CN1040910A - Extracting method of drone nutrient and uses thereof - Google Patents
Extracting method of drone nutrient and uses thereof Download PDFInfo
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- CN1040910A CN1040910A CN88106581A CN88106581A CN1040910A CN 1040910 A CN1040910 A CN 1040910A CN 88106581 A CN88106581 A CN 88106581A CN 88106581 A CN88106581 A CN 88106581A CN 1040910 A CN1040910 A CN 1040910A
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- drone
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- ethanol
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Abstract
The invention provides a kind of extracting method of drone nutrient, and point out the purposes of the drone nutrient that extracts.
Drone nutrient method of the present invention be with drone, drone larvae and drone pupae through technical process such as fragmentation-dissolving-filtration-residue treatment-concentrate, the various nutrients in the drone body is extracted.In view of the drone nutrient that is extracted contains the most of content that surpasses in royal jelly of amino acid needed by human body, the multiple thing of supporting one's family, protein and its content, available drone nutrient is as the primary raw material of health medicine and the additive of nutraceutical.
Description
The invention provides a kind of extracting method of drone nutrient, and point out that it occupy pharmaceutical sanitary field and food additives field with the purposes of drone nutrient as the primary raw material and the nutraceutical additive of health medicine.
Bee products by people's development and use for many years, honey, royal jelly, pollen, bee venom is developed to multiple series of products by people, particularly the queen bee of every group of honeybees in the 3-5 of post-coitum every day with the speed reproduction of more than 1,000 ovum (surpass himself weight), this unusual biological phenomenon causes that people pay attention to the nutritive value height of grain-royal jelly of queen bee, yet do health medicine and high-grade nutrient food has formed upsurge in the world with royal jelly., human for providing a unique in life mating of honeybee queen, cause queen bee to produce ovum and reach drone more than 1,500,000, but do not attach the importance as yet.Also contain great variety of goods, amino acid needed by human body that quantity is enough in the drone body, contain multivitamin, protein, and the most of content that surpasses in royal jelly of its content, they are extracted, will inevitably bring benefit to the mankind.
The object of the present invention is to provide a kind of effective method, extract containing nutrient abundant in the drone body, and point out the purposes of these drone nutrients as health medicine primary raw material and nutraceutical additive.
The extracting method of drone nutrient provided by the present invention is with normotrophic, fresh or freezing drone, drone larvae and drone pupae, thrin, two or three merge and after fragmentation, to add in the solvent, transferring the pH value of this solution with acid again is 4～6, stir and extract, filter, filtration residue is dissolved in adds edible alkaline matter in the mixed liquor of organic solvent or organic solvent and water again and make solution keep neutral, repeat to stir and extract, filtering technique, the drone nutrient liquid that will directly extract from the drone raw material concentrates with being dissolved in the drone nutrient liquid difference or the merging decompression of extracting in the organic solvent residue, or makes the drone nutrient freeze-dried powder after concentrating.Solvent described in the said method is the aqueous solution of water, salt or the mixed liquor of water and organic solvent, and quantity of solvent is 1.5～8 times of molten broken drone amount, and institute's water is distilled water or drinking water, and said organic solvent is an ethanol, and the weight ratio of ethanol and water is 1: 1.Said filtering technique is normal temperature sieving and heating two steps of suction filtration in the said method.Filtration residue is dissolved in the mixed liquor of organic solvent or organic solution and water in the said method, and said organic solvent is an ethanol, and ethanol and water weight ratio are 1: 1, and used organic solvent amount is 1～6 times of molten filtration residue amount.
This extracting method is that fresh or freezing drone, drone larvae or drone pupae are pressed the device fragmentation with tissue mashing machine, colloid mill or multi-functional strand, be convenient to separating out of drone endotrophic element, with its broad be in order to promote the dissolving of drone nutrient in the aqueous solution that is weak property, filter and adopt the normal temperature sieving, be for the general graininess residue of elimination, the heating suction filtration is to be the elimination macro-molecular protein, for preventing destruction to nutrient, temperature must be no more than 20 minutes 80 ℃ of maintenances below 80 ℃.Can lose a part of protein like this, but can make product specious, produce floccule when having avoided the manufacturing oral liquid.Be to adopt the normal temperature sieving, still after the normal temperature sieving, heat suction filtration again and will see the purposes of product in the future and decide.Can with the nutrient solution that extracts after the normal temperature sieving directly decompression concentrate make the drone nutrient concentrate or concentrate after make the drone nutrient freeze-dried powder, also can make freeze-dried powder after the nutrient solution that extract behind the suction filtration concentrates or concentrates, make the drone nutrient freeze-dried powder after also the drone nutrient liquid merging of being extracted in drone nutrient liquid that extracts and the residue that is dissolved in the organic solvent can being concentrated or concentrates behind the heating suction filtration heating.
Extraction drone nutrient method provided by the present invention, equipment needed thereby is simple, leaching process economy, processing ease, can easily the nutrition in the drone body be extracted.
In view of drone nutrient contains multiple amino acid needed by human body, vitamin, protein and antibiotic etc., the primary raw material that drone nutrient concentrate that extracts with this law or drone nutrient powder freeze-dried powder can be used to do health medicine, do the made health medicine of main raw material with it, very strong tonic effect is arranged, insomnia, neurasthenia, person in poor health are had the effect that improves the health.Owing to the high nutritive value of drone nutrient self, can be used for doing the additive of high-grade nutrient food.
Describe extracting method of the present invention in detail below in conjunction with embodiment.
Embodiment A
Get freezing drone larvae and pupa in 8～23 days length of time, use tissue mashing machine's fragmentation after removing putrid and deteriorated person, claim its weight, be placed on the distilled water that adds 5 times of weight in the container, transfer solution pH value to 5.5 with citric acid again, this solution is placed under the electric mixer, stir and extracted 1.5 hours, this moment, solution was creamy white, collect filtrate and filtration residue respectively with 100 mesh sieve normal temperature filtering solutions, filtrate is heated together with the container water-bath, and connect automatic temperature control instrument, the filtrate temperature was kept 15 minutes at 80 ℃, connect vavuum pump then, take advantage of hot suction filtration so that two-layer middling speed filter is low, used filtrate low temperature is placed a night, next day, suction filtration was once collected filtrate again.95% the ethanol that the filtration residue of above collection is added 4 times of its weight, adding proper amount of edible soda transfers solution value to 7 to stir extraction 1.5 hours, filter, waste, filtrate is left standstill, refilter next day and the filtrate of above twice collection is integrated with decompression concentrates in the vacuum concentration pan. freezing then, make the drone nutrient freeze-dried powder.
Embodiment B
With fresh drone and drone larvae half and half, sending into strand presses in the device broken, in the water and alcohol mixeding liquid (water and ethanol are by weight half and half) that the drone and the larva of fragmentation is incorporated as 7 times of amounts of own wt, add an amount of sodium chloride solution again, and, stir and extracted two hours with citric acid accent pH value to 5.8.Leave standstill after 45 minutes and filter with 100 order nylon mesh, filter with double gauze again, collect filtrate and filter residue, the water-soluble again mixed liquor with ethanol of filter residue, its amount stirs and extracted 1 hour for 4 times of filter residue weight, leaves standstill and filters with double gauze after 20 minutes, collect this filtrate, twice filtrate merging sent into be condensed into the drone nutrient concentrate in the vacuum concentration pan.
Claims (4)
1, a kind of extracting method of drone nutrient is characterized in that normotrophic, fresh or freezing drone, drone larvae and drone pupae, one of them, two or all, warp
(a) fragmentation, then,
(b) add in the solvent, transferring the pH value of this solution with acid again is 4～6;
(c) stir extraction, filtration;
(d) residue that will filter is dissolved in the mixed liquor of organic solution and water, adds to use alkaline matter, transfers solution pH value to 7, repeats (c);
(e) will through (c) (d) the drone nutrient liquid that extracts of technology respectively or merge and reduce pressure concentratedly or after concentrating, make freeze-dried powder.
2, method according to claim 1 is characterized in that
(f) be the aqueous solution of water, salt or the mixed liquor of water and organic solvent at solvent described in (b), quantity of solvent is 1.5～8 times of molten broken drone weight, and institute's water is distilled water or water, and used organic solvent is an ethanol, and the weight of ethanol and water is 1: 1;
(g) used filtering technique is normal temperature sieving or normal temperature sieving and heating two steps of suction filtration in the method;
(h) in (d) technology used organic solvent or organic solvent and water mix liquid measure 1～6 times by molten filtration residue weight, used organic solvent is an ethanol, the weight ratio of ethanol and water is 1: 1;
3, the drone nutrient that extracts with said method is used as the primary raw material of health medicine.
4, the drone nutrient that extracts with said method is used as the additive of nutraceutical.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN88106581A CN1028200C (en) | 1988-09-07 | 1988-09-07 | Extraction process and application of drone nutrient |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN88106581A CN1028200C (en) | 1988-09-07 | 1988-09-07 | Extraction process and application of drone nutrient |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1040910A true CN1040910A (en) | 1990-04-04 |
| CN1028200C CN1028200C (en) | 1995-04-19 |
Family
ID=4834299
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN88106581A Expired - Fee Related CN1028200C (en) | 1988-09-07 | 1988-09-07 | Extraction process and application of drone nutrient |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1028200C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102791149A (en) * | 2009-03-13 | 2012-11-21 | 帕拉法姆有限责任公司 | Biologically active food supplement |
| CN103005466A (en) * | 2012-12-31 | 2013-04-03 | 浙江省中医药研究院 | Application for drone pupae polypeptide extract |
| CN103153319A (en) * | 2011-05-31 | 2013-06-12 | "Parafarm"有限责任公司 | Method for filling cavity formations in metaphyseal (trabecular) bone sections with calcium and for preventing secretion of calcium therefrom. |
-
1988
- 1988-09-07 CN CN88106581A patent/CN1028200C/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102791149A (en) * | 2009-03-13 | 2012-11-21 | 帕拉法姆有限责任公司 | Biologically active food supplement |
| CN103153319A (en) * | 2011-05-31 | 2013-06-12 | "Parafarm"有限责任公司 | Method for filling cavity formations in metaphyseal (trabecular) bone sections with calcium and for preventing secretion of calcium therefrom. |
| CN103005466A (en) * | 2012-12-31 | 2013-04-03 | 浙江省中医药研究院 | Application for drone pupae polypeptide extract |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1028200C (en) | 1995-04-19 |
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