CN104059520B - A kind of for antiseptic wash processing aluminium sheet and preparation method thereof - Google Patents
A kind of for antiseptic wash processing aluminium sheet and preparation method thereof Download PDFInfo
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- CN104059520B CN104059520B CN201410290011.8A CN201410290011A CN104059520B CN 104059520 B CN104059520 B CN 104059520B CN 201410290011 A CN201410290011 A CN 201410290011A CN 104059520 B CN104059520 B CN 104059520B
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- parts
- aluminium sheet
- rotating speed
- preparation
- processing aluminium
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- 239000004411 aluminium Substances 0.000 title claims abstract description 29
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 29
- 230000002421 anti-septic effect Effects 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims abstract description 26
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims abstract description 24
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 13
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 13
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000004952 Polyamide Substances 0.000 claims abstract description 13
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002956 ash Substances 0.000 claims abstract description 13
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 13
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 13
- 239000003822 epoxy resin Substances 0.000 claims abstract description 13
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 13
- 229910000077 silane Inorganic materials 0.000 claims abstract description 13
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 13
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 13
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 13
- 239000010902 straw Substances 0.000 claims abstract description 13
- 229960000892 attapulgite Drugs 0.000 claims abstract description 12
- 229910052625 palygorskite Inorganic materials 0.000 claims abstract description 12
- 239000012188 paraffin wax Substances 0.000 claims abstract description 12
- 229920002647 polyamide Polymers 0.000 claims abstract description 12
- 229910000027 potassium carbonate Inorganic materials 0.000 claims abstract description 12
- 239000010455 vermiculite Substances 0.000 claims abstract description 11
- 229910052902 vermiculite Inorganic materials 0.000 claims abstract description 11
- 235000019354 vermiculite Nutrition 0.000 claims abstract description 11
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims abstract description 10
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims description 15
- 239000006185 dispersion Substances 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims 2
- 239000004575 stone Substances 0.000 claims 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 6
- 239000000853 adhesive Substances 0.000 abstract description 4
- 230000001070 adhesive effect Effects 0.000 abstract description 4
- 238000000280 densification Methods 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- 150000003839 salts Chemical class 0.000 abstract description 2
- 239000007921 spray Substances 0.000 abstract description 2
- 230000032683 aging Effects 0.000 abstract 1
- 239000003755 preservative agent Substances 0.000 description 6
- 230000002335 preservative effect Effects 0.000 description 6
- 241000218195 Lauraceae Species 0.000 description 3
- 235000017858 Laurus nobilis Nutrition 0.000 description 3
- 235000005212 Terminalia tomentosa Nutrition 0.000 description 3
- 239000003818 cinder Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- AYOHIQLKSOJJQH-UHFFFAOYSA-N dibutyltin Chemical compound CCCC[Sn]CCCC AYOHIQLKSOJJQH-UHFFFAOYSA-N 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- LUZSPGQEISANPO-UHFFFAOYSA-N butyltin Chemical compound CCCC[Sn] LUZSPGQEISANPO-UHFFFAOYSA-N 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of for antiseptic wash processing aluminium sheet and preparation method thereof, be made up of the raw material of following weight portion: polyamide 30 50 parts, acrylic resin 20 30 parts, bisphenol A type epoxy resin 30 40 parts, nano-calcium carbonate 23 parts, 68 parts of straw ashes, butyl acetate 8 10 parts, sodium benzoate 8 10 parts, vermiculite power 35 parts, attapulgite 35 parts, dibutyl tin laurate 13 parts, silane coupler 13 parts, potassium carbonate 23 parts, chlorinated paraffin 23 parts.The antiseptic wash for processing aluminium sheet of the present invention; in aluminium sheet preparation process; for processing aluminium sheet; the protecting film of densification is formed at plate surface; sheet material is made to have superior antiseptic property, superpower salt spray resistance, wet-hot aging performance; adhesive force is good, fast drying, environment friendly and pollution-free, and preparation method is simple, and the surface anticorrosion that can be widely applied to aluminium sheet processes.
Description
Technical field
The present invention relates to freeze processing technique field, particularly relate to a kind of antiseptic wash for processing aluminium sheet and
Its preparation method.
Background technology
Aluminium sheet is widely used in the industry such as refrigeration system of refrigerator liner, solar water heater water tank reflector.Aluminium sheet
After casting completes, need its surface is carried out preservative treatment, in refrigeration processing technique field, preventing of aluminium sheet
Rotten process, is important procedure of processing, directly affects the quality of aluminium sheet.At preservative in currently available technology
Reason, universal existence can unstable, adhesive force is low, easy to fall off, waterproof, rustless property is low, the most friendly to environment
Good problem.
Summary of the invention
It is an object of the invention to overcome the deficiencies in the prior art, it is provided that a kind of preservative treatment for processing aluminium sheet
Liquid, has that antiseptic property is good, adhesive force is good, scrub resistance, environment friendly and pollution-free advantage.
It is a further object of the present invention to provide the preparation method of a kind of antiseptic wash for processing aluminium sheet.
The present invention adopts the following technical scheme that to achieve these goals
A kind of antiseptic wash for processing aluminium sheet, is made up of the raw material of following weight portion: polyamide
30-50 part, acrylic resin 20-30 part, bisphenol A type epoxy resin 30-40 part, nano-calcium carbonate 2-3
Part, straw ashes 6-8 part, butyl acetate 8-10 part, sodium benzoate 8-10 part, vermiculite power 3-5 part, recessed
Convex rod soil 3-5 part, dibutyl tin laurate 1-3 part, silane coupler 1-3 part, potassium carbonate 2-3 part, chlorine
Fossil waxes 2-3 part.
Preferably, the described antiseptic wash for processing aluminium sheet, it is made up of the raw material of following weight portion: poly-
Amide resin 40 parts, acrylic resin 25 parts, bisphenol A type epoxy resin 35 parts, nano-calcium carbonate 3 parts,
8 parts of straw ashes, butyl acetate 10 parts, sodium benzoate 10 parts, vermiculite power 5 parts, attapulgite 5 parts,
Dibutyl tin laurate 2 parts, silane coupler 2 parts, potassium carbonate 2 parts, chlorinated paraffin 3 parts.
The preparation method of the described antiseptic wash for processing aluminium sheet, including following preparation process:
(1) by above-mentioned weight ratio by polyamide, acrylic resin, bisphenol A type epoxy resin,
Nano-calcium carbonate, silane coupler join in dispersion machine, divide under the rotating speed that rotating speed is 1500-1600rpm
Dissipate stirring 20-30 minute；
(2) the most by weight ratio add straw ashes, vermiculite power, attapulgite, dibutyl tin laurate,
Dispersion stirring 10-15 minute under the rotating speed that rotating speed is 1200-1400rpm；
(3) last ratio by weight adds butyl acetate, sodium benzoate, potassium carbonate, chlorinated paraffin,
Rotating speed be 800-1000rpm rotating speed under stir 8-10 minute, get product.
Compared with the prior art, beneficial effects of the present invention is as follows:
The antiseptic wash for processing aluminium sheet of the present invention, in aluminium sheet preparation process, is used for processing aluminium sheet,
Form the protecting film of densification at plate surface, make sheet material have superior antiseptic property, superpower salt spray resistance, moisture-proof
Hot property, adhesive force is good, fast drying, environment friendly and pollution-free, and preparation method is simple, can be widely applied to
The surface anticorrosion of aluminium sheet processes.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1:
A kind of antiseptic wash for processing aluminium sheet, is made up of the raw material of following weight portion: polyamide
30 parts, acrylic resin 30 parts, bisphenol A type epoxy resin 30 parts, nano-calcium carbonate 3 parts, straw ash
6 parts of cinder, butyl acetate 8 parts, sodium benzoate 8 parts, vermiculite power 5 parts, attapulgite 3 parts, two Laurels two
Butyl tin 1 part, silane coupler 3 parts, potassium carbonate 2 parts, chlorinated paraffin 3 parts.
Preparation method, including following preparation process:
(1) by above-mentioned weight ratio by polyamide, acrylic resin, bisphenol A type epoxy resin,
Nano-calcium carbonate, silane coupler join in dispersion machine, dispersion stirring under the rotating speed that rotating speed is 1500rpm
30 minutes；
(2) the most by weight ratio add straw ashes, vermiculite power, attapulgite, dibutyl tin laurate,
Dispersion stirring 15 minutes under the rotating speed that rotating speed is 1200rpm；
(3) last ratio by weight adds butyl acetate, sodium benzoate, potassium carbonate, chlorinated paraffin,
Rotating speed be 1000rpm rotating speed under stir 10 minutes, get product.
Embodiment 2:
A kind of antiseptic wash for processing aluminium sheet, is made up of the raw material of following weight portion: polyamide
40 parts, acrylic resin 25 parts, bisphenol A type epoxy resin 35 parts, nano-calcium carbonate 3 parts, straw ash
8 parts of cinder, butyl acetate 10 parts, sodium benzoate 10 parts, vermiculite power 5 parts, attapulgite 5 parts, two Laurels
Dibutyl tin 2 parts, silane coupler 2 parts, potassium carbonate 2 parts, chlorinated paraffin 3 parts.
Preparation method, including following preparation process:
(1) by above-mentioned weight ratio by polyamide, acrylic resin, bisphenol A type epoxy resin,
Nano-calcium carbonate, silane coupler join in dispersion machine, dispersion stirring under the rotating speed that rotating speed is 1600rpm
30 minutes；
(2) the most by weight ratio add straw ashes, vermiculite power, attapulgite, dibutyl tin laurate,
Dispersion stirring 15 minutes under the rotating speed that rotating speed is 1400rpm；
(3) last ratio by weight adds butyl acetate, sodium benzoate, potassium carbonate, chlorinated paraffin,
Rotating speed be 1000rpm rotating speed under stir 10 minutes, get product.
Embodiment 3:
A kind of antiseptic wash for processing aluminium sheet, is made up of the raw material of following weight portion: polyamide
50 parts, acrylic resin 30 parts, bisphenol A type epoxy resin 40 parts, nano-calcium carbonate 3 parts, straw ash
8 parts of cinder, butyl acetate 10 parts, sodium benzoate 10 parts, vermiculite power 5 parts, attapulgite 3 parts, two Laurels
Dibutyl tin 3 parts, silane coupler 3 parts, potassium carbonate 3 parts, chlorinated paraffin 3 parts.
Preparation method, including following preparation process:
(1) by above-mentioned weight ratio by polyamide, acrylic resin, bisphenol A type epoxy resin,
Nano-calcium carbonate, silane coupler join in dispersion machine, dispersion stirring under the rotating speed that rotating speed is 1500rpm
30 minutes；
(2) the most by weight ratio add straw ashes, vermiculite power, attapulgite, dibutyl tin laurate,
Dispersion stirring 15 minutes under the rotating speed that rotating speed is 1400rpm；
(3) last ratio by weight adds butyl acetate, sodium benzoate, potassium carbonate, chlorinated paraffin,
Rotating speed be 1000rpm rotating speed under stir 10 minutes, get product.
Test example:
The antiseptic wash that embodiment 1, embodiment 2 and embodiment 3 preparation are used for processing aluminium sheet carries out sulfur
Acid mantoquita acidometric titration test:
Test method: add 20g cupric sulfate crystals, 20ml hydrochloric acid in volumetric flask, and dilute with deionized water
Release to 1000ml, under condition of different temperatures, drop in and prepare by embodiment 1, embodiment 2, embodiment 3
On the aluminium sheet that antiseptic wash and common preservative processed, calculate the time (min) of variable color.Result is as follows
Table:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Common preservative | |
| 10℃ | 32min | 38min | 36min | 7min |
| 20℃ | 28min | 35min | 33min | 5min |
| 30℃ | 23min | 25min | 24min | 3min |
| 10℃ | 19min | 22min | 20min | 2min |
As can be known from the above table, the antiseptic wash antiseptic effect of the present invention is substantially better than common preservative.
Claims (3)
1. the antiseptic wash being used for processing aluminium sheet, it is characterised in that: by the raw material group of following weight portion
Become: polyamide 30-50 part, acrylic resin 20-30 part, bisphenol A type epoxy resin 30-40 part,
Nano-calcium carbonate 2-3 part, straw ashes 6-8 part, butyl acetate 8-10 part, sodium benzoate 8-10 part, trematodiasis
Stone powder 3-5 part, attapulgite 3-5 part, dibutyl tin laurate 1-3 part, silane coupler 1-3 part, carbon
Acid potassium 2-3 part, chlorinated paraffin 2-3 part.
Antiseptic wash for processing aluminium sheet the most according to claim 1, it is characterised in that: by with
The raw material composition of lower weight portion: polyamide 40 parts, acrylic resin 25 parts, bisphenol A type epoxy resin
35 parts, nano-calcium carbonate 3 parts, 8 parts of straw ashes, butyl acetate 10 parts, sodium benzoate 10 parts, trematodiasis
Stone powder 5 parts, attapulgite 5 parts, dibutyl tin laurate 2 parts, silane coupler 2 parts, potassium carbonate 2
Part, chlorinated paraffin 3 parts.
3. a preparation method for the antiseptic wash for processing aluminium sheet as claimed in claim 1 or 2,
It is characterized in that: include following preparation process:
(1) by above-mentioned weight ratio by polyamide, acrylic resin, bisphenol A type epoxy resin,
Nano-calcium carbonate, silane coupler join in dispersion machine, divide under the rotating speed that rotating speed is 1500-1600rpm
Dissipate stirring 20-30 minute；
(2) the most by weight ratio add straw ashes, vermiculite power, attapulgite, dibutyl tin laurate,
Dispersion stirring 10-15 minute under the rotating speed that rotating speed is 1200-1400rpm；
(3) last ratio by weight adds butyl acetate, sodium benzoate, potassium carbonate, chlorinated paraffin,
Rotating speed be 800-1000rpm rotating speed under stir 8-10 minute, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410290011.8A CN104059520B (en) | 2014-06-20 | 2014-06-20 | A kind of for antiseptic wash processing aluminium sheet and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410290011.8A CN104059520B (en) | 2014-06-20 | 2014-06-20 | A kind of for antiseptic wash processing aluminium sheet and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104059520A CN104059520A (en) | 2014-09-24 |
| CN104059520B true CN104059520B (en) | 2016-08-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410290011.8A Expired - Fee Related CN104059520B (en) | 2014-06-20 | 2014-06-20 | A kind of for antiseptic wash processing aluminium sheet and preparation method thereof |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106189712A (en) * | 2016-08-24 | 2016-12-07 | 何国美 | Glass coating |
| CN107722822A (en) * | 2017-08-30 | 2018-02-23 | 蚌埠市好思家太阳能有限公司 | A kind of flat-plate solar collector anti-corrosion surface coating material and its preparation technology |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102352170A (en) * | 2011-09-05 | 2012-02-15 | 安徽省易达电子有限公司 | Epoxy polyester metal corrosion resistant paint and preparation method thereof |
| CN103103532A (en) * | 2012-11-13 | 2013-05-15 | 铜陵祥云消防科技有限责任公司 | Metal antirust agent containing modified nanometer calcined zeolite powder |
| CN103820035A (en) * | 2014-02-20 | 2014-05-28 | 铜陵祥云消防科技有限责任公司 | Flame retardant adhesive containing modified kaolin |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8562126B1 (en) * | 2012-03-29 | 2013-10-22 | Eastman Kodak Company | Pre-treatment composition for inkjet printing |
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2014
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102352170A (en) * | 2011-09-05 | 2012-02-15 | 安徽省易达电子有限公司 | Epoxy polyester metal corrosion resistant paint and preparation method thereof |
| CN103103532A (en) * | 2012-11-13 | 2013-05-15 | 铜陵祥云消防科技有限责任公司 | Metal antirust agent containing modified nanometer calcined zeolite powder |
| CN103820035A (en) * | 2014-02-20 | 2014-05-28 | 铜陵祥云消防科技有限责任公司 | Flame retardant adhesive containing modified kaolin |
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| Publication number | Publication date |
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| CN104059520A (en) | 2014-09-24 |
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Denomination of invention: Anti-corrosion treating fluid for treating aluminum plate and preparation method thereof Effective date of registration: 20171024 Granted publication date: 20160817 Pledgee: Merchants Bank of Hefei Economic Development Zone Branch Pledgor: Hefei Great Wall Refrigeration Technology Co., Ltd. Registration number: 2017340000307 |
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Date of cancellation: 20190116 Granted publication date: 20160817 Pledgee: Merchants Bank of Hefei Economic Development Zone Branch Pledgor: Hefei Great Wall Refrigeration Technology Co., Ltd. Registration number: 2017340000307 |
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Effective date of registration: 20190212 Address after: 230000 Tiandu Road 139, Hefei Economic and Technological Development Zone, Anhui Province Patentee after: HEFEI TAITONG REFRIGERATING TECHNOLOGY CO., LTD. Address before: 230000 Peach Blossom Industrial Zone, Hefei Economic and Technological Development Zone, Anhui Province Patentee before: Hefei Great Wall Refrigeration Technology Co., Ltd. |
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