CN104016364A - Sodium modified chlorite - Google Patents
Sodium modified chlorite Download PDFInfo
- Publication number
- CN104016364A CN104016364A CN201410237833.XA CN201410237833A CN104016364A CN 104016364 A CN104016364 A CN 104016364A CN 201410237833 A CN201410237833 A CN 201410237833A CN 104016364 A CN104016364 A CN 104016364A
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- CN
- China
- Prior art keywords
- chlorite
- sodium
- flap
- mixture
- batching
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000011734 sodium Substances 0.000 title claims abstract description 46
- 229910052708 sodium Inorganic materials 0.000 title claims abstract description 46
- -1 Sodium modified chlorite Chemical class 0.000 title abstract description 9
- 229910001919 chlorite Inorganic materials 0.000 claims abstract description 91
- 229910052619 chlorite group Inorganic materials 0.000 claims abstract description 91
- QBWCMBCROVPCKQ-UHFFFAOYSA-N chlorous acid Chemical compound OCl=O QBWCMBCROVPCKQ-UHFFFAOYSA-N 0.000 claims abstract description 91
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 38
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 claims abstract description 13
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 8
- 235000019820 disodium diphosphate Nutrition 0.000 claims abstract description 8
- GYQBBRRVRKFJRG-UHFFFAOYSA-L disodium pyrophosphate Chemical compound [Na+].[Na+].OP([O-])(=O)OP(O)([O-])=O GYQBBRRVRKFJRG-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 8
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 8
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 8
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 6
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 6
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 9
- 239000000428 dust Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 4
- 235000012054 meals Nutrition 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 3
- 238000000855 fermentation Methods 0.000 claims description 3
- 230000004151 fermentation Effects 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 abstract description 4
- 239000000843 powder Substances 0.000 abstract description 3
- 238000006243 chemical reaction Methods 0.000 abstract description 2
- 238000013329 compounding Methods 0.000 abstract description 2
- 239000000945 filler Substances 0.000 abstract description 2
- 239000000314 lubricant Substances 0.000 abstract description 2
- 230000004048 modification Effects 0.000 abstract description 2
- 238000012986 modification Methods 0.000 abstract description 2
- 239000002594 sorbent Substances 0.000 abstract description 2
- 239000000375 suspending agent Substances 0.000 abstract description 2
- 239000000725 suspension Substances 0.000 abstract description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 abstract 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 abstract 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 abstract 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 abstract 2
- 239000010426 asphalt Substances 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- 235000019422 polyvinyl alcohol Nutrition 0.000 abstract 1
- 238000007780 powder milling Methods 0.000 abstract 1
- 235000019794 sodium silicate Nutrition 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 238000005065 mining Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- PZZYQPZGQPZBDN-UHFFFAOYSA-N aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 229910052626 biotite Inorganic materials 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 229910052892 hornblende Inorganic materials 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052901 montmorillonite Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000031068 symbiosis, encompassing mutualism through parasitism Effects 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses sodium modified chlorite, and the key points of the technical scheme are that: sodium modified chlorite ingredients comprise chlorite, magnesium oxide, sodium carbonate, instant sodium silicate, polyvinyl alcohol, hydroxypropyl methyl cellulose and sodium acid pyrophosphate. A production method of the sodium modified chlorite is as follows: sodium modified chlorite ingredients are transported into a mill for powder milling, and the milled powder is the sodium modified chlorite. By first sodium modification and then ingredient compounding, chemical reaction of the sodium carbonate and the instant sodium silicate, the polyvinyl alcohol and the hydroxypropyl methyl cellulose can be avoided. According to the needs of product quality, the sodium acid pyrophosphate is used for adjusting the PH of the sodium modified chlorite. The sodium modified chlorite has the characteristics of good adsorption, suspension property, thixotropy, lubricity and thermal stability and high plasticity, and is applicable to the production of filler, sorbents, suspending agents and lubricants for asphalt felts, paper making, pesticides and fire control products.
Description
Technical field
The present invention relates to sodium processing, be specifically related to the chlorite after a kind of sodium.
Background technology
Chlorite is a kind of aluminium silicate mineral, and normal and spontaneous quartzy symbiosis, is needle shape, bobbles shape, rose-shaped, and the occurrence in hole has hole liner and pore filling.General needle shape chlorite mostly is hole liner and is wrapped in particle surface, bobbles shape and rose-shaped being filled in hole.Chlorite can be by Mineral Transformation such as biotite, hornblende, montmorillonites, and authigenic chlorite is generally rich in high price iron ion, and easily produce precipitation with the acid solution effect such as HCL in drilling fluid, and cause reservoir damage, be acid sensitivity mineral.
In chlorite mining area, usage mining machine carries out mechanical mining chlorite raw ore, excavate out be a kind of compact mass chlorite raw ore, can not be directly used in sodium processing.
Sodium is not carried out follow-up complementary modification after processing, and can not improve the quality of chlorite product comprehensively.
Summary of the invention
The object of the invention is to overcome weak point in prior art, the chlorite after a kind of sodium is provided.
Chlorite batching after sodium is made up of chlorite, magnesium oxide, sodium carbonate, quick dissolved sodium silicate, polyvinyl alcohol, Vltra tears and sodium acid pyrophosphate.
The production method of the chlorite after sodium: by abrasive dust in the chlorite batching input grinding machine after sodium, the meal after abrasive dust is the chlorite after sodium.
Chlorite is extensively present in occurring in nature using forms such as particulate aggregate, crystallization lamellar bodies as the product of normal metamorphism, sedimentation and hydrothermal alteration effect conventionally.Its crystalline structure, physical properties, Chemical Composition and geological occurrence are in close relations, have certain metallogenic relation, chlorite particle fineness≤0.5 millimeter that the present invention selects.
Magnesium oxide has the general character of basic oxide, belongs to gelling material, can improve the colloidal property of chlorite.
Sodium carbonate has the general character and the thermostability of salt, soluble in water, and its aqueous solution is alkalescence, is the main raw material of sodium in the present invention.
Quick dissolved sodium silicate is white pulverulent material, can be dissolved in fast water, has that cohesive force is strong, intensity is higher, acid resistance, good heat resistance, the feature of alkali resistance and poor water resistance.
Polyethenol series white solid, that external form is divided is cotton-shaped, particulate state, Powdered three kinds; Nonpoisonous and tasteless, particulate state can be dissolved in 80--90 DEG C of water, pulverously after other powders pre-dispersed, can dissolve at normal temperatures.There is good viscosity, polymerizability, cohesiveness and water-retentivity.
Vltra tears has thickening capabilities, salt discharge, pH stability, water-retentivity, dimensional stability, good film-forming properties and the feature such as resistance to enzyme, dispersiveness and cohesiveness widely.
Sodium acid pyrophosphate is a kind of white powder, and relative density 1.86 is water-soluble, and the pH value of 1% aqueous solution is 3.5～4.5, for adjusting the chlorite pH value after sodium.
The present invention is achieved by following technical proposals:
1, the batching of the chlorite after sodium is made up of following component by weight percentage: chlorite flap 90～98%, quick dissolved sodium silicate 0.1～5%, polyvinyl alcohol 0.1～5%, Vltra tears 0.01～3% and sodium acid pyrophosphate 0～5%.
2, the production method of the chlorite after sodium: by abrasive dust in the chlorite batching input grinding machine after sodium, particle fineness≤0.074 millimeter, the meal after abrasive dust is the chlorite after sodium.
3, the production method of chlorite flap: (1) by chlorite mixture input fermentation vat, then water is slowly added in chlorite mixture and soaks sodium, sodium soak time is 24～72 hours; (2) take out the chlorite mixture after soaking, input is stirred in biaxial rneader, inputs and in extrusion machine, be extruded into chlorite flap, chlorite thickness of flap≤3 millimeter after stirring.
(3) chlorite flap is transported in rotary type stoving oven and is dried, drying time control is 1～3 hour, and bake out temperature is controlled at 80～100 DEG C, and the chlorite flap water content after oven dry is 10～15%, and PCm is weight percentage.
4, the batching of chlorite flap is made up of following component by weight percentage: chlorite mixture 65～85% and water 15～35%.
5, the production method of chlorite mixture: by stirring in the batching input stirrer of chlorite mixture, be chlorite mixture after stirring.
6, the batching of chlorite mixture is made up of following component by weight percentage: chlorite 92～98%, magnesium oxide 0.5～5% and sodium carbonate 0.5～5%.
The production method of the chlorite after sodium takes first sodium to carry out compounding ingredient again, can avoid sodium carbonate and quick dissolved sodium silicate, polyvinyl alcohol and Vltra tears generation chemical reaction, give full play to raw-material characteristic separately in batching, and obtain complementation, guarantee the chlorite inner quality after sodium.
According to the needs of quality product, adopt sodium acid pyrophosphate to adjust the chlorite pH value after sodium.
Chlorite after sodium has good adsorptivity, suspension, thixotropy, oilness, thermostability and higher plasticity-feature.
Chlorite after sodium is applicable to produce filler, sorbent material, suspension agent and the lubricant of malthoid, papermaking, agricultural chemicals, fire product.
Embodiment
Below in conjunction with embodiment, the invention will be further described:
1, the batching of the chlorite after sodium is made up of following component by weight percentage: chlorite flap 95.6%, quick dissolved sodium silicate 2.1%, polyvinyl alcohol 1.6%, Vltra tears 0.5% and sodium acid pyrophosphate 0.2%.
2, the production method of the chlorite after sodium: by abrasive dust in the chlorite batching input grinding machine after sodium, particle fineness≤0.074 millimeter, the meal after abrasive dust is the chlorite after sodium.
3, the production method of chlorite flap: (1) by chlorite mixture input fermentation vat, then water is slowly added in chlorite mixture and soaks sodium, sodium soak time is 48 hours; (2) take out the chlorite mixture after soaking, input is stirred in biaxial rneader, inputs and in extrusion machine, be extruded into chlorite flap, chlorite thickness of flap≤3 millimeter after stirring; (3) chlorite flap is transported in rotary type stoving oven and is dried, drying time control is 2 hours, and bake out temperature is controlled at 80～100 DEG C, and the chlorite flap water content after oven dry is 10～12%.
4, the batching of chlorite flap is made up of following component by weight percentage: chlorite mixture 76% and water 24%.
5, the production method of chlorite mixture: by stirring in the batching input stirrer of chlorite mixture, be chlorite mixture after stirring.
6, the batching of chlorite mixture is made up of following component by weight percentage: chlorite 94.5%, magnesium oxide 3% and sodium carbonate 2.5%.
Claims (7)
1. the chlorite after a sodium, it is characterized in that, the chlorite batching after sodium is made up of following component by weight percentage: chlorite flap 90～98%, quick dissolved sodium silicate 0.1～5%, polyvinyl alcohol 0.1～5%, Vltra tears 0.01～3% and sodium acid pyrophosphate 0～5%.
2. the production method of the chlorite after sodium according to claim 1, is characterized in that, by abrasive dust in the chlorite batching input grinding machine after sodium, and particle fineness≤0.074 millimeter, the meal after abrasive dust is the chlorite after sodium.
3. the production method of chlorite flap according to claim 1, is characterized in that, (1) by chlorite mixture input fermentation vat, then water is slowly added in chlorite mixture and soaks sodium, and sodium soak time is 24～72 hours; (2) take out the chlorite mixture after soaking, input is stirred in biaxial rneader, inputs and in extrusion machine, be extruded into chlorite flap, chlorite thickness of flap≤3 millimeter after stirring; (3) chlorite flap is transported in rotary type stoving oven and is dried, drying time control is 1～3 hour, and bake out temperature is controlled at 80～100 DEG C, and the chlorite flap water content after oven dry is 10～15%, and PCm is weight percentage.
4. the batching of chlorite flap according to claim 1, is characterized in that, the batching of chlorite flap is made up of following component by weight percentage: chlorite mixture 65～85% and water 15～35%.
5. the production method of chlorite mixture according to claim 3, is characterized in that, by stirring in the batching input stirrer of chlorite mixture, is chlorite mixture after stirring.
6. the batching of chlorite mixture according to claim 5, is characterized in that, the batching of chlorite mixture is made up of following component by weight percentage: chlorite 92～98%, magnesium oxide 0.5～5% and sodium carbonate 0.5～5%.
7. chlorite according to claim 6, is characterized in that chlorite particle fineness≤0.5 millimeter of selecting.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410237833.XA CN104016364B (en) | 2014-06-01 | 2014-06-01 | Chlorite after sodium |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410237833.XA CN104016364B (en) | 2014-06-01 | 2014-06-01 | Chlorite after sodium |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104016364A true CN104016364A (en) | 2014-09-03 |
| CN104016364B CN104016364B (en) | 2016-07-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410237833.XA Active CN104016364B (en) | 2014-06-01 | 2014-06-01 | Chlorite after sodium |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104016364B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58135121A (en) * | 1982-01-30 | 1983-08-11 | Osaka Soda Co Ltd | Manufacture of formed zeolite |
| CN1912015A (en) * | 2006-08-25 | 2007-02-14 | 蒋文兰 | Concave convex rod suspension agent |
| CN101781881A (en) * | 2009-12-08 | 2010-07-21 | 许庆华 | Method for absorbing and cleaning road surface oil |
-
2014
- 2014-06-01 CN CN201410237833.XA patent/CN104016364B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58135121A (en) * | 1982-01-30 | 1983-08-11 | Osaka Soda Co Ltd | Manufacture of formed zeolite |
| CN1912015A (en) * | 2006-08-25 | 2007-02-14 | 蒋文兰 | Concave convex rod suspension agent |
| CN101781881A (en) * | 2009-12-08 | 2010-07-21 | 许庆华 | Method for absorbing and cleaning road surface oil |
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| Publication number | Publication date |
|---|---|
| CN104016364B (en) | 2016-07-06 |
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| C41 | Transfer of patent application or patent right or utility model | ||
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Effective date of registration: 20151210 Address after: 510640, room 715-716, China Education building, No. five, 371-1 mountain road, Guangzhou, Guangdong, Tianhe District Applicant after: GUANGDONG HUABO ENTERPRISE MANAGEMENT CONSULTING Co.,Ltd. Address before: 211700 Huaian, Xuyi province Timor King international residential area, building 2, unit 202 room 18 Applicant before: Xu Shengying |
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Effective date of registration: 20160301 Address after: Tianhe District Tong East Road Guangzhou city Guangdong province 510665 B-101 No. 5, room B-118 Applicant after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: 510640, room 715-716, China Education building, No. five, 371-1 mountain road, Guangzhou, Guangdong, Tianhe District Applicant before: GUANGDONG HUABO ENTERPRISE MANAGEMENT CONSULTING Co.,Ltd. |
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| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Tang Ke Inventor before: Huang Feixiang Inventor before: Huang Yunjin Inventor before: Chen Liping Inventor before: Xu Shengying Inventor before: Xu Qinghua Inventor before: Jiang Wenlan |
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Effective date of registration: 20160603 Address after: 401320, No. 113 South Main Road, Banan District, Chongqing Applicant after: CHONGQING HUANDE TECHNOLOGY Co.,Ltd. Address before: Tianhe District Tong East Road Guangzhou city Guangdong province 510665 B-101 No. 5, room B-118 Applicant before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. |
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Effective date of registration: 20200416 Address after: 401320 No. 249 Yunan Avenue, Banan District, Chongqing, 8-29 Patentee after: Chongqing Boshi Intellectual Property Service Co.,Ltd. Address before: 401320, No. 113 South Main Road, Banan District, Chongqing Patentee before: CHONGQING HUANDE TECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20201202 Address after: 313000 Fang Qiaotou, Zhili village, Zhili Town, Wuxing District, Huzhou, Zhejiang Patentee after: Zhejiang Chuangwei New Material Co.,Ltd. Address before: 401320 No. 249 Yunan Avenue, Banan District, Chongqing, 8-29 Patentee before: Chongqing Boshi Intellectual Property Service Co.,Ltd. |
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Denomination of invention: Sodium chlorite Effective date of registration: 20221216 Granted publication date: 20160706 Pledgee: Huzhou Wuxing Rural Commercial Bank Co.,Ltd. Zhili sub branch Pledgor: Zhejiang Chuangwei New Material Co.,Ltd. Registration number: Y2022330003684 |
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Granted publication date: 20160706 Pledgee: Huzhou Wuxing Rural Commercial Bank Co.,Ltd. Zhili sub branch Pledgor: Zhejiang Chuangwei New Material Co.,Ltd. Registration number: Y2022330003684 |
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Denomination of invention: Sodium treated chlorite Granted publication date: 20160706 Pledgee: Huzhou Wuxing Rural Commercial Bank Co.,Ltd. Zhili sub branch Pledgor: Zhejiang Chuangwei New Material Co.,Ltd. Registration number: Y2024330000894 |