CN104016658A - Method of preparing interior wall tile by using local wastes in Inner Mongolia and interior wall tile product prepared by same - Google Patents
Method of preparing interior wall tile by using local wastes in Inner Mongolia and interior wall tile product prepared by same Download PDFInfo
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- CN104016658A CN104016658A CN201410269470.8A CN201410269470A CN104016658A CN 104016658 A CN104016658 A CN 104016658A CN 201410269470 A CN201410269470 A CN 201410269470A CN 104016658 A CN104016658 A CN 104016658A
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- internal wall
- wall brick
- inner mongol
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- inner mongolia
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention relates to a method of preparing an interior wall tile by using local wastes in Inner Mongolia, wherein the blank is prepared from the following components in percentage by weight: 30-60% of Inner Mongolia Kubuqi yellow sands, 20-40% of Inner Mongolia Tarangaolei gangues, 5-20% of Hanggin #1 clay, 5-20% of Hanggin #2 clay and 5-10% of Hayehutong feldspar; the glaze is prepared from the following components in percentage by weight: 22-36% of Inner Mongolia Kubuqi yellow sands, 22-40% of Hayehutong feldspar, 5-12% of Xikuang argil, 8-15% of zirconium silicate, 8-15% of calcite, 2-4% of talc and 1-4% of zinc oxide. The interior wall tile product is obtained by biscuiting, glazing, drying and calcining the blank. The blank and the glaze provided by the invention use a lot of Inner Mongolia Tarangaolei gangues and Inner Mongolia Kubuqi yellow sands, so that the tile is wide in source and low in cost, has great significance in resource protection and resource utilization of industrial wastes, so that the tile has a wide market space.
Description
Technical field
The invention belongs to ceramic (pottery) field, be specifically related to a kind of internal wall brick product that utilizes the local waste material in the Inner Mongol to prepare the method for internal wall brick and make.
Background technology
The waste rock that coal gangue gives off in construction of coal mine, coal mining and the course of processing.China's spoil output is about 15 ~ 20% of raw coal ultimate production, accumulates and reaches 7,000,000,000 tons, takes up an area 70 km
2, and with the speed increment of 11,500,000,000 tons of annual emissions.And the comprehensive utilization of coal gangue is still less than 15%, remaining coal gangue adopts circular cone type or cheuch Dumpage type to be naturally stacked loosely in mine surrounding more.The coal gangue of storing up in a large number and discharging, is a kind of source of pollution, is again a kind of available stock, as long as rationally utilize, just can turn waste into wealth.State Economic and Trade Commission's major tasks of comprehensive utilization using the comprehensive utilization of coal gangue as china natural resources always.
The Deserts in China total area approximately 700,000 sq-kms, if be 1,280,000 sq-kms together with the Gobi desert of more than 50 ten thousand sq-kms at the interior total area, account for 13% of the national land total area.Reconstruction in Northwest Arid Region of China is the most concentrated area of Deserts in China, account for 80% of the national desert total area, and the Desertification in soil has caused soil cannot cultivate utilization.The present invention is innovating optimization and utilizes Inner Mongol scrap feed material and local raw material to prepare the formula of internal wall brick after experiment, guaranteeing under the prerequisite of performance quality, (the annual coal production amount in the Inner Mongol has approached 1,000,000,000 tons of products to have adopted the local coal gangue of Inner Mongol Hangjin Banner, follow a large amount of coal gangues) and yellow sand replace high quality raw material, both fully recycled industrial residue, yellow sand, turn waste into wealth, reduced production cost, reduced again the destruction of these waste residues to environment, pollute, greatly saved and stacked the required land area of these waste residue material, improve the mankind's living environment.Therefore the present invention has good environmental protection, social effect to waste residue material recycling.
It is main formula material that storehouse, the Inner Mongol its yellow sand of cloth is take in the present invention, is equipped with the right height of Inner Mongol tower and strangles coal gangue waste material and prepare internal wall brick with other clay classes of area and feldspar raw material.The coal gangue regional with other (as Pingxiang Jiangxi's coal gangue) compared, and tower right height in the Inner Mongol is strangled coal gangue silicon, aluminium content is low, and loss on ignition is large, up to 44wt%.And with regional clay also possess silicon, aluminium content is low, the feature that content of calcium and magnesium is high, especially calcium oxide content.Hangjin Banner periphery clay by Inner Mongolia area carries out composition analysis, finds that its CaO content is up to 6.98wt%～10.38wt%, is typical high calcium clay.Therefore utilize Inner Mongol coal gangue and its Hangjin Banner periphery clay can form in warm internal wall brick (1080～1180 ℃), by the formulation of rational temperature schedule and the rational proportion of other raw material, reach the object of relatively large use Inner Mongol coal gangue waste material.
Meanwhile, in order to coordinate the calcining system of internal wall brick, by its yellow sand of storehouse cloth and higher one of clay raw materials and the feldspar raw material of local plasticity, coordinate other traditional industry enamel frit makeing raw materials to prepare the internal wall brick opaque glaze that melt temperature and base substrate maturing temperature adapt.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of internal wall brick product that utilizes the local waste material in the Inner Mongol to prepare the method for internal wall brick and make.
For solving above technical problem, technical scheme of the present invention is: a kind of method of utilizing the local waste material in the Inner Mongol to prepare internal wall brick, take storehouse, the Inner Mongol its yellow sand of cloth, the right height of Inner Mongol tower strangles coal gangue as main raw material, other natural matter of the Inner Mongol is auxiliary material, and the weight percent of its base substrate and glaze formula consists of:
Base substrate: storehouse, the Inner Mongol its yellow sand of cloth 30～60wt%, the right height of Inner Mongol tower are strangled coal gangue 20～40wt%, No. 1 clay 5～20wt% of Hanggin, No. 2 clay 5～20wt% of Hanggin, Ha Ye lane feldspar 5～10wt%;
Glaze: storehouse, the Inner Mongol its yellow sand of cloth 22～36wt%, Ha Ye lane feldspar 22～40wt%, western ore deposit potter's clay 5～12wt%, zirconium silicate 8～15wt%, calcite 8～15wt%, talcum 2～4wt%, zinc oxide 1～4wt%;
By the weight percent of above-mentioned glaze formula, by standby after raw material mix, pulverizing, ball milling, mistake 250 mesh sieves;
By the weight percent of above-mentioned blank formulation, by raw material mix, pulverizing, dry, granulation, dry-pressing, dry after in 1020 ℃ of biscuitings, the internal wall brick goods that biscuiting obtains by biscuit glazing, drying and calcining.
Described calcining temperature is: 1080～1180 ℃, highest temperature soaking time is 10 ~ 30min.
In described biscuiting process, 600～900 ℃ of temperature ranges, by 2 ~ 5 ℃/min speed, heat up.
The water-intake rate of described base substrate is 6.0 ~ 6.5%, the modulus of rupture is 44.5 ~ 49.8Mpa.
The above-mentioned prepared internal wall brick product of internal wall brick method of preparing, is characterized in that: described internal wall brick glaze whiteness is 55.44 ~ 62.51%, glossiness is 6.45 ~ 8.03%.
In base of the present invention, glaze relatively large employing the right height of Inner Mongol tower strangle coal gangue and storehouse, the Inner Mongol its yellow sand of cloth; its wide material sources; with low cost; the internal wall brick product making has the higher modulus of rupture; compare and there is larger cost and performance advantage with like product on market; the recycling of conservation of resources and industrial waste is had to great meaning simultaneously, therefore there is the wide market space.
Embodiment
The main chemical constitution of each raw material is as following table:
Embodiment 1:
By the weight percent of following glaze formula, standby by raw material mix, pulverizing, ball milling, after sieving;
Glaze formula is: its yellow sand of storehouse cloth 31wt %, Ha Ye lane feldspar 35wt %, western ore deposit potter's clay 10wt %, zirconium silicate 10wt %, calcite 10wt %, talcum 2wt %, zinc oxide 2wt %;
By the weight percent of following blank formulation, by raw material mix, pulverizing, dry, granulation, dry-pressing, dry after in 1020 ℃ of biscuitings, and heat up by 2 ℃/min speed 600～900 ℃ of temperature ranges, the internal wall brick goods that biscuiting obtains by biscuit glazing, drying and calcining, its calcining temperature is 1080 ℃, top temperature point insulation 30 minutes;
Blank formulation is: its yellow sand of storehouse cloth 40wt %, the right height of tower are strangled coal gangue 30wt %, Ha Ye lane feldspar 10wt %, No. 1 clay 10wt % of Hanggin, No. 2 clay 10wt % of Hanggin.
Embodiment 2:
By the weight percent of following glaze formula, standby by raw material mix, pulverizing, ball milling, after sieving;
Glaze formula is: its yellow sand of storehouse cloth 22wt%, Ha Ye lane feldspar 40wt%, western ore deposit potter's clay 8wt%, zirconium silicate 10wt%, calcite 15wt%, talcum 4wt%, zinc oxide 1wt%;
By the weight percent of following blank formulation, by raw material mix, pulverizing, dry, granulation, dry-pressing, dry after in 1020 ℃ of biscuitings, and heat up by 4 ℃/min speed 600～900 ℃ of temperature ranges, the internal wall brick goods that biscuiting obtains by biscuit glazing, drying and calcining, its calcining temperature is 1110 ℃, top temperature point insulation 15 minutes;
Blank formulation is: its yellow sand of storehouse cloth 50 wt %, the right height of tower are strangled coal gangue 20wt %, Ha Ye lane feldspar 5wt %, No. 1 clay 10wt % of Hanggin, No. 2 clay 15wt % of Hanggin.
Embodiment 3:
By the weight percent of following glaze formula, standby by raw material mix, pulverizing, ball milling, after sieving;
Glaze formula is: its yellow sand of storehouse cloth 35wt %, Ha Ye lane feldspar 34wt %, western ore deposit potter's clay 8wt %, zirconium silicate 8 wt %, calcite 10wt %, talcum 3wt %, zinc oxide 2wt %;
By the weight percent of following blank formulation, by raw material mix, pulverizing, dry, granulation, dry-pressing, dry after in 1020 ℃ of biscuitings, and heat up by 4 ℃/min speed 600～900 ℃ of temperature ranges, the internal wall brick goods that biscuiting obtains by biscuit glazing, drying and calcining, its calcining temperature is 1140 ℃, top temperature point insulation 15 minutes;
Blank formulation is: its yellow sand of storehouse cloth 40wt %, the right height of tower are strangled coal gangue 30wt %, Ha Ye lane feldspar 5wt %, No. 1 clay 20wt % of Hanggin, No. 2 clay 5wt % of Hanggin.
Embodiment 4:
By the weight percent of following glaze formula, standby by raw material mix, pulverizing, ball milling, after sieving;
Glaze formula is: its yellow sand of storehouse cloth 36 wt %, Ha Ye lane feldspar 22 wt %, western ore deposit potter's clay 12wt %, zirconium silicate 14 wt %, calcite 8wt %, talcum 4wt %, zinc oxide 4wt %;
By the weight percent of following blank formulation, by raw material mix, pulverizing, dry, granulation, dry-pressing, dry after in 1020 ℃ of biscuitings, and heat up by 5 ℃/min speed 600～900 ℃ of temperature ranges, the internal wall brick goods that biscuiting obtains by biscuit glazing, drying and calcining, its calcining temperature is 1180 ℃, top temperature point insulation 10 minutes;
Blank formulation is: its yellow sand of storehouse cloth 60 wt %, the right height of tower are strangled coal gangue 20wt %, Ha Ye lane feldspar 5wt %, No. 1 clay 5wt % of Hanggin, No. 2 clay 10wt % of Hanggin.
Above-described embodiment 1-4 is carried out to water-intake rate, the modulus of rupture and testing flatness to base substrate, the whiteness of glaze and glossiness be the results are shown in to following table:
Claims (5)
1. utilize the local waste material in the Inner Mongol to prepare a method for internal wall brick, take storehouse, the Inner Mongol its yellow sand of cloth, the right height of Inner Mongol tower to strangle coal gangue as main raw material, other natural matter of the Inner Mongol is auxiliary material, and the weight percent of its base substrate and glaze formula consists of:
Base substrate: storehouse, the Inner Mongol its yellow sand of cloth 30～60wt%, the right height of Inner Mongol tower are strangled coal gangue 20～40wt%, No. 1 clay 5～20wt% of Hanggin, No. 2 clay 5～20wt% of Hanggin, Ha Ye lane feldspar 5～10wt%;
Glaze: storehouse, the Inner Mongol its yellow sand of cloth 22～36wt%, Ha Ye lane feldspar 22～40wt%, western ore deposit potter's clay 5～12wt%, zirconium silicate 8～15wt%, calcite 8～15wt%, talcum 2～4wt%, zinc oxide 1～4wt%;
By the weight percent of above-mentioned glaze formula, standby by raw material mix, pulverizing, ball milling, after sieving;
By the weight percent of above-mentioned blank formulation, by raw material mix, pulverizing, dry, granulation, dry-pressing, dry after in 1020 ℃ of biscuitings, the internal wall brick goods that biscuiting obtains by biscuit glazing, drying and calcining.
2. the method for preparing internal wall brick according to claim 1, is characterized in that: described calcining temperature is: 1080～1180 ℃, the soaking time of top temperature is 10 ~ 30min.
3. the method for preparing internal wall brick according to claim 1, is characterized in that: in described biscuiting process, 600～900 ℃ of temperature ranges, by 2 ~ 5 ℃/min speed, heat up.
4. the method for preparing internal wall brick according to claim 1, is characterized in that: the water-intake rate of described base substrate is 6.0 ~ 6.5%, the modulus of rupture is 44.5 ~ 49.8Mpa.
5. according to the arbitrary described prepared internal wall brick product of internal wall brick method of preparing of claim 1-4, it is characterized in that: described internal wall brick glaze whiteness is 55.44 ~ 62.51%, glossiness is 6.45 ~ 8.03%.
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| CN201410269470.8A CN104016658B (en) | 2014-06-17 | 2014-06-17 | A kind of local waste material in the Inner Mongol that utilizes prepares the method for internal wall brick and obtained internal wall brick product thereof |
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| CN104016658B CN104016658B (en) | 2015-07-29 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104671758A (en) * | 2015-02-14 | 2015-06-03 | 景德镇陶瓷学院 | Low-expansion building ceramic material prepared by utilizing desert sand and wastes and preparation method of low-expansion building ceramic material |
Citations (5)
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|---|---|---|---|---|
| JP2000063169A (en) * | 1998-08-07 | 2000-02-29 | Yukinori Hayashi | Baked compact using grinder sludge |
| CN101164961A (en) * | 2007-09-27 | 2008-04-23 | 王儒林 | Formulation for producing ceramic tile by using phosphorus slag and producing method thereof |
| CN101234885A (en) * | 2008-03-06 | 2008-08-06 | 朝阳华龙企业集团有限公司 | Coal gangue sintering porous decorative brick and manufacturing method thereof |
| CN102786290A (en) * | 2012-07-18 | 2012-11-21 | 程永科 | Technology for manufacturing green sintered wall material through utilizing construction wastes |
| CN103833329A (en) * | 2014-03-12 | 2014-06-04 | 于国泉 | Preparation method of reinforced bone china and product prepared therefrom |
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2014
- 2014-06-17 CN CN201410269470.8A patent/CN104016658B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000063169A (en) * | 1998-08-07 | 2000-02-29 | Yukinori Hayashi | Baked compact using grinder sludge |
| CN101164961A (en) * | 2007-09-27 | 2008-04-23 | 王儒林 | Formulation for producing ceramic tile by using phosphorus slag and producing method thereof |
| CN101234885A (en) * | 2008-03-06 | 2008-08-06 | 朝阳华龙企业集团有限公司 | Coal gangue sintering porous decorative brick and manufacturing method thereof |
| CN102786290A (en) * | 2012-07-18 | 2012-11-21 | 程永科 | Technology for manufacturing green sintered wall material through utilizing construction wastes |
| CN103833329A (en) * | 2014-03-12 | 2014-06-04 | 于国泉 | Preparation method of reinforced bone china and product prepared therefrom |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104671758A (en) * | 2015-02-14 | 2015-06-03 | 景德镇陶瓷学院 | Low-expansion building ceramic material prepared by utilizing desert sand and wastes and preparation method of low-expansion building ceramic material |
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