CN103993510A - Fuel oil filter paper capable of realizing oil-water separation and preparation method thereof - Google Patents

Fuel oil filter paper capable of realizing oil-water separation and preparation method thereof Download PDF

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Publication number
CN103993510A
CN103993510A CN201410169904.7A CN201410169904A CN103993510A CN 103993510 A CN103993510 A CN 103993510A CN 201410169904 A CN201410169904 A CN 201410169904A CN 103993510 A CN103993510 A CN 103993510A
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CN
China
Prior art keywords
parts
water
filter paper
auxiliary agent
fuel oil
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Pending
Application number
CN201410169904.7A
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Chinese (zh)
Inventor
金鑫
胡辉
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BENGBU SHOUCHUANG FILTER Co Ltd
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BENGBU SHOUCHUANG FILTER Co Ltd
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Priority to CN201410169904.7A priority Critical patent/CN103993510A/en
Publication of CN103993510A publication Critical patent/CN103993510A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a fuel oil filter paper capable of realizing oil-water separation. The fuel oil filter paper is characterized by being prepared from the following raw materials by weight: 52 to 55 parts of masson pine pulp, 49 to 51 parts of Korean pine pulp, 3 to 5 parts of dried Korean pine pulp, 11 to 12 parts of an acrylic resin emulsion, 1 to 2 parts of a dispersant NNO, 0.4 to 0.6 part of OP-10, 2 to 3 parts of calcium peroxide, 1 to 2 parts of a zeolite molecular sieve, 1 to 2 parts of hectorite, 2 to 3 parts of zircon, 0.6 to 0.8 part of Arabic gum, 0.4 to 0.6 part of sodium tripolyphosphate, 3 to 5 parts of turpentine, 2 to 4 parts of acetic acid, 1 to 2 parts of an auxiliary agent and a proper amount of water. The filter paper provided by the invention has a reasonable formula, uniformly dispersed components and good adsorption and filtering effects; the auxiliary agent is added, which is safe and environment-friendly, small pores are formed in the surface of the filter paper, so adsorptivity is improved; and the filter paper has good water resistance and fuel oil resistance stability and realizes oil-water separation.

Description

A kind of fuel oil filter paper of realizing water-oil separating and preparation method thereof
Technical field
The present invention relates to automobile filter field, particularly a kind of fuel oil filter paper of realizing water-oil separating and preparation method thereof.
Background technology
As the fuel filter paper of one of automobile three filter paper, Main Function is filter fuel, and the impurity in clean fuel oil prevents that them from entering injection valve and cold start-up device, reduces mechanical wear, guarantees engine stable operation, improves reliability.In order to ensure that internal combustion engine carries out safely and effectively, supporting filter material must possess good mechanical property and certain water resistant, fire resistant oil stability with it, with the strainability that ensures that filter paper is good.The filter paper using in fuel filter product on existing market is mostly the common filter paper of the solid-phase contaminants in can only filter fuel, but existing common filter paper is helpless to the separation of moisture content in fuel oil.And water in fuel oil has sizable harm, enter water in fuel oil and will cause the corrosion of oil supply system precision part and cylinder.
Summary of the invention
The object of this invention is to provide a kind of fuel oil filter paper of realizing water-oil separating and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
Realize a fuel oil filter paper for water-oil separating, made by the raw material of following weight portion: masson s pine pulp 52-55, Korean pine slurry 49-51, dry Korean pine leaf 3-5, emulsion acrylic resin 11-12, dispersant NNO 1-2, OP-10 0.4-0.6, calper calcium peroxide 2-3, zeolite molecular sieve 1-2, hectorite 1-2, zircon 2-3, Arabic gum 0.6-0.8, sodium phosphate trimer 0.4-0.6, turpentine oil 3-5, acetic acid 2-4, auxiliary agent 1-2, water are appropriate;
Described auxiliary agent is made up of the raw material of following weight portion: caulis bambusae in taenian 2-3, grape pip 1-2, charcoal 3-4, attapulgite 3-5, nano titanium oxide 2-3, guar gum 3-5, acrylate and vinyl acetate emulsion 2-3, polyvinyl alcohol 1-2, water 50-60; First preparation method rolls into a ball into caulis bambusae in taenian the chopping of little group, and putting into pulverizer together with grape pip, to pulverize 120-140 object mixed-powder stand-by; Then guar gum, acrylate and vinyl acetate emulsion, polyvinyl alcohol are mixed, add appropriate water to stir, be heated to 30-35 DEG C of continuation stirring and add attapulgite, nano titanium oxide after 10-15 minute, continue insulation 20-25 minute, finally add mixed-powder to stir, form turbid liquid.
A kind of fuel oil filter paper of realizing water-oil separating of the present invention, made by following concrete steps:
(1) will be dried Korean pine leaf, zeolite molecular sieve, hectorite, zircon and mix, grind to form 50-100 object powder, add dispersant NNO, with the speed of 850-950 rev/min, stir 25-30 minute, then 50-60 DEG C dry 1.5-2.5 hour stand-by;
(2) masson s pine pulp, Korean pine slurry are put into hydrabrusher size degradation, then through beater, beating consistency is controlled at 5.5-6.6%, makes slurry;
(3) compound of step (1) is added in slurry, add OP-10, calper calcium peroxide, be heated to 65-75 DEG C, stir, add appropriate water size mixing to solid content be 2.4-3.0%, the slurry mixing up, after forming web moulding, aspirates dehydration to the l Water Paper after moulding under the vacuum condition of 0.05-0.08Mpa;
(4) by all the other the residual components mixing and stirring except auxiliary agent, the water that adds 2-3 doubly to measure, then heating, temperature is controlled at 60-70 DEG C, boils 50-60 minute, insulation 25-30 minute, be warming up to 70-75 DEG C, stir and make maceration extract and put into dipping tank;
(5) body paper after step (3) dehydration is passed through to dipping tank with the speed of 3-3.5m/s, maceration extract is uniformly coated on body paper, in electric drying oven with forced convection, dries 4-5min, then auxiliary agent is coated on the body paper of oven dry, dry 6-10min on last ray machine, after taking-up and get final product.
The invention has the beneficial effects as follows: filter paper formula of the present invention is reasonable, and each component is uniformly dispersed, and adsorption filtration is effective, add auxiliary agent, safety and environmental protection, the small hole forming on filter paper surface, increase adsorptivity, there is good resistance to water and fire resistant oil stability, realized water-oil separating.
Specific embodiments
Below by instantiation, the present invention is described in detail.
Realize a fuel oil filter paper for water-oil separating, by following weight portion (kilogram) raw material make: masson s pine pulp 52, Korean pine slurry 49, dry Korean pine leaf 3, emulsion acrylic resin 11, dispersant NNO 1, OP-10 0.4, calper calcium peroxide 2, zeolite molecular sieve 1, hectorite 1, zircon 2, Arabic gum 0.6, sodium phosphate trimer 0.4, turpentine oil 3, acetic acid 2, auxiliary agent 1, water are appropriate;
Described auxiliary agent by following weight portion (kilogram) raw material make: caulis bambusae in taenian 2, grape pip 1, charcoal 3, attapulgite 3, nano titanium oxide 2, guar gum 3, acrylate and vinyl acetate emulsion 2, polyvinyl alcohol 1, water 50; First preparation method rolls into a ball into caulis bambusae in taenian the chopping of little group, and putting into pulverizer together with grape pip, to pulverize 120-140 object mixed-powder stand-by; Then guar gum, acrylate and vinyl acetate emulsion, polyvinyl alcohol are mixed, add appropriate water to stir, be heated to 30-35 DEG C of continuation stirring and add attapulgite, nano titanium oxide after 10-15 minute, continue insulation 20-25 minute, finally add mixed-powder to stir, form turbid liquid.
A kind of fuel oil filter paper of realizing water-oil separating of the present invention, made by following concrete steps:
(1) will be dried Korean pine leaf, zeolite molecular sieve, hectorite, zircon and mix, grind to form 50-100 object powder, add dispersant NNO, with the speed of 850-950 rev/min, stir 25-30 minute, then 50-60 DEG C dry 1.5-2.5 hour stand-by;
(2) masson s pine pulp, Korean pine slurry are put into hydrabrusher size degradation, then through beater, beating consistency is controlled at 5.5-6.6%, makes slurry;
(3) compound of step (1) is added in slurry, add OP-10, calper calcium peroxide, be heated to 65-75 DEG C, stir, add appropriate water size mixing to solid content be 2.4-3.0%, the slurry mixing up, after forming web moulding, aspirates dehydration to the l Water Paper after moulding under the vacuum condition of 0.05-0.08Mpa;
(4) by all the other the residual components mixing and stirring except auxiliary agent, the water that adds 2-3 doubly to measure, then heating, temperature is controlled at 60-70 DEG C, boils 50-60 minute, insulation 25-30 minute, be warming up to 70-75 DEG C, stir and make maceration extract and put into dipping tank;
(5) body paper after step (3) dehydration is passed through to dipping tank with the speed of 3-3.5m/s, maceration extract is uniformly coated on body paper, in electric drying oven with forced convection, dries 4-5min, then auxiliary agent is coated on the body paper of oven dry, dry 6-10min on last ray machine, after taking-up and get final product.
The Air permenbility 85-90 L/m of the filter paper that after testing, the present invention makes 2between s, maximum diameter of hole is 53-55 μ m, and average pore size is 45 μ m.

Claims (2)

1. realize the fuel oil filter paper of water-oil separating for one kind, it is characterized in that, made by the raw material of following weight portion: masson s pine pulp 52-55, Korean pine slurry 49-51, dry Korean pine leaf 3-5, emulsion acrylic resin 11-12, dispersant NNO 1-2, OP-10 0.4-0.6, calper calcium peroxide 2-3, zeolite molecular sieve 1-2, hectorite 1-2, zircon 2-3, Arabic gum 0.6-0.8, sodium phosphate trimer 0.4-0.6, turpentine oil 3-5, acetic acid 2-4, auxiliary agent 1-2, water are appropriate;
Described auxiliary agent is made up of the raw material of following weight portion: caulis bambusae in taenian 2-3, grape pip 1-2, charcoal 3-4, attapulgite 3-5, nano titanium oxide 2-3, guar gum 3-5, acrylate and vinyl acetate emulsion 2-3, polyvinyl alcohol 1-2, water 50-60; First preparation method rolls into a ball into caulis bambusae in taenian the chopping of little group, and putting into pulverizer together with grape pip, to pulverize 120-140 object mixed-powder stand-by; Then guar gum, acrylate and vinyl acetate emulsion, polyvinyl alcohol are mixed, add appropriate water to stir, be heated to 30-35 DEG C of continuation stirring and add attapulgite, nano titanium oxide after 10-15 minute, continue insulation 20-25 minute, finally add mixed-powder to stir, form turbid liquid.
2. a kind of fuel oil filter paper of realizing water-oil separating according to claim 1, is characterized in that, is made up of following concrete steps:
(1) will be dried Korean pine leaf, zeolite molecular sieve, hectorite, zircon and mix, grind to form 50-100 object powder, add dispersant NNO, with the speed of 850-950 rev/min, stir 25-30 minute, then 50-60 DEG C dry 1.5-2.5 hour stand-by;
(2) masson s pine pulp, Korean pine slurry are put into hydrabrusher size degradation, then through beater, beating consistency is controlled at 5.5-6.6%, makes slurry;
(3) compound of step (1) is added in slurry, add OP-10, calper calcium peroxide, be heated to 65-75 DEG C, stir, add appropriate water size mixing to solid content be 2.4-3.0%, the slurry mixing up, after forming web moulding, aspirates dehydration to the l Water Paper after moulding under the vacuum condition of 0.05-0.08Mpa;
(4) by all the other the residual components mixing and stirring except auxiliary agent, the water that adds 2-3 doubly to measure, then heating, temperature is controlled at 60-70 DEG C, boils 50-60 minute, insulation 25-30 minute, be warming up to 70-75 DEG C, stir and make maceration extract and put into dipping tank;
(5) body paper after step (3) dehydration is passed through to dipping tank with the speed of 3-3.5m/s, maceration extract is uniformly coated on body paper, in electric drying oven with forced convection, dries 4-5min, then auxiliary agent is coated on the body paper of oven dry, dry 6-10min on last ray machine, after taking-up and get final product.
CN201410169904.7A 2014-04-25 2014-04-25 Fuel oil filter paper capable of realizing oil-water separation and preparation method thereof Pending CN103993510A (en)

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CN201410169904.7A CN103993510A (en) 2014-04-25 2014-04-25 Fuel oil filter paper capable of realizing oil-water separation and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201410169904.7A CN103993510A (en) 2014-04-25 2014-04-25 Fuel oil filter paper capable of realizing oil-water separation and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105986528A (en) * 2016-01-29 2016-10-05 蚌埠首创滤清器有限公司 Hydraulic oil filter paper capable of separating oil from water efficiently
CN112553963A (en) * 2020-12-02 2021-03-26 中国科学院长春应用化学研究所 Diatomite-based filter paper, and preparation method and application thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101988279A (en) * 2009-08-06 2011-03-23 苏州新业造纸有限公司 Production process of oil-water separation filter paper
CN102533032A (en) * 2010-12-10 2012-07-04 深圳市嘉达高科产业发展有限公司 Automatic indoor humidity adjusting coating
CN102877372A (en) * 2012-09-25 2013-01-16 蚌埠凤凰滤清器有限责任公司 High temperature-resisting filter paper for automobile filter
CN102877369A (en) * 2012-09-20 2013-01-16 蚌埠凤凰滤清器有限责任公司 Bamboo load-bearing chitosan industrial filter paper for automobiles and preparation method of bamboo load-bearing chitosan industrial filter paper
CN102912680A (en) * 2012-09-20 2013-02-06 蚌埠凤凰滤清器有限责任公司 High-temperature resistant fiber filter paper for engine oil filter and preparation method of high-temperature resistant fiber filter paper

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101988279A (en) * 2009-08-06 2011-03-23 苏州新业造纸有限公司 Production process of oil-water separation filter paper
CN102533032A (en) * 2010-12-10 2012-07-04 深圳市嘉达高科产业发展有限公司 Automatic indoor humidity adjusting coating
CN102877369A (en) * 2012-09-20 2013-01-16 蚌埠凤凰滤清器有限责任公司 Bamboo load-bearing chitosan industrial filter paper for automobiles and preparation method of bamboo load-bearing chitosan industrial filter paper
CN102912680A (en) * 2012-09-20 2013-02-06 蚌埠凤凰滤清器有限责任公司 High-temperature resistant fiber filter paper for engine oil filter and preparation method of high-temperature resistant fiber filter paper
CN102877372A (en) * 2012-09-25 2013-01-16 蚌埠凤凰滤清器有限责任公司 High temperature-resisting filter paper for automobile filter

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105986528A (en) * 2016-01-29 2016-10-05 蚌埠首创滤清器有限公司 Hydraulic oil filter paper capable of separating oil from water efficiently
CN112553963A (en) * 2020-12-02 2021-03-26 中国科学院长春应用化学研究所 Diatomite-based filter paper, and preparation method and application thereof
CN112553963B (en) * 2020-12-02 2022-05-06 中国科学院长春应用化学研究所 Diatomite-based filter paper, and preparation method and application thereof

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