CN103988035A - 用于从低温烃类组合物中去除氮气的方法和装置 - Google Patents
用于从低温烃类组合物中去除氮气的方法和装置 Download PDFInfo
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- CN103988035A CN103988035A CN201280061161.0A CN201280061161A CN103988035A CN 103988035 A CN103988035 A CN 103988035A CN 201280061161 A CN201280061161 A CN 201280061161A CN 103988035 A CN103988035 A CN 103988035A
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- stripping
- nitrogen
- liquid
- vapor
- steam
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title claims abstract description 470
- 229910052757 nitrogen Inorganic materials 0.000 title claims abstract description 236
- 150000002430 hydrocarbons Chemical class 0.000 title claims abstract description 159
- 229930195733 hydrocarbon Natural products 0.000 title claims abstract description 158
- 238000000034 method Methods 0.000 title claims abstract description 138
- 239000004215 Carbon black (E152) Substances 0.000 title claims abstract description 132
- 239000000203 mixture Substances 0.000 title claims abstract description 75
- 239000007788 liquid Substances 0.000 claims abstract description 173
- 230000008569 process Effects 0.000 claims abstract description 104
- 239000007789 gas Substances 0.000 claims abstract description 48
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 112
- 239000003507 refrigerant Substances 0.000 claims description 84
- 239000012530 fluid Substances 0.000 claims description 50
- 239000002912 waste gas Substances 0.000 claims description 27
- 238000009833 condensation Methods 0.000 claims description 25
- 230000005494 condensation Effects 0.000 claims description 25
- 238000001816 cooling Methods 0.000 claims description 24
- 230000005484 gravity Effects 0.000 claims description 20
- 238000000926 separation method Methods 0.000 claims description 18
- 239000007791 liquid phase Substances 0.000 claims description 14
- 239000000446 fuel Substances 0.000 claims description 13
- 238000010992 reflux Methods 0.000 claims description 12
- 238000011144 upstream manufacturing Methods 0.000 claims description 11
- 239000002737 fuel gas Substances 0.000 claims description 7
- 235000013372 meat Nutrition 0.000 claims description 5
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- 238000001704 evaporation Methods 0.000 claims description 4
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- 238000000605 extraction Methods 0.000 claims description 3
- 241000628997 Flos Species 0.000 claims description 2
- 238000002513 implantation Methods 0.000 claims description 2
- 238000011068 loading method Methods 0.000 description 22
- 239000003949 liquefied natural gas Substances 0.000 description 18
- 238000007906 compression Methods 0.000 description 12
- 238000007710 freezing Methods 0.000 description 11
- 230000008014 freezing Effects 0.000 description 11
- 238000010438 heat treatment Methods 0.000 description 8
- 239000003345 natural gas Substances 0.000 description 8
- 230000008901 benefit Effects 0.000 description 7
- 238000011084 recovery Methods 0.000 description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 6
- 230000001105 regulatory effect Effects 0.000 description 6
- 230000006835 compression Effects 0.000 description 5
- 239000002826 coolant Substances 0.000 description 5
- 230000006837 decompression Effects 0.000 description 5
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 5
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 4
- 238000013459 approach Methods 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 238000011026 diafiltration Methods 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 239000000945 filler Substances 0.000 description 3
- 239000001294 propane Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 230000005587 bubbling Effects 0.000 description 2
- 125000004122 cyclic group Chemical group 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000008485 antagonism Effects 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000007701 flash-distillation Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000001282 iso-butane Substances 0.000 description 1
- 235000013847 iso-butane Nutrition 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 239000007793 ph indicator Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- -1 sulphur compounds Chemical class 0.000 description 1
- 238000002207 thermal evaporation Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
Classifications
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- F25J2200/50—Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2200/00—Processes or apparatus using separation by rectification
- F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2200/00—Processes or apparatus using separation by rectification
- F25J2200/90—Details relating to column internals, e.g. structured packing, gas or liquid distribution
- F25J2200/94—Details relating to the withdrawal point
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2205/00—Processes or apparatus using other separation and/or other processing means
- F25J2205/02—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2210/00—Processes characterised by the type or other details of the feed stream
- F25J2210/06—Splitting of the feed stream, e.g. for treating or cooling in different ways
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2215/00—Processes characterised by the type or other details of the product stream
- F25J2215/04—Recovery of liquid products
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2230/00—Processes or apparatus involving steps for increasing the pressure of gaseous process streams
- F25J2230/60—Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being hydrocarbons or a mixture of hydrocarbons
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2240/00—Processes or apparatus involving steps for expanding of process streams
- F25J2240/30—Dynamic liquid or hydraulic expansion with extraction of work, e.g. single phase or two-phase turbine
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2245/00—Processes or apparatus involving steps for recycling of process streams
- F25J2245/02—Recycle of a stream in general, e.g. a by-pass stream
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2245/00—Processes or apparatus involving steps for recycling of process streams
- F25J2245/90—Processes or apparatus involving steps for recycling of process streams the recycled stream being boil-off gas from storage
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2280/00—Control of the process or apparatus
- F25J2280/02—Control in general, load changes, different modes ("runs"), measurements
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- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11192922.0 | 2011-12-12 | ||
| EP11192922 | 2011-12-12 | ||
| PCT/EP2012/074957 WO2013087569A2 (fr) | 2011-12-12 | 2012-12-10 | Procédé et appareil pour retirer l'azote d'une composition d'hydrocarbures cryogéniques |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103988035A true CN103988035A (zh) | 2014-08-13 |
Family
ID=47351658
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201280061161.0A Pending CN103988035A (zh) | 2011-12-12 | 2012-12-10 | 用于从低温烃类组合物中去除氮气的方法和装置 |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP2791601B1 (fr) |
| JP (1) | JP2015501917A (fr) |
| KR (1) | KR20140103144A (fr) |
| CN (1) | CN103988035A (fr) |
| AU (1) | AU2012350742B2 (fr) |
| CA (1) | CA2858152C (fr) |
| MY (1) | MY172968A (fr) |
| RU (1) | RU2607198C2 (fr) |
| WO (1) | WO2013087569A2 (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110114627A (zh) * | 2016-10-28 | 2019-08-09 | 乔治洛德方法研究和开发液化空气有限公司 | 用于低温分离氢气和一氧化碳的混合物的方法 |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150308737A1 (en) * | 2014-04-24 | 2015-10-29 | Air Products And Chemicals, Inc. | Integrated Nitrogen Removal in the Production of Liquefied Natural Gas Using Intermediate Feed Gas Separation |
| US9945604B2 (en) | 2014-04-24 | 2018-04-17 | Air Products And Chemicals, Inc. | Integrated nitrogen removal in the production of liquefied natural gas using refrigerated heat pump |
| US9816754B2 (en) * | 2014-04-24 | 2017-11-14 | Air Products And Chemicals, Inc. | Integrated nitrogen removal in the production of liquefied natural gas using dedicated reinjection circuit |
| US11221176B2 (en) * | 2018-08-14 | 2022-01-11 | Air Products And Chemicals, Inc. | Natural gas liquefaction with integrated nitrogen removal |
| AU2021364547A1 (en) * | 2020-10-19 | 2023-06-01 | Conocophillips Company | Process composition analysis via online mass spectrometry |
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| US20080066493A1 (en) * | 2004-07-12 | 2008-03-20 | Cornelis Buijs | Treating Liquefied Natural Gas |
| DE102007010032A1 (de) * | 2007-03-01 | 2008-09-04 | Linde Ag | Verfahren zum Abtrennen von Stickstoff aus verflüssigtem Erdgas |
| CN101631934A (zh) * | 2007-01-31 | 2010-01-20 | 尤米科尔股份公司及两合公司 | 贫燃发动机排气装置中的碳烟过滤器的再生方法，以及用于贫燃发动机的排气装置 |
| WO2011009832A2 (fr) * | 2009-07-21 | 2011-01-27 | Shell Internationale Research Maatschappij B.V. | Procédé pour le traitement d'un courant d'hydrocarbure à plusieurs phases et appareil correspondant |
| US20110239701A1 (en) * | 2008-11-03 | 2011-10-06 | Sander Kaart | Method of rejecting nitrogen from a hydrocarbon stream to provide a fuel gas stream and an apparatus therefor |
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| US5669234A (en) | 1996-07-16 | 1997-09-23 | Phillips Petroleum Company | Efficiency improvement of open-cycle cascaded refrigeration process |
| DE19716415C1 (de) | 1997-04-18 | 1998-10-22 | Linde Ag | Verfahren zum Verflüssigen eines Kohlenwasserstoff-reichen Stromes |
| TW477890B (en) | 1998-05-21 | 2002-03-01 | Shell Int Research | Method of liquefying a stream enriched in methane |
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| TW480325B (en) | 1999-12-01 | 2002-03-21 | Shell Int Research | Plant for liquefying natural gas |
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| RU2447382C2 (ru) | 2006-08-17 | 2012-04-10 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Способ и устройство для сжижения потока сырья, содержащего углеводороды |
| US20080141711A1 (en) | 2006-12-18 | 2008-06-19 | Mark Julian Roberts | Hybrid cycle liquefaction of natural gas with propane pre-cooling |
-
2012
- 2012-12-10 EP EP12799178.4A patent/EP2791601B1/fr active Active
- 2012-12-10 AU AU2012350742A patent/AU2012350742B2/en active Active
- 2012-12-10 JP JP2014546441A patent/JP2015501917A/ja active Pending
- 2012-12-10 CA CA2858152A patent/CA2858152C/fr active Active
- 2012-12-10 CN CN201280061161.0A patent/CN103988035A/zh active Pending
- 2012-12-10 MY MYPI2014701220A patent/MY172968A/en unknown
- 2012-12-10 KR KR1020147019092A patent/KR20140103144A/ko not_active Application Discontinuation
- 2012-12-10 WO PCT/EP2012/074957 patent/WO2013087569A2/fr unknown
- 2012-12-10 RU RU2014128669A patent/RU2607198C2/ru active
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN86107895A (zh) * | 1983-03-18 | 1988-06-01 | 戴尔·戈登·琼斯 | 从燃烧气体排除氮和硫的氧化物之方法和装置 |
| US20080066493A1 (en) * | 2004-07-12 | 2008-03-20 | Cornelis Buijs | Treating Liquefied Natural Gas |
| CN101631934A (zh) * | 2007-01-31 | 2010-01-20 | 尤米科尔股份公司及两合公司 | 贫燃发动机排气装置中的碳烟过滤器的再生方法，以及用于贫燃发动机的排气装置 |
| DE102007010032A1 (de) * | 2007-03-01 | 2008-09-04 | Linde Ag | Verfahren zum Abtrennen von Stickstoff aus verflüssigtem Erdgas |
| US20110239701A1 (en) * | 2008-11-03 | 2011-10-06 | Sander Kaart | Method of rejecting nitrogen from a hydrocarbon stream to provide a fuel gas stream and an apparatus therefor |
| WO2011009832A2 (fr) * | 2009-07-21 | 2011-01-27 | Shell Internationale Research Maatschappij B.V. | Procédé pour le traitement d'un courant d'hydrocarbure à plusieurs phases et appareil correspondant |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110114627A (zh) * | 2016-10-28 | 2019-08-09 | 乔治洛德方法研究和开发液化空气有限公司 | 用于低温分离氢气和一氧化碳的混合物的方法 |
| CN110114627B (zh) * | 2016-10-28 | 2022-02-25 | 乔治洛德方法研究和开发液化空气有限公司 | 用于低温分离氢气和一氧化碳的混合物的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20140103144A (ko) | 2014-08-25 |
| CA2858152A1 (fr) | 2013-06-20 |
| WO2013087569A2 (fr) | 2013-06-20 |
| EP2791601A2 (fr) | 2014-10-22 |
| AU2012350742B2 (en) | 2015-08-20 |
| EP2791601B1 (fr) | 2020-06-24 |
| RU2014128669A (ru) | 2016-02-10 |
| RU2607198C2 (ru) | 2017-01-10 |
| WO2013087569A3 (fr) | 2014-05-01 |
| JP2015501917A (ja) | 2015-01-19 |
| MY172968A (en) | 2019-12-16 |
| AU2012350742A1 (en) | 2014-05-22 |
| CA2858152C (fr) | 2020-04-14 |
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