CN103989747A - Method for comprehensively utilizing mulberry twig through medicine extraction and pulping - Google Patents
Method for comprehensively utilizing mulberry twig through medicine extraction and pulping Download PDFInfo
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- CN103989747A CN103989747A CN201410235988.XA CN201410235988A CN103989747A CN 103989747 A CN103989747 A CN 103989747A CN 201410235988 A CN201410235988 A CN 201410235988A CN 103989747 A CN103989747 A CN 103989747A
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- ramulus mori
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Abstract
The invention discloses a method for comprehensively utilizing mulberry twigs through medicine extraction and pulping. The method is characterized by comprising the following steps: A, cutting raw material into segments by using a cutting machine, so as to make a crude material; B, screening the crude material, and washing to make a refined material; C, heating and decocting the refined material in an extraction tank, separating the material from liquid after decoction, wherein the separated material is used as decocted material and the separated liquid is used as decoction; D mixing the decoction into medicine ( half-finished product ointment liquid such as mulberry twig ointment) by an evaporation tank; E, peeling off the skin of the decocted material in a peeling machine to separate the skin and the stalks; and F, pulping the separated skin and stalks. By adopting the method, waste resources can be comprehensively utilized in a cross-industry manner, the waste is turned into wealthy, the environment pollution is avoided, the production cost is lowered, and the resource utilization rate of the mulberry twigs is improved; meanwhile a new way is provided for high additional value conversion and utilization of the mulberry twigs, and relatively great economic, social and environmental benefits are achieved.
Description
One, technical field:
The invention belongs to pharmacy and pulping and paper-making industry, be specifically related to a kind of method of extracting medicine and slurrying comprehensive utilization Ramulus Mori, be applicable to the comprehensive utilization to Ramulus Mori.
Two, background technology.
Ramulus Mori is a kind of paper making raw material of high-quality, is again a kind of traditional Chinese crude drug, and China's planting mulberry and breeding silkworm are with a long history, Ramulus Mori resource and abundant, but these raw materials are at pulping and paper-making, and pharmaceutical field consumption is less, most of local Ramulus Mori is burnt as domestic fuel by common people, or on-site incineration, and air is contaminated, cause some regional haze weather serious, trace it to its cause, main existence for pulp and paper industry, skin bar separation difficulty, full stalk pulping by cooking consumes high, and loss is large, and black liquor is difficult; For pharmaceutical industry, the problem such as garbage is difficult, production cost height.
Look through Chinese patent communique and a large amount of books, the existing technology adopting mainly contains: Ramulus Mori has for slurrying: sulfate pulping, full stalk pulping with ammonium sulfite method, soda anthraquinone process etc.Have for pharmacy: Ramulus Mori decocts with water rear concentrated, formula, reconcentration, produces the medicines such as Ramulus Mori cream.Above technology causes Ramulus Mori utilization rate not high.
Chinese patent application discloses a kind of pulping process that utilizes the chemi-mechanical pulp that mulberry branch is raw material for No. 200610020910, and it is successively by section; Decatize before washing; Washing; Decatize after washing; One section of squeezing; Two-stage nitration squeezing; Dipping; Reaction and post-processing step carry out.
No. CN02113004, Chinese patent application, discloses a kind of Ramulus Mori extract and has been prepared into the health product of prevention hyperuricemia and the medicine for the treatment of hyperuricemia.This Ramulus Mori extract is to extract and obtain by following method: get dry Ramulus Mori decoction pieces, with 7 times of volume 60% ethanol waters, hot reflux three times, each 2 hours, extracting solution is merged, concentrating under reduced pressure, removes extracting solution after ethanol through polyamide column chromatography, water, 30% ethanol, 60% ethanol and 80% ethanol eluting successively, reclaim respectively solvent, concentrate drying.
No. 201010142525, Chinese patent application, disclose a kind of Ramulus Mori and manufactured the method for fireproof density plate, after Ramulus Mori is pulverized, with oxygen magnesium cement, perlite, Pulvis Talci or silica flour in mass ratio for 1-2: 5-8: prepare burden at 0.1: 0.3, add coagulant to carry out stirring to pulp, slurry after accomplishing fluently is put into rapidly to roll squeezer roll-in, sizing after fixing, demoulding, then according to target specification cutting plain cushion maintenance 5-8 days, put into water and soak 6-10 hour, then taking-up is dried or is air-dry, and according to target specification is carried out montage, cutting, classification, inspection.
No. 201010585888, Chinese patent application, discloses a kind of cultural method of Ganoderma (cultivated with Ramulus Mori).The method comprises the steps: A, pack; B, disinfection inoculation; C, cultivation; D, urge flower bud occur; E educates mushroom management; F, grafting; G, aeration-drying; H, spray paint, mounted box.
The common problem existing of technique scheme is: Ramulus Mori conversion ratio, output capacity are lower, does not realize the resource value of Ramulus Mori completely.
How rationally to make good use of Ramulus Mori raw material, both met national industrial policies, again can be for common people increase income, increase idle labor employment, Ramulus Mori has fully utilized into a difficult problem.
Three, summary of the invention:
The object of the invention is: inventor, in order to solve a Ramulus Mori comprehensive development and utilization difficult problem, according to the feature of Ramulus Mori raw material, works out a kind of method of extracting medicine and slurrying comprehensive utilization Ramulus Mori, the defect existing to overcome prior art.
Concrete technical solution of the present invention is as follows;
A method of extracting medicine and slurrying comprehensive utilization Ramulus Mori, is characterized in that the step of the method is as follows;
A, prepare enough Ramulus Mori branches, form raw material after removing the impurity on branch, raw material is cut into joint with stock-cutter, every joint length is controlled at 10-60 millimeter, forms coarse fodder.
B, coarse fodder is screened with screening machine, after screening, wash with scrubber, remove the silt particle on coarse fodder, dust and other impurity, form concentrate.
C, concentrate are amounted to into over dry material, deliver to extraction pot by the proportioning of material-water ratio 1: 4-8, and heat temperature raising decocts for the first time.Decoct 100 DEG C of temperature, time 3-6 hour.Decoct and finish, carry out feed liquid separation, the material of separating carries out secondary decoction, send into extraction pot heating by the proportioning of material-water ratio 1: 2-6 and boost to after extraction pot internal pressure 0.1-0.4MP a, be incubated 1 one 4 hours, then carry out feed liquid separation, the material of separating forms to decoct and expects, the liquid of separating and first separation liquid out merges, and leaves standstill, and leaching supernatant forms decoction liquor.
D, decoction liquor are delivered to evaporator by the process of existing production Ramulus Mori cream etc., extract and meet the semi-finished product cream liquid of producing Ramulus Mori cream etc.
E, decoction expect to deliver to energy-saving branch wet method peeling machine or energy-saving type induced draft formula peeling machine carries out peeling processing, isolates epidermis, bast and stalk.
F, the epidermis separating reclaim and do the utilization of resources, and bast and stalk adopt the method slurrying such as bioanalysis, APMP or extrusion machinery method.
The stock-cutter adopting in the present invention, the equipment such as screening machine, scrubber, extraction pot, evaporator need meet pharmaceutical industry standard-required, can adopt existing mature equipment, also can manufacture separately by implementing specific design requirement of the present invention, in the present invention, institute's water water quality is by water quality standard for drinking water requirement.The semi-finished product cream liquid quality of producing is by pharmaceutical industry standard-required.
The invention has the beneficial effects as follows:
1, utilize method of the present invention, Ramulus Mori is first produced to meet and is produced Chinese medicine medicine---the semi-finished product cream liquid of Ramulus Mori cream etc., the stalk material of producing after cream liquid carries out the separation of skin stalk again, skin stalk separate after for slurrying, to produce like this Chinese medicine and slurrying and combine use Ramulus Mori, without garbage, non-wastewater discharge, the conversion ratio of raw material, output capacity improve, reduce production cost, overcome the deficiency in existing technology.
2, the semi-finished product cream liquid of producing is made further processing purification processes, can produce the higher product of the output value such as Ramulus Mori cream, Ramulus Mori granule.
3, utilize method of the present invention, the skin of Ramulus Mori (bast) and stalk are separated separately completely, good separating effect, skin stalk quality after separation is good, bast and stalk separately can separate slurrying, solve the difficult problem that in conventional art, full stalk is high-alkali, steaming and decocting under high pressure slurrying cost is high, black liquor refractory is managed, for production high-quality, low consumption, free of contamination Ramulus Mori slurry provide new approach.
4, bast is made long fibered pulp, for the production of speciality paper, also can be used for the high value added products such as textile garment industry production textile, has wide market prospect, has improved the use value of bast.
Stalk has passed through the processing such as screening, washing, decoction, silt particle, heteroproteose cell and soluble substance are removed, its slurrying cost and wastewater treatment expense and existing high pressure, high-alkali, pulping by cooking cost are compared and can greatly be reduced with wastewater treatment expense, and the paper pulp of making can be produced cultural paper, newsprint, wrapping paper etc.
5, there is significant society, economy and environment benefit.
(1) take inter-trade comprehensive development and utilization and converting wastes resource, protected environment, improved Ramulus Mori resource utilization.
(2) adopt peeling machine to carry out skin stalk separating treatment through the Ramulus Mori stalk material extracting after Chinese medicine medicine, after skin stalk separates, the paper pulp yield rate that bast and stalk make is respectively high, quality is good, and energy consumption of unit product is low, and water consumption is few, and pollutional load is light, be convenient to administer, can realize cleaner production.
(3) raw material resources that take full advantage of dispersion are pulping and paper-making, pharmaceutical industry service.For common people increase income, avoid raw material by open incineration contaminated air, cause haze weather serious.
Four, detailed description of the invention.
Provide specific embodiments of the invention below, but enforcement of the present invention is not limited to the following example.Can also have many distortion, all distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention, all should think protection scope of the present invention.
Example 1,
A, prepare enough Ramulus Mori branches, form raw material after removing the impurity on branch, raw material is cut into joint with stock-cutter, every joint length is controlled at 20 millimeters, forms coarse fodder.
B, coarse fodder is screened with screening machine, after screening, wash with scrubber, remove the silt particle on coarse fodder, dust and other impurity, form concentrate.
C, concentrate are amounted to into over dry material, deliver to extraction pot by the material-water ratio proportioning of 1: 5, and heat temperature raising decocts for the first time.Decoct 100 DEG C of temperature, 4 hours time.Decoct and finish, carry out feed liquid separation, the material of separating carries out secondary decoction, send into extraction pot heating by the material-water ratio proportioning of 1: 5 and boost to after extraction pot internal pressure 0.1MP a, be incubated 3 hours, then carry out feed liquid separation, the material of separating forms to decoct and expects, the liquid of separating and first separation liquid out merges, and leaves standstill, and leaching supernatant forms decoction liquor.
D, decoction liquor are delivered to evaporator by the process of existing production Ramulus Mori cream etc., extract and meet the semi-finished product cream liquid of producing Ramulus Mori cream etc.
E, decoction expect to deliver to energy-saving branch wet method peeling machine or energy-saving type induced draft formula peeling machine carries out peeling processing, isolates epidermis, bast and stalk.
F, the epidermis separating reclaim and do the utilization of resources, and bast and stalk adopt the method slurrying such as bioanalysis, APMP or extrusion machinery method.
Example 2,
A, prepare enough Ramulus Mori branches, form raw material after removing the impurity on branch, raw material is cut into joint with stock-cutter, every joint length is controlled at 40 millimeters, forms coarse fodder.
B, coarse fodder is screened with screening machine, after screening, wash with scrubber, remove the silt particle on coarse fodder, dust and other impurity, form concentrate.
C, concentrate are amounted to into over dry material, deliver to extraction pot by the material-water ratio proportioning of 1: 6, and heat temperature raising decocts for the first time.Decoct 100 DEG C of temperature, 5 hours time.Decoct and finish, carry out feed liquid separation, the material of separating carries out secondary decoction, send into extraction pot heating by the material-water ratio proportioning of 1: 4 and boost to after extraction pot internal pressure 0.2MP a, be incubated 2 hours, then carry out feed liquid separation, the material of separating forms to decoct and expects, the liquid of separating and first separation liquid out merges, and leaves standstill, and leaching supernatant forms decoction liquor.
C, decoction liquor are delivered to evaporator by the process of existing production Ramulus Mori cream etc., extract and meet the semi-finished product cream liquid of producing Ramulus Mori cream etc.
D, decoction expect to deliver to energy-saving branch wet method peeling machine or energy-saving type induced draft formula peeling machine carries out peeling processing, isolates epidermis, bast and stalk.
E, the epidermis separating reclaim and do the utilization of resources, and bast and stalk adopt the method slurrying such as bioanalysis, APMP or extrusion machinery method.
Example 3,
A, prepare enough Ramulus Mori branches, form raw material after removing the impurity on branch, raw material is cut into joint with stock-cutter, every joint length is controlled at 60 millimeters, forms coarse fodder.
B, coarse fodder is screened with screening machine, after screening, wash with scrubber, remove the silt particle on coarse fodder, dust and other impurity, form concentrate.
C, concentrate are amounted to into over dry material, deliver to extraction pot by the material-water ratio proportioning of 1: 7, and heat temperature raising decocts for the first time.Decoct 100 DEG C of temperature, 6 hours time.Decoct and finish, carry out feed liquid separation, the material of separating carries out secondary decoction, send into extraction pot heating by the material-water ratio proportioning of 1: 3 and boost to after extraction pot internal pressure 0.3MP a, be incubated 1 hour, then carry out feed liquid separation, the material of separating forms to decoct and expects, the liquid of separating and first separation liquid out merges, and leaves standstill, and leaching supernatant forms decoction liquor.
D, decoction liquor are delivered to evaporator by the process of existing production Ramulus Mori cream etc., extract and meet the semi-finished product cream liquid of producing Ramulus Mori cream etc.
E, decoction expect to deliver to energy-saving branch wet method peeling machine or energy-saving type induced draft formula peeling machine carries out peeling processing, isolates epidermis, bast and stalk.
F, the epidermis separating reclaim and do the utilization of resources, and bast and stalk adopt the method slurrying such as bioanalysis, APMP or extrusion machinery method.
Claims (1)
1. a method of extracting medicine and slurrying comprehensive utilization Ramulus Mori, is characterized in that the step of the method is as follows;
A, prepare enough Ramulus Mori branches, form raw material after removing the impurity on branch, raw material is cut into joint with stock-cutter, every joint length is controlled at 10-60 millimeter, forms coarse fodder.
B, coarse fodder is screened with screening machine, after screening, wash with scrubber, remove the silt particle on coarse fodder, dust and other impurity, form concentrate.
C, concentrate are amounted to into over dry material, deliver to extraction pot by the proportioning of material-water ratio 1: 4-8, and heat temperature raising decocts for the first time.Decoct 100 DEG C of temperature, time 3-6 hour.Decoct and finish, carry out feed liquid separation, the material of separating carries out secondary decoction, send into extraction pot heating by the proportioning of material-water ratio 1: 2-6 and boost to after extraction pot internal pressure 0.1-0.4MP a, insulation 1-4 hour, then carries out feed liquid separation, the material of separating forms to decoct and expects, the liquid of separating and first separation liquid out merges, and leaves standstill, and leaching supernatant forms decoction liquor.
D, decoction liquor are delivered to evaporator by the process of existing production Ramulus Mori cream etc., extract and meet the semi-finished product cream liquid of producing Ramulus Mori cream etc.
E, decoction expect to deliver to energy-saving branch wet method peeling machine or energy-saving type induced draft formula peeling machine carries out peeling processing, isolates epidermis, bast and stalk.
F, the epidermis separating reclaim and do the utilization of resources, and bast and stalk adopt the method slurrying such as bioanalysis, APMP or extrusion machinery method.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106546461A (en) * | 2016-11-07 | 2017-03-29 | 赣南师范大学 | A kind of Citrus phloem sap preparation method |
| CN108017722A (en) * | 2018-01-31 | 2018-05-11 | 张明勋 | One kind utilizes mulberry branch separation cladding and bar material, Preparation method and use |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103538131A (en) * | 2013-11-10 | 2014-01-29 | 张明勋 | Bast-stalk separation technique |
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2014
- 2014-05-30 CN CN201410235988.XA patent/CN103989747A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103538131A (en) * | 2013-11-10 | 2014-01-29 | 张明勋 | Bast-stalk separation technique |
Non-Patent Citations (1)
| Title |
|---|
| 刘刚等: "桑枝的营养功能成分及其综合利用", 《河北农业科学》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106546461A (en) * | 2016-11-07 | 2017-03-29 | 赣南师范大学 | A kind of Citrus phloem sap preparation method |
| CN106546461B (en) * | 2016-11-07 | 2019-03-22 | 赣南师范大学 | A kind of citrus phloem sap preparation method |
| CN108017722A (en) * | 2018-01-31 | 2018-05-11 | 张明勋 | One kind utilizes mulberry branch separation cladding and bar material, Preparation method and use |
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Application publication date: 20140820 |