CN104059520A - Anti-corrosion treating fluid for treating aluminum plate and preparation method thereof - Google Patents
Anti-corrosion treating fluid for treating aluminum plate and preparation method thereof Download PDFInfo
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- CN104059520A CN104059520A CN201410290011.8A CN201410290011A CN104059520A CN 104059520 A CN104059520 A CN 104059520A CN 201410290011 A CN201410290011 A CN 201410290011A CN 104059520 A CN104059520 A CN 104059520A
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- parts
- rotating speed
- aluminum plate
- corrosion
- preparation
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- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 30
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 238000005260 corrosion Methods 0.000 title abstract 6
- 239000012530 fluid Substances 0.000 title abstract 4
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims abstract description 26
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 15
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 14
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims abstract description 14
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 13
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 13
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 13
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 13
- 239000003822 epoxy resin Substances 0.000 claims abstract description 13
- 229920006122 polyamide resin Polymers 0.000 claims abstract description 13
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 13
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 13
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 13
- 239000010455 vermiculite Substances 0.000 claims abstract description 13
- 229910052902 vermiculite Inorganic materials 0.000 claims abstract description 13
- 235000019354 vermiculite Nutrition 0.000 claims abstract description 13
- 229960000892 attapulgite Drugs 0.000 claims abstract description 8
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 8
- 229910052625 palygorskite Inorganic materials 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 8
- 239000004411 aluminium Substances 0.000 claims description 23
- 230000000855 fungicidal effect Effects 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 15
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims description 12
- 239000002956 ash Substances 0.000 claims description 12
- 235000015320 potassium carbonate Nutrition 0.000 claims description 12
- -1 2 parts Substances 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 claims description 5
- 230000001681 protective effect Effects 0.000 abstract description 2
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 239000012975 dibutyltin dilaurate Substances 0.000 abstract 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 abstract 1
- 239000012188 paraffin wax Substances 0.000 abstract 1
- 229910000027 potassium carbonate Inorganic materials 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 239000010902 straw Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000002421 anti-septic effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 239000002481 rotproofing Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- SPZAGEJGELYZAM-UHFFFAOYSA-L copper sulfate hydrochloride Chemical compound Cl.[Cu+2].[O-]S([O-])(=O)=O SPZAGEJGELYZAM-UHFFFAOYSA-L 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses an anti-corrosion treating fluid for treating an aluminum plate and a preparation method thereof. The anti-corrosion treating fluid comprises the following raw materials in parts by weight: 30-50 parts of polyamide resin, 20-30 parts of acrylic resin, 30-40 parts of bisphenol A type epoxide resin, 2-3 parts of nanometer calcium carbonate, 6-8 parts of straw ash, 8-10 parts of butyl acetate, 8-10 parts of sodium benzoate, 3-5 parts of vermiculite powder, 3-5 parts of attapulgite, 1-3 parts of dibutyltin dilaurate, 1-3 parts of silane coupling agents, 2-3 parts of potassium carbonate and 2-3 parts of chlorinated paraffin. The anti-corrosion treating fluid is used for treating the aluminum plate in the preparation process of the aluminum plate, can form a compact protective film on the surface of the aluminum plate so that the aluminum plate has excellent anti-corrosion property and ultrahigh salt-fog resistant property and dampness-heat resistant property, has good adhesive force, can be dried quickly, is friendly to the environment, does not cause pollution, is prepared by a simple preparation method and can be widely applied to the anti-corrosion treatment of the surface of the aluminum plate.
Description
Technical field
The present invention relates to the processing technique field of freezing, relate in particular to a kind of fungicidal wash for the treatment of aluminium sheet and preparation method thereof.
Background technology
Aluminium sheet is widely used in the industries such as refrigerator refrigeration system liner, solar water heater water tank reflector.Aluminium sheet, after casting completes, need to carry out rotproofing to its surface, and in refrigeration processing technique field, the rotproofing of aluminium sheet, is important procedure of processing, directly affects the quality of aluminium sheet.Sanitas in currently available technology is processed, and ubiquity performance is unstable, sticking power is low, easily come off, waterproof, rustless property are low, to the disagreeableness problem of environment.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of fungicidal wash for the treatment of aluminium sheet is provided, have that antiseptic property is good, sticking power is good, scrub resistance, environment friendly and pollution-free advantage.
Another object of the present invention is to provide a kind of preparation method of the fungicidal wash for the treatment of aluminium sheet.
The present invention adopts following technical scheme to achieve these goals:
For the treatment of a fungicidal wash for aluminium sheet, by the raw material of following weight part, formed: polyamide resin 30-50 part, acrylic resin 20-30 part, bisphenol A type epoxy resin 30-40 part, nano-calcium carbonate 2-3 part, stalk ashes 6-8 part, N-BUTYL ACETATE 8-10 part, Sodium Benzoate 8-10 part, vermiculite power 3-5 part, attapulgite 3-5 part, dibutyl tin laurate 1-3 part, silane coupling agent 1-3 part, salt of wormwood 2-3 part, clorafin 2-3 part.
Preferably, the described fungicidal wash for the treatment of aluminium sheet, is comprised of the raw material of following weight part: 40 parts of polyamide resins, 25 parts of acrylic resins, 35 parts of bisphenol A type epoxy resins, 3 parts of nano-calcium carbonates, 8 parts, stalk ashes, 10 parts of N-BUTYL ACETATEs, 10 parts of Sodium Benzoates, 5 parts of vermiculite powers, 5 parts of attapulgites, 2 parts of dibutyl tin laurates, 2 parts of silane coupling agents, 2 parts, salt of wormwood, 3 parts of clorafins.
The preparation method of the described fungicidal wash for the treatment of aluminium sheet, comprises following preparation process:
(1) by above-mentioned weight ratio, polyamide resin, acrylic resin, bisphenol A type epoxy resin, nano-calcium carbonate, silane coupling agent are joined in dispersion machine, under the rotating speed that is 1500-1600rpm at rotating speed, disperse to stir 20-30 minute;
(2) ratio adds stalk ashes, vermiculite power, attapulgite, dibutyl tin laurate, disperses to stir 10-15 minute under the rotating speed that is 1200-1400rpm at rotating speed by weight again;
(3) finally ratio adds N-BUTYL ACETATE, Sodium Benzoate, salt of wormwood, clorafin by weight, under the rotating speed that is 800-1000rpm, stirs 8-10 minute at rotating speed, gets product.
Compared with the prior art, beneficial effect of the present invention is as follows:
Fungicidal wash for the treatment of aluminium sheet of the present invention; in aluminium sheet preparation process; for the treatment of aluminium sheet; at plate surface, form fine and close protective membrane; make sheet material there is superior antiseptic property, superpower salt spray resistance, wet-hot aging performance; sticking power is good, fast drying, environment friendly and pollution-free, and preparation method is simple, and the surface anticorrosion that can be widely used in aluminium sheet is processed.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1:
For the treatment of a fungicidal wash for aluminium sheet, by the raw material of following weight part, formed: 30 parts of polyamide resins, 30 parts of acrylic resins, 30 parts of bisphenol A type epoxy resins, 3 parts of nano-calcium carbonates, 6 parts, stalk ashes, 8 parts of N-BUTYL ACETATEs, 8 parts of Sodium Benzoates, 5 parts of vermiculite powers, 3 parts of attapulgites, 1 part of dibutyl tin laurate, 3 parts of silane coupling agents, 2 parts, salt of wormwood, 3 parts of clorafins.
Preparation method, comprises following preparation process:
(1) by above-mentioned weight ratio, polyamide resin, acrylic resin, bisphenol A type epoxy resin, nano-calcium carbonate, silane coupling agent are joined in dispersion machine, under the rotating speed that is 1500rpm at rotating speed, disperse to stir 30 minutes;
(2) ratio adds stalk ashes, vermiculite power, attapulgite, dibutyl tin laurate, disperses to stir 15 minutes under the rotating speed that is 1200rpm at rotating speed by weight again;
(3) finally ratio adds N-BUTYL ACETATE, Sodium Benzoate, salt of wormwood, clorafin by weight, stirs 10 minutes at rotating speed under the rotating speed that is 1000rpm, gets product.
Embodiment 2:
For the treatment of a fungicidal wash for aluminium sheet, by the raw material of following weight part, formed: 40 parts of polyamide resins, 25 parts of acrylic resins, 35 parts of bisphenol A type epoxy resins, 3 parts of nano-calcium carbonates, 8 parts, stalk ashes, 10 parts of N-BUTYL ACETATEs, 10 parts of Sodium Benzoates, 5 parts of vermiculite powers, 5 parts of attapulgites, 2 parts of dibutyl tin laurates, 2 parts of silane coupling agents, 2 parts, salt of wormwood, 3 parts of clorafins.
Preparation method, comprises following preparation process:
(1) by above-mentioned weight ratio, polyamide resin, acrylic resin, bisphenol A type epoxy resin, nano-calcium carbonate, silane coupling agent are joined in dispersion machine, under the rotating speed that is 1600rpm at rotating speed, disperse to stir 30 minutes;
(2) ratio adds stalk ashes, vermiculite power, attapulgite, dibutyl tin laurate, disperses to stir 15 minutes under the rotating speed that is 1400rpm at rotating speed by weight again;
(3) finally ratio adds N-BUTYL ACETATE, Sodium Benzoate, salt of wormwood, clorafin by weight, stirs 10 minutes at rotating speed under the rotating speed that is 1000rpm, gets product.
Embodiment 3:
For the treatment of a fungicidal wash for aluminium sheet, by the raw material of following weight part, formed: 50 parts of polyamide resins, 30 parts of acrylic resins, 40 parts of bisphenol A type epoxy resins, 3 parts of nano-calcium carbonates, 8 parts, stalk ashes, 10 parts of N-BUTYL ACETATEs, 10 parts of Sodium Benzoates, 5 parts of vermiculite powers, 3 parts of attapulgites, 3 parts of dibutyl tin laurates, 3 parts of silane coupling agents, 3 parts, salt of wormwood, 3 parts of clorafins.
Preparation method, comprises following preparation process:
(1) by above-mentioned weight ratio, polyamide resin, acrylic resin, bisphenol A type epoxy resin, nano-calcium carbonate, silane coupling agent are joined in dispersion machine, under the rotating speed that is 1500rpm at rotating speed, disperse to stir 30 minutes;
(2) ratio adds stalk ashes, vermiculite power, attapulgite, dibutyl tin laurate, disperses to stir 15 minutes under the rotating speed that is 1400rpm at rotating speed by weight again;
(3) finally ratio adds N-BUTYL ACETATE, Sodium Benzoate, salt of wormwood, clorafin by weight, stirs 10 minutes at rotating speed under the rotating speed that is 1000rpm, gets product.
Test example:
The fungicidal wash for the treatment of aluminium sheet to embodiment 1, embodiment 2 and embodiment 3 preparations carries out copper sulfate hydrochloric acid burette test:
Test method: add 20g cupric sulfate crystals, 20ml hydrochloric acid in volumetric flask, and be diluted to 1000ml with deionized water, under condition of different temperatures, drop on the aluminium sheet of processing with fungicidal wash and the common sanitas of embodiment 1, embodiment 2, embodiment 3 preparations the time (min) of calculating variable color.Result is as following table:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Common sanitas | |
| 10℃ | 32min | 38min | 36min | 7min |
| 20℃ | 28min | 35min | 33min | 5min |
| 30℃ | 23min | 25min | 24min | 3min |
| 10℃ | 19min | 22min | 20min | 2min |
As can be known from the above table, fungicidal wash preservative effect of the present invention is obviously better than common sanitas.
Claims (3)
1. for the treatment of a fungicidal wash for aluminium sheet, it is characterized in that: the raw material by following weight part forms: polyamide resin 30-50 part, acrylic resin 20-30 part, bisphenol A type epoxy resin 30-40 part, nano-calcium carbonate 2-3 part, stalk ashes 6-8 part, N-BUTYL ACETATE 8-10 part, Sodium Benzoate 8-10 part, vermiculite power 3-5 part, attapulgite 3-5 part, dibutyl tin laurate 1-3 part, silane coupling agent 1-3 part, salt of wormwood 2-3 part, clorafin 2-3 part.
2. the fungicidal wash for the treatment of aluminium sheet according to claim 1, is characterized in that: the raw material by following weight part forms: 40 parts of polyamide resins, 25 parts of acrylic resins, 35 parts of bisphenol A type epoxy resins, 3 parts of nano-calcium carbonates, 8 parts, stalk ashes, 10 parts of N-BUTYL ACETATEs, 10 parts of Sodium Benzoates, 5 parts of vermiculite powers, 5 parts of attapulgites, 2 parts of dibutyl tin laurates, 2 parts of silane coupling agents, 2 parts, salt of wormwood, 3 parts of clorafins.
3. a preparation method for the fungicidal wash for the treatment of aluminium sheet as claimed in claim 1 or 2, is characterized in that: comprise following preparation process:
(1) by above-mentioned weight ratio, polyamide resin, acrylic resin, bisphenol A type epoxy resin, nano-calcium carbonate, silane coupling agent are joined in dispersion machine, under the rotating speed that is 1500-1600rpm at rotating speed, disperse to stir 20-30 minute;
(2) ratio adds stalk ashes, vermiculite power, attapulgite, dibutyl tin laurate, disperses to stir 10-15 minute under the rotating speed that is 1200-1400rpm at rotating speed by weight again;
(3) finally ratio adds N-BUTYL ACETATE, Sodium Benzoate, salt of wormwood, clorafin by weight, under the rotating speed that is 800-1000rpm, stirs 8-10 minute at rotating speed, gets product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410290011.8A CN104059520B (en) | 2014-06-20 | 2014-06-20 | A kind of for antiseptic wash processing aluminium sheet and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410290011.8A CN104059520B (en) | 2014-06-20 | 2014-06-20 | A kind of for antiseptic wash processing aluminium sheet and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104059520A true CN104059520A (en) | 2014-09-24 |
| CN104059520B CN104059520B (en) | 2016-08-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410290011.8A Expired - Fee Related CN104059520B (en) | 2014-06-20 | 2014-06-20 | A kind of for antiseptic wash processing aluminium sheet and preparation method thereof |
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| Country | Link |
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| CN (1) | CN104059520B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106189712A (en) * | 2016-08-24 | 2016-12-07 | 何国美 | Glass coating |
| CN107722822A (en) * | 2017-08-30 | 2018-02-23 | 蚌埠市好思家太阳能有限公司 | A kind of flat-plate solar collector anti-corrosion surface coating material and its preparation technology |
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|---|---|---|---|---|
| CN102352170A (en) * | 2011-09-05 | 2012-02-15 | 安徽省易达电子有限公司 | Epoxy polyester metal corrosion resistant paint and preparation method thereof |
| CN103103532A (en) * | 2012-11-13 | 2013-05-15 | 铜陵祥云消防科技有限责任公司 | Metal antirust agent containing modified nanometer calcined zeolite powder |
| US20130257988A1 (en) * | 2012-03-29 | 2013-10-03 | Yang Xiang | Pre-treatment composition for inkjet printing |
| CN103820035A (en) * | 2014-02-20 | 2014-05-28 | 铜陵祥云消防科技有限责任公司 | Flame retardant adhesive containing modified kaolin |
-
2014
- 2014-06-20 CN CN201410290011.8A patent/CN104059520B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102352170A (en) * | 2011-09-05 | 2012-02-15 | 安徽省易达电子有限公司 | Epoxy polyester metal corrosion resistant paint and preparation method thereof |
| US20130257988A1 (en) * | 2012-03-29 | 2013-10-03 | Yang Xiang | Pre-treatment composition for inkjet printing |
| CN103103532A (en) * | 2012-11-13 | 2013-05-15 | 铜陵祥云消防科技有限责任公司 | Metal antirust agent containing modified nanometer calcined zeolite powder |
| CN103820035A (en) * | 2014-02-20 | 2014-05-28 | 铜陵祥云消防科技有限责任公司 | Flame retardant adhesive containing modified kaolin |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106189712A (en) * | 2016-08-24 | 2016-12-07 | 何国美 | Glass coating |
| CN107722822A (en) * | 2017-08-30 | 2018-02-23 | 蚌埠市好思家太阳能有限公司 | A kind of flat-plate solar collector anti-corrosion surface coating material and its preparation technology |
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| Publication number | Publication date |
|---|---|
| CN104059520B (en) | 2016-08-17 |
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Denomination of invention: Anti-corrosion treating fluid for treating aluminum plate and preparation method thereof Effective date of registration: 20171024 Granted publication date: 20160817 Pledgee: Merchants Bank of Hefei Economic Development Zone Branch Pledgor: Hefei Great Wall Refrigeration Technology Co., Ltd. Registration number: 2017340000307 |
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Date of cancellation: 20190116 Granted publication date: 20160817 Pledgee: Merchants Bank of Hefei Economic Development Zone Branch Pledgor: Hefei Great Wall Refrigeration Technology Co., Ltd. Registration number: 2017340000307 |
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Effective date of registration: 20190212 Address after: 230000 Tiandu Road 139, Hefei Economic and Technological Development Zone, Anhui Province Patentee after: HEFEI TAITONG REFRIGERATING TECHNOLOGY CO., LTD. Address before: 230000 Peach Blossom Industrial Zone, Hefei Economic and Technological Development Zone, Anhui Province Patentee before: Hefei Great Wall Refrigeration Technology Co., Ltd. |
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