CN104087491A - Bee collected rape pollen wine and preparation methods thereof - Google Patents

Bee collected rape pollen wine and preparation methods thereof Download PDF

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Publication number
CN104087491A
CN104087491A CN201410338116.6A CN201410338116A CN104087491A CN 104087491 A CN104087491 A CN 104087491A CN 201410338116 A CN201410338116 A CN 201410338116A CN 104087491 A CN104087491 A CN 104087491A
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solid
pollen
lixiviate
brassica campestris
wine
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冯瑛
王永宁
石玉平
张世满
赵生元
马昌
韩海洪
郭珍
刘春缨
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Qinghai Normal University
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Qinghai Normal University
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Abstract

The invention belongs to the technical field of deep research and processing of bee collected rape pollen wine and particularly relates to bee collected rape pollen wine which is researched and prepared by taking a raw material bee collected rape pollen and preparation methods of the wine. The bee collected rape pollen wine is prepared by three preparation methods. The technological process of the preparation method I adopts a process of breaking wall of the raw material; the preparation method II is direct extraction of the raw material; the preparation method III adopts a process of solid-liquid separation to obtain an extract. The bee collected rape pollen wine has the advantages that the bee collected rape pollen wine not only has the functions of common wine and is good in taste, but also has various health functions of the bee collected rape pollen; the bee collected rape pollen wine contains the effective components such as flavone, amino acids, proteins, polysaccharides, microelements and the like, so that the bee collected rape pollen wine has the effects of enhancing the immune function of a human body, resisting radiation, promoting health of cardio and cerebral vessels of the human body, enhancing the physical power and preventing fatigue, preventing myocardial anoxia, beautifying and delaying senescence and the like; as no additives are added in production, the product has the characteristics of no pollution and nature.

Description

Brassica campestris L pollen wine and preparation method thereof
one, technical field:the invention belongs to the technical field of the Depth Study processing of Brassica campestris L pollen, particularly a kind ofly take Brassica campestris L pollen wine that Brassica campestris L pollen develops as raw material and preparation method thereof.
two, background technology:
Rape plant is in all generally plantations of wide geographic area of China, especially North China of China, northwest, Sichuan, the area such as Qinghai and Tibet is plantation in a large number especially, rape plant can produce a large amount of Pollen Brassicae campestriss in plantation, Pollen Brassicae campestris gathers through the honeybee of cultivation, while gathering pollen, add that the roughings such as the special glandular secretion thing of honeybee oneself and nectar become pollinarium, the pollen basket that it is put into back leg is taken back honeycomb and is stored and obtain, the Pollen Brassicae campestris being gathered by honeybee is exactly the Brassica campestris L pollen that we say usually, Brassica campestris L pollen is the male sex-cell of flowering plant, undertaking the task of plant genetic, have the required complete nutrients matter of development of plants, it is the source of plant life, also be the grain of a kind of young honeybee.It is very abundant that pollen includes nutritive substance, in pollen, protein, unsaturated fatty acids, Flavonoid substances, nucleic acid material, organized enzyme, micro-equal size are all very high, therefore it has the good reputation of " miniature nutrition library ", and become the fine work of full nutrition type.Therefore Brassica campestris L pollen is compared with other any foods, contains more a high proportion of needed by human nutritive ingredient in Brassica campestris L pollen.In Brassica campestris L pollen, just contain 8 kinds of essential amino acids: as Threonine, tryptophane, Methionin, α-amino-isovaleric acid, methionine(Met), phenylalanine, leucine, Isoleucine etc.Amino acid is the raw material of various enzymes, antibody and some hormone in synthetic protein, constituting body, and amino acid can maintain nitrogen equilibrium and regulate physiological function, promotes biology growing to grow, and supplements metabolic exhaustion energy.In Brassica campestris L pollen, also contain a large amount of flavonoid compounds, it can effectively prevent and treat cardio-cerebrovascular diseases, it has very important physiologically active and medicinal, health-care effect, so be widely used in treating constipation, ulcer, coronary heart disease, atherosclerosis, varix, reduction cholesterol level, the disease such as anticancer.In Brassica campestris L pollen, also contain abundant polysaccharide, polysaccharide is the biomacromolecule that a class has important physiological function, can improve quantity and the function of body T lymphocyte and scavenger cell, improve human serum immunoglobulin IgG level, there is the effect of reducing blood-fat, antiviral, antitumor, anticoagulation and thrombus, enhancing body immunity.In addition it also contains the trace element of 14 kinds of needed by human, as iron (Fe), copper (Cu), zinc (Zn), chromium (Cr), cobalt (Co), fluorine (F), manganese (Mn), iodine (I), vanadium (V), nickel (Ni), molybdenum (Mo), selenium (Se), strontium (Sr) and tin (Sn) etc.Also contain vitamin V E, VC, VB simultaneously 6with various enzymes.The nutritive substance that contains a large amount of human body needs due to Brassica campestris L pollen, people are also more and more deep to its research at present, having had many employing Brassica campestris L pollens is that various healthcare products and the food that raw material is made occurs, but the alcohol product that the Brassica campestris L pollen of also not take is made as raw material occurs, alcohol product is the mankind's conventional product, therefore researching and developing out and take the alcohol product that Brassica campestris L pollen makes as raw material, is to take Brassica campestris L pollen one of unsolved technical barrier also at present in raw material is furtherd investigate.
three, summary of the invention:
The object of the invention is for existing alcohol product above shortcomings, and research and design is a kind of, take Brassica campestris L pollen wine that Brassica campestris L pollen makes as main raw material and preparation method thereof, the advantage of this Brassica campestris L pollen wine and preparation method thereof is: Brassica campestris L pollen wine not only has the function of common wine, mouthfeel is good, there is unique color and luster, but also there is the plurality of health care functions of Brassica campestris L pollen, because the present invention has also adopted Brassica campestris L pollen broken wall treatment, make the effective constituent of Brassica campestris L pollen obtain more effectively utilizing, this Brassica campestris L pollen wine contains flavones, amino acid, the effective constituents such as protein and polysaccharide and trace element, make it have the immunologic function that strengthens human body, radioprotective, contribute to people body-centered, cerebrovascular health care, physical strength reinforcing and antifatigue, anti-myocardial anoxia, beauty treatment and the texts that delays senility, in process of production, do not add any additive, this product is had pollution-free, natural feature, the raw material sources of its preparation method are extensive, easily purchase and be easy to get, low price, production technique is simple, stable, easily control, its economic and social benefit is very remarkable.
Technical scheme is: Brassica campestris L pollen wine is to be prepared from by following three kinds of preparation methods, and its preparation method one is: (one). technical process is: impurity removing, raw material broken wall, solid-liquid separation, solid extracts active ingredients, solid-liquid separation, blend modulation, test package obtains product; (2). processing condition are: raw material broken wall is Brassica campestris L pollen to be carried out to the technique of broken wall, and wall-breaking method adopts catalysis broken wall (patent applied for,, number of patent application is 201310727729.4), and the raw material after broken wall enters solid-liquid separation process again; Solid extracts active ingredients adopts white wine or edible ethanol to carry out lixiviate, solid-liquid mass ratio is 1:5-30, lixiviate can be carried out at ambient temperature, extraction time is 48-200 hour, effective constituent in the Brassica campestris L pollen of extraction broken wall, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid can carry out second and third lixiviate, the vat liquor that repeatedly obtains is merged or blends separately modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Then work in-process tested, pack and be qualified product.Remaining solid after lixiviate can be used as filler, foodstuff additive, cosmetics additive of medicine etc.
Preparation method two is: (one). technical process is: impurity removing, material effective component directly extraction, solid-liquid separation, blend modulation, test package obtains product, (2). processing condition are: it is to adopt white wine or edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component directly extracts, solid-liquid mass ratio is 1:5-30, lixiviate is carried out at ambient temperature, extraction time is 48-200 hour, extract effective constituent in Brassica campestris L pollen, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid can carry out second, three times or extracted many times, the vat liquor that repeatedly obtains is merged or blend separately modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.Remaining solid after lixiviate can be used as the uses such as the filler, foodstuff additive, cosmetics additive of medicine.
Preparation method three is: (one). technical process is: impurity removing, material effective component extract, solid-liquid separation obtains medicinal extract, blends modulation, test package obtains product, (2). processing condition are: it is to adopt white wine or edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component extracts, solid-liquid mass ratio is 1:5-30, lixiviate is carried out at ambient temperature, extraction time is 48-200 hour, extract effective constituent in Brassica campestris L pollen, after lixiviate, first carry out solid-liquid separation, solid after lixiviate can carry out second, three times or extracted many times, gained liquid obtains medicinal extract through rotary evaporation, medicinal extract is for containing Brassica campestris L pollen effective constituent, the medicinal extract that repeatedly obtains is merged or blend separately modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.Remaining solid after lixiviate can be used as the uses such as the filler, foodstuff additive, cosmetics additive of medicine.
Advantage of the present invention is: Brassica campestris L pollen wine not only has the function of common wine, mouthfeel is good, but also there is the plurality of health care functions of Brassica campestris L pollen, because the present invention has also adopted Brassica campestris L pollen broken wall treatment, make the effective constituent of Brassica campestris L pollen obtain more effectively utilizing, this Brassica campestris L pollen wine contains flavones, amino acid, the effective constituents such as protein and polysaccharide and trace element, make it have the immunologic function that strengthens human body, radioprotective, contribute to people body-centered, cerebrovascular health care, physical strength reinforcing and antifatigue, anti-myocardial anoxia, beauty treatment and the texts that delays senility, in process of production, do not add any additive, this product is had pollution-free, natural feature, the raw material sources of its preparation method are extensive, easily purchase and be easy to get, low price, production technique is simple, stable, easily control, its economic and social benefit is very remarkable.
four, embodiment:
Embodiment 1: Brassica campestris L pollen wine, is made by the method for being prepared as follows: (one). technical process is: impurity removing, raw material broken wall, solid-liquid separation, solid extracts active ingredients, solid-liquid separation, blend modulation, test package obtains product, (2). processing condition are: raw material broken wall is Brassica campestris L pollen to be carried out to the technique of broken wall, and wall-breaking method adopts catalysis broken wall (patent applied for, number of patent application is 201310727729.4), and the raw material after broken wall enters solid-liquid separation process again, solid extracts active ingredients adopts white wine to carry out lixiviate, solid-liquid mass ratio is that 1:5(broken pollen quality is by propollen quality), lixiviate is carried out at ambient temperature, extraction time is 48 hours, effective constituent in the Brassica campestris L pollen of extraction broken wall, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, solid after solid-liquid separation carries out second again, three solid extracts active ingredients, still adopt white wine to carry out lixiviate, lixiviate is carried out at ambient temperature, extraction time is 100 hours, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, the vat liquor repeatedly obtaining is merged and blends modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, then work in-process tested, pack and be qualified product.Remaining solid after lixiviate can be used as the filler of medicine.
Embodiment 2: Brassica campestris L pollen wine is made by the method for being prepared as follows: (one). technical process is: impurity removing, raw material broken wall, solid-liquid separation, solid extracts active ingredients, solid-liquid separation, blend modulation, test package obtains product; (2). processing condition are: raw material broken wall is Brassica campestris L pollen to be carried out to the technique of broken wall, and wall-breaking method adopts catalysis broken wall (patent applied for, number of patent application is 201310727729.4), and the raw material after broken wall enters solid-liquid separation process again; Solid extracts active ingredients adopts edible ethanol to carry out lixiviate, solid-liquid mass ratio is that 1:30(broken pollen quality is by propollen quality), lixiviate is carried out at ambient temperature, extraction time is 200 hours, effective constituent in the Brassica campestris L pollen of extraction broken wall, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid carries out lixiviate for the second time again, the vat liquor obtaining for twice is blent separately to modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Then work in-process tested, pack and be qualified product.Remaining solid after lixiviate can be used as foodstuff additive.
Embodiment 3: Brassica campestris L pollen wine is to be made by the method for being prepared as follows: (one). technical process is: impurity removing, material effective component directly extraction, solid-liquid separation, blend modulation, test package obtains product; (2). processing condition are: it is to adopt white wine to carry out lixiviate Brassica campestris L pollen that material effective component directly extracts, solid-liquid mass ratio is 1:5, lixiviate is carried out at ambient temperature, extraction time is 72 hours, extract effective constituent in Brassica campestris L pollen, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, solid after lixiviate carries out 4 lixiviates again, the vat liquor that repeatedly obtains is merged and blends modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Finally work in-process tested, pack and be qualified product.Remaining solid after lixiviate can be used as cosmetics additive and uses.
Embodiment 4: Brassica campestris L pollen wine is made by the method for being prepared as follows: (one). technical process is: impurity removing, material effective component directly extraction, solid-liquid separation, blend modulation, test package obtains product; (2). processing condition are: it is to adopt edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component directly extracts, solid-liquid mass ratio is 1:30, lixiviate is carried out at ambient temperature, extraction time is 200 hours, extract effective constituent in Brassica campestris L pollen, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, solid after lixiviate carries out lixiviate for the second time again, the vat liquor obtaining for twice is blent separately to modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Finally work in-process tested, pack and be qualified product.The filler that remaining solid after lixiviate can be used as medicine is used.
Embodiment 5: Brassica campestris L pollen wine is made by the method for being prepared as follows: (one). and technical process is: impurity removing, material effective component extract, solid-liquid separation obtains medicinal extract, blends modulation, test package obtains product, (2). processing condition are: it is to adopt white wine to carry out lixiviate Brassica campestris L pollen that material effective component extracts, solid-liquid mass ratio is 1:30, lixiviate is carried out at ambient temperature, extraction time is 150 hours, extract effective constituent in Brassica campestris L pollen, after lixiviate, first carry out solid-liquid separation, solid after lixiviate carries out second again, three lixiviates, gained liquid obtains medicinal extract through rotary evaporation, medicinal extract is for containing Brassica campestris L pollen effective constituent, the medicinal extract repeatedly obtaining is merged and blends modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.
Embodiment 6: Brassica campestris L pollen wine is made by the method for being prepared as follows: (one). and technical process is: impurity removing, material effective component extract, solid-liquid separation obtains medicinal extract, blends modulation, test package obtains product; (2). processing condition are: it is to adopt edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component extracts, solid-liquid mass ratio is 1:5, lixiviate is carried out at ambient temperature, extraction time is 72 hours, extract effective constituent in Brassica campestris L pollen, after lixiviate, first carry out solid-liquid separation, solid after lixiviate carries out 2 lixiviates again, gained liquid obtains medicinal extract through rotary evaporation, medicinal extract is for containing Brassica campestris L pollen effective constituent, the medicinal extract repeatedly obtaining is blent separately to modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Finally work in-process tested, pack and be qualified product.

Claims (6)

1. a Brassica campestris L pollen wine, is characterized in that what it was made by the method for being prepared as follows: (one). technical process is: impurity removing, raw material broken wall, solid-liquid separation, solid extracts active ingredients, solid-liquid separation, blend modulation, test package obtains product; (2). processing condition are: raw material broken wall is Brassica campestris L pollen to be carried out to the technique of broken wall, and wall-breaking method adopts catalysis broken wall, and the raw material after broken wall enters solid-liquid separation process again; Solid extracts active ingredients adopts white wine or edible ethanol to carry out lixiviate, solid-liquid mass ratio is 1:5-30, lixiviate can be carried out at ambient temperature, extraction time is 48-200 hour, effective constituent in the Brassica campestris L pollen of extraction broken wall, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid can carry out second and third lixiviate, the vat liquor that repeatedly obtains is merged or blends separately modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Then work in-process tested, pack and be qualified product.
2. a preparation method for Brassica campestris L pollen wine, is characterized in that: (one). technical process is: impurity removing, raw material broken wall, solid-liquid separation, solid extracts active ingredients, solid-liquid separation, blend modulation, test package obtains product; (2). processing condition are: raw material broken wall is Brassica campestris L pollen to be carried out to the technique of broken wall, and wall-breaking method adopts catalysis broken wall, and the raw material after broken wall enters solid-liquid separation process again; Solid extracts active ingredients adopts white wine or edible ethanol to carry out lixiviate, solid-liquid mass ratio is 1:5-30, lixiviate can be carried out at ambient temperature, extraction time is 48-200 hour, effective constituent in the Brassica campestris L pollen of extraction broken wall, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid can carry out second and third lixiviate, the vat liquor that repeatedly obtains is merged or blends separately modulation, obtain the work in-process that different wine precision, different taste are applicable to different crowd; Then work in-process tested, pack and be qualified product.
3. a Brassica campestris L pollen wine, is characterized in that what it was made by the method for being prepared as follows: (one). technical process is: impurity removing, material effective component directly extraction, solid-liquid separation, blend modulation, test package obtains product, (2). processing condition are: it is to adopt white wine or edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component directly extracts, solid-liquid mass ratio is 1:5-30, lixiviate is carried out at ambient temperature, extraction time is 48-200 hour, extract effective constituent in Brassica campestris L pollen, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid can carry out second, three times or extracted many times, the vat liquor that repeatedly obtains is merged or blend separately modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.
4. a preparation method for Brassica campestris L pollen wine, is characterized in that: (one). technical process is: impurity removing, material effective component directly extraction, solid-liquid separation, blend modulation, test package obtains product, (2). processing condition are: it is to adopt white wine or edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component directly extracts, solid-liquid mass ratio is 1:5-30, lixiviate is carried out at ambient temperature, extraction time is 48-200 hour, extract effective constituent in Brassica campestris L pollen, after lixiviate, carry out solid-liquid separation, liquid is the vat liquor that contains Brassica campestris L pollen effective constituent, its solid can carry out second, three times or extracted many times, the vat liquor that repeatedly obtains is merged or blend separately modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.
5. a Brassica campestris L pollen wine, is characterized in that what it was made by the method for being prepared as follows: (one). technical process is: impurity removing, material effective component extract, solid-liquid separation obtains medicinal extract, blends modulation, test package obtains product, (2). processing condition are: it is to adopt white wine or edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component extracts, solid-liquid mass ratio is 1:5-30, lixiviate is carried out at ambient temperature, extraction time is 48-200 hour, extract effective constituent in Brassica campestris L pollen, after lixiviate, first carry out solid-liquid separation, solid after lixiviate can carry out second, three times or extracted many times, gained liquid obtains medicinal extract through rotary evaporation, medicinal extract is for containing Brassica campestris L pollen effective constituent, the medicinal extract that repeatedly obtains is merged or blend separately modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.
6. a preparation method for Brassica campestris L pollen wine, is characterized in that: (one). technical process is: impurity removing, material effective component extract, solid-liquid separation obtains medicinal extract, blends modulation, test package obtains product, (2). processing condition are: it is to adopt white wine or edible ethanol to carry out lixiviate Brassica campestris L pollen that material effective component extracts, solid-liquid mass ratio is 1:5-30, lixiviate is carried out at ambient temperature, extraction time is 48-200 hour, extract effective constituent in Brassica campestris L pollen, after lixiviate, first carry out solid-liquid separation, solid after lixiviate can carry out second, three times or extracted many times, gained liquid obtains medicinal extract through rotary evaporation, medicinal extract is for containing Brassica campestris L pollen effective constituent, the medicinal extract that repeatedly obtains is merged or blend separately modulation, obtain different wine precision, different taste is applicable to the work in-process of different crowd, finally work in-process tested, pack and be qualified product.
CN201410338116.6A 2014-07-16 2014-07-16 Bee collected rape pollen wine and preparation methods thereof Pending CN104087491A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105886289A (en) * 2016-06-17 2016-08-24 湖北赛纯生物技术有限公司 Pollen wine and method for preparing same
CN111454811A (en) * 2020-05-22 2020-07-28 米云峰 Wall-broken bee pollen honey wine and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101683130A (en) * 2008-09-28 2010-03-31 王平 Pine pollen wine and preparation method thereof
CN102389069A (en) * 2011-11-14 2012-03-28 西华大学 Bee pollen cell-wall breaking method, bee pollen oral solution and its preparation method
CN102671420A (en) * 2012-05-17 2012-09-19 杭州天厨蜜源保健品有限公司 Pollen extract production technology
CN102871015A (en) * 2012-09-03 2013-01-16 何德枫 Pollen health care product and preparation method of pollen health care product
CN103689309A (en) * 2013-12-26 2014-04-02 青海师范大学 Method for breaking wall of rape bee-pollen through catalysis

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101683130A (en) * 2008-09-28 2010-03-31 王平 Pine pollen wine and preparation method thereof
CN102389069A (en) * 2011-11-14 2012-03-28 西华大学 Bee pollen cell-wall breaking method, bee pollen oral solution and its preparation method
CN102671420A (en) * 2012-05-17 2012-09-19 杭州天厨蜜源保健品有限公司 Pollen extract production technology
CN102871015A (en) * 2012-09-03 2013-01-16 何德枫 Pollen health care product and preparation method of pollen health care product
CN103689309A (en) * 2013-12-26 2014-04-02 青海师范大学 Method for breaking wall of rape bee-pollen through catalysis

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105886289A (en) * 2016-06-17 2016-08-24 湖北赛纯生物技术有限公司 Pollen wine and method for preparing same
CN105886289B (en) * 2016-06-17 2018-12-28 湖北赛纯生物技术有限公司 Pollen liquor and preparation method thereof
CN111454811A (en) * 2020-05-22 2020-07-28 米云峰 Wall-broken bee pollen honey wine and preparation method thereof

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Application publication date: 20141008