged on device frame, described chemical instruments are installed on corresponding chemical industry equipment or chemical pipeline, it is overall that described chemical industry equipment is connected as one by chemical pipeline, described chemical industry equipment includes storage tank, dynamic equipment, reactor, tower and heat exchanger, and described chemical industry equipment and chemical instruments are placed on the position adapted and coordinate chemical pipeline to form a complete chemical process flow;
Described storage tank includes head tank (V6101) and return tank, wherein head tank (V6101) is arranged at whole chemical equipment checking maintenance instructional device foremost, described head tank (V6101) be aided with flange by chemical pipeline between upstream device and be connected, described return tank includes the first return tank (V6201), the second return tank (V6301) and the 3rd return tank (V6501), and described return tank is aided with flange with upstream and downstream equipment by chemical pipeline and is connected;
Described dynamic equipment includes expecting pump and vacuum pump set (C6501), described material pump includes raw material pump (P6101), elevator pump and reflux pump, described elevator pump includes the first elevator pump (P6102), second elevator pump (P6201), 3rd elevator pump (P6301), described reflux pump includes the first reflux pump (P6202), second reflux pump (P6302) and the 3rd reflux pump (P6501), described raw material pump (P6101) is installed on the downstream of head tank (V6101), described elevator pump and reflux pump are aided with flange with upper by chemical pipeline respectively, the equipment in downstream is connected, described vacuum pump set (C6501) is connected with vapor delivery line by flange;
Described reactor includes two reactors, described two reactors include the first reactor (R6101) and the second reactor (R6102), described first reactor (R6101) is internal coil-tube type reactor, described second reactor (R6102) is jacket type reactor, the upstream extremity of described two reactors is connected with head tank (V6101) by chemical pipeline, it is provided with raw material pump (P6101) between described two reactors and head tank (V6101), the downstream of described two reactors is aided with flange with upstream device by chemical pipeline and is connected, the first elevator pump (P6102) it is provided with between described two reactors and corresponding upstream device;
nullDescribed tower includes at least two plate column and a packed tower (T6301),Said two plate column includes the first plate column (T6201) and the second plate column (T6501),The upstream extremity of described first plate column (T6201) is connected by chemical pipeline and two reactors,It is provided with the first elevator pump (P6102) between described first plate column (T6201) and two reactors,The downstream of described first plate column (T6201) is aided with flange with the upstream extremity of packed tower (T6301) by chemical pipeline and is connected,It is provided with the second elevator pump (P6201) between described first plate column (T6201) and packed tower (T6301),The downstream of described packed tower (T6301) is aided with flange with the upstream extremity of the second plate column (T6501) by chemical pipeline and is connected,The 3rd elevator pump (P6301) it is provided with between described packed tower (T6301) and the second plate column (T6501),Described first plate column (T6201) is that sectional type four saves tower tray,Often joint tower tray is followed successively by bubble-cap type from top to bottom、Sieve-board type、Float-valve type and tongue shape formula,Described second plate column (T6501) is made of one piece tower tray,It is set to upper and lower two-layer,Every layer of tower tray is designed as float-valve type and sieve-board type tower tray the most successively,Described packed tower (T6301) is set to the upper and lower,The upper strata of described packed tower (T6301) is gauze structured packing,The lower floor of described packed tower (T6301) is Pall ring random packing;
nullDescribed heat exchanger includes reboiler (E6201)、Condenser and cooler,Described condenser includes the first condenser (E6202)、Second condenser (E6301) and the 3rd condenser (E6501),Described cooler includes the first cooler (E6203)、Second cooler (E6302) and the 3rd cooler (E6502),Described reboiler (E6201) is connected with the first plate column (T6201) and is located at the side-lower of the first plate column (T6201),Described first plate column (T6201)、First condenser (E6202)、First cooler (E6203) and the first return tank (V6201) the most end to end formation loop,It is provided with the first reflux pump (P6202) between described first plate column (T6201) and the first return tank (V6201),Described packed tower (T6301)、Second condenser (E6301)、Second cooler (E6302) and the second return tank (V6301) the most end to end formation loop,The second reflux pump (P6302) it is provided with between described packed tower (T6301) and the second return tank (V6301),Described second plate column (T6501)、3rd condenser (E6501)、3rd cooler (E6502) and the 3rd return tank (V6501) the most end to end formation loop,It is provided with the 3rd reflux pump (P6501) between described second plate column (T6501) and the 3rd return tank (V6501),Described reboiler (E6201)、Condenser and cooler are respectively adopted fixed tube sheet type、Floating head type and U-shaped pipe heat exchanger.
Chemical equipment checking maintenance instructional device the most according to claim 1, it is characterised in that: the diameter of described tower is suitable with the manhole for checking maintenance, handling tower tray and filler.
Chemical equipment checking maintenance instructional device the most according to claim 1, it is characterised in that: described chemical instruments include thermometer, Pressure gauge, flow meter, content gauge, Field adjustment valve and in-situ transducer.
Chemical equipment checking maintenance instructional device the most according to claim 1, it is characterised in that: described device frame is set to two-layer.
Chemical equipment checking maintenance instructional device the most according to claim 1, it is characterised in that: described chemical industry equipment is arranged over double girder crane.
6. chemical process flow based on the chemical equipment checking maintenance instructional device described in claim 1, it is characterised in that: comprise the following steps,
1) in head tank (V6101), the raw material outside battery limit (BL), head tank (V6101) storage of raw materials are put into;
2) being got by the raw material in head tank (V6101) by raw material pump (P6101) and enter in two reactors, raw material carries out reacting until having reacted by stirring in two reactors;
null3) material after having reacted is got from two reactors through the first elevator pump (P6102) and is entered in the first plate column (T6201),Light component in material is discharged from the tower top of the first plate column (T6201),And sequentially pass through the first condenser (E6202)、First cooler (E6203) carries out condensing cooling down operation,Flow into afterwards in the first return tank (V6201),Got from the first return tank (V6201) by the first reflux pump (P6202),A part returns in the first plate column (T6201) as the overhead reflux liquid of the first plate column (T6201),Remainder is then as the extraction of light component product I,Heavy constituent in material heats to evaporate light component further through reboiler (E6201) at the tower bottom of the first plate column (T6201),It is deposited on the tower bottoms of the first plate column (T6201) tower bottom in entrance packed tower (T6301) got by the second elevator pump (P6201);
null4) after during the tower bottoms of the first plate column (T6201) enters into packed tower (T6301),Light component in the tower bottoms of the first plate column (T6201) is discharged from the tower top of packed tower (T6301),Sequentially pass through the second condenser (E6301)、Second cooler (E6302) carries out condensing cooling down operation,Flow into afterwards in the second return tank (V6301),Got from the second return tank (V6301) by the second reflux pump (P6302),A part returns in packed tower (T6301) as the overhead reflux liquid of packed tower (T6301),Remainder is as the extraction of light component product II,It is deposited on the tower bottoms of packed tower (T6301) bottom in entrance the second plate column (T6501) got by the 3rd elevator pump (P6301);
null5) after the tower bottoms in packed tower (T6301) enters in the second plate column (T6501),Under the vacuum condition that vacuum pump set (C6501) provides,Light component in the tower bottoms of packed tower (T6301) is discharged from the tower top of the second plate column (T6501),Sequentially pass through the 3rd condenser (E6501)、3rd cooler (E6502) carries out condensing cooling down operation,Flow into afterwards in the 3rd return tank (V6501),Got from the 3rd return tank (V6501) by the 3rd reflux pump (P6501),A part returns in the second plate column (T6501) as the overhead reflux liquid of the second plate column (T6501),Remainder is as the extraction of light component product IV,The tower bottoms being deposited on the second plate column (T6501) tower bottom is discharged from tower bottom as final component product III.
Chemical process flow the most according to claim 6, it is characterized in that: step 2) in, the first reactor (R6101) in two reactors, the second reactor (R6102) blocked operation, raw material carries out reacting required heat in two reactors to be provided by adding vapours, and reaction temperature is by adding the amount of vapours to regulate control.
Chemical process flow the most according to claim 6, it is characterised in that: in step 5), vacuum pump set (C6501) is arranged on the outlet gas line of the 3rd cooler (E6502), is connected with vapor delivery line by flange.
CN201410362576.2A 2014-07-28 2014-07-28 Chemical equipment checking maintenance instructional device and chemical process flow Expired - Fee Related CN104091515B (en)

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