CN103980544B - A kind of fire-retardant non-metallic powder - Google Patents
A kind of fire-retardant non-metallic powder Download PDFInfo
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- CN103980544B CN103980544B CN201410149508.8A CN201410149508A CN103980544B CN 103980544 B CN103980544 B CN 103980544B CN 201410149508 A CN201410149508 A CN 201410149508A CN 103980544 B CN103980544 B CN 103980544B
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- flame retardant
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Abstract
The invention discloses a kind of fire-retardant non-metallic powder, it is to be made by the raw material of following weight parts: neatly stone flour 50-55, diatomite 10-20, compound flame retardant 15-20, oyster shell whiting 10-15, triethyl phosphate 1-2, tartaric acid 0.8-1.2, dioctyl adipate 1-2, silane coupler DL1712-4, alcohol ether glucoside 1-2, magnesium naphthenate 1-2, barium mahogany sulfonate 0.3-0.5; The present invention fills a prescription rationally, and preparation is simple, by making adding of compound flame retardant the present invention have good fire resistance, can be widely used in the field such as plastic reinforcing agent, coating filler.
Description
Technical field
The present invention relates to multiple modified non-metallic powder field, is exactly a kind of fire-retardant non-metallic powder.
Background technology
The material that nonmetallic materials are made up of nonmetalloid or compound. Since 19th century, along with producing and scienceThe progress of technology, especially inorganic chemistry and organic chemistry industrial expansion, the mankind taking natural mineral, plant, oil etc. asRaw material, manufactures and has synthesized many novel metalloid materials, as cement, Delanium, special cermacis, synthetic rubber, synthetic treeFat (plastics), synthetic fibers etc. These nonmetallic materials are because having the performance of various excellences, are natural nonmetallic materials and certainA little metal materials can't be obtained, thereby the purposes in the modern industry constantly expands, and develops rapidly.
Non-metallic powder is widely used in the industry such as coating, plastics, papermaking, printing-ink, chemical fibre, rubber, cosmetics.
Summary of the invention
The object of the present invention is to provide a kind of fire-retardant non-metallic powder.
Above-mentioned purpose realizes by following scheme:
A kind of fire-retardant non-metallic powder, is characterized in that: it is to be made by the raw material of following weight parts: neatly stone flour 50-55, diatomite 10-20, compound flame retardant 15-20, oyster shell whiting 10-15, triethyl phosphate 1-2, tartaric acid 0.8-1.2, adipic acidDioctyl ester 1-2, silane coupler DL1712-4, alcohol ether glucoside 1-2, magnesium naphthenate 1-2, barium mahogany sulfonate 0.3-0.5;
Described compound flame retardant is made by the raw material of following weight parts:
Silane coupling agent KH550 1-2, imvite 50-60, Nano Silver 1-2, magnesium hydroxide 40-50, cobalt aluminate 2-5, lemonLemon acid 1-2, lauryl sodium sulfate 2-4, encapsulated red phosphorus 4-8, urea 1-2;
The preparation method of described compound flame retardant is:
Urea, imvite add in suitable quantity of water stirs 20-30 minute, after oven dry, after all the other raw material blendings, in 40-50 DEG CLower stirring 30-50 minute, to obtain final product.
The preparation method of described fire-retardant non-metallic powder, is characterized in that: comprise the following steps:
(1) neatly stone flour is added in high-speed mixer, then add respectively diatomite and compound flame retardant, stir and riseTemperature, in the time that temperature reaches 70-80 DEG C, is incubated 10-20 minute and anhydrates point to dry;
(2) add again alcohol ether glucoside, triethyl phosphate, barium mahogany sulfonate, be warming up to 140-150 DEG C, then be incubated 8-12 and divideClock, is cooled to 60-70 DEG C, and insulation 10-20 minute, then adds all the other raw materials, after stirring, cooling and get final product.
Beneficial effect of the present invention is: the present invention fills a prescription rationally, and preparation is simple, by adding of compound flame retardantEnter to make the present invention to there is good fire resistance, can be widely used in the field such as plastic reinforcing agent, coating filler.
Detailed description of the invention
A kind of fire-retardant non-metallic powder, it is to be made by the raw material of following weight kg: neatly stone flour 55, diatomite 20, multipleJoin fire retardant 20, oyster shell whiting 15, triethyl phosphate 2, tartaric acid 1.2, dioctyl adipate 2, silane coupler DL1714, alcoholEther glucosides 2, magnesium naphthenate 2, barium mahogany sulfonate 0.5;
Described compound flame retardant is made by the raw material of following weight kg:
Silane coupling agent KH550 2, imvite 60, Nano Silver 2, magnesium hydroxide 50, cobalt aluminate 5, citric acid 2, dodecaneBase sodium sulphate 4, encapsulated red phosphorus 8, urea 2;
The preparation method of described compound flame retardant is:
Urea, imvite add in suitable quantity of water stirs 30 minutes, after oven dry, after all the other raw material blendings, at 50 DEG C, stirs50 minutes, to obtain final product.
The preparation method of described fire-retardant non-metallic powder, comprises the following steps:
(1) neatly stone flour is added in high-speed mixer, then add respectively diatomite and compound flame retardant, stir and riseTemperature, in the time that temperature reaches 80 DEG C, is incubated 20 minutes and anhydrates point to dry;
(2) add again alcohol ether glucoside, triethyl phosphate, barium mahogany sulfonate, be warming up to 150 DEG C, then be incubated 12 minutes, coolingTo 70 DEG C, be incubated 20 minutes, then add all the other raw materials, after stirring, cooling and get final product.
Add the prepared plastics of the present embodiment, its flame retardant rating reaches V1.
Claims (2)
1. a fire-retardant non-metallic powder, is characterized in that: it is to be made by the raw material of following weight parts: neatly stone flour 50-55, diatomite 10-20, compound flame retardant 15-20, oyster shell whiting 10-15, triethyl phosphate 1-2, tartaric acid 0.8-1.2, adipic acidDioctyl ester 1-2, silane coupler DL1712-4, alcohol ether glucoside 1-2, magnesium naphthenate 1-2, barium mahogany sulfonate 0.3-0.5;
Described compound flame retardant is made by the raw material of following weight parts:
Silane coupling agent KH550 1-2, imvite 50-60, Nano Silver 1-2, magnesium hydroxide 40-50, cobalt aluminate 2-5, citric acid1-2, lauryl sodium sulfate 2-4, encapsulated red phosphorus 4-8, urea 1-2;
The preparation method of described compound flame retardant is:
Urea, imvite add in suitable quantity of water stirs 20-30 minute, after oven dry, after all the other raw material blendings, at 40-50 DEG C, stirsMix 30-50 minute, to obtain final product.
2. a preparation method for fire-retardant non-metallic powder according to claim 1, is characterized in that: comprise following stepRapid:
(1) neatly stone flour is added in high-speed mixer, then add respectively diatomite and compound flame retardant, stir and heat up, whenWhen temperature reaches 70-80 DEG C, be incubated 10-20 minute and anhydrate point to dry;
(2) add again alcohol ether glucoside, triethyl phosphate, barium mahogany sulfonate, be warming up to 140-150 DEG C, then be incubated 8-12 minute, fallTemperature is to 60-70 DEG C, and insulation 10-20 minute, then adds all the other raw materials, after stirring, cooling and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410149508.8A CN103980544B (en) | 2014-04-15 | 2014-04-15 | A kind of fire-retardant non-metallic powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410149508.8A CN103980544B (en) | 2014-04-15 | 2014-04-15 | A kind of fire-retardant non-metallic powder |
Publications (2)
| Publication Number | Publication Date |
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| CN103980544A CN103980544A (en) | 2014-08-13 |
| CN103980544B true CN103980544B (en) | 2016-05-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410149508.8A Active CN103980544B (en) | 2014-04-15 | 2014-04-15 | A kind of fire-retardant non-metallic powder |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108727668A (en) * | 2018-06-04 | 2018-11-02 | 芜湖同达新材料科技有限公司 | A kind of composite modified halogen-free flameproof pulvis and its preparation method and application |
| CN108912444A (en) * | 2018-06-04 | 2018-11-30 | 芜湖同达新材料科技有限公司 | A kind of environment friendly halogen-free fireproof master batch and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093525A (en) * | 2010-12-30 | 2011-06-15 | 苏州科技学院 | Method for preparing macromolecular flame retardant containing hydrotalcite-like compounds |
| CN102604246A (en) * | 2012-03-19 | 2012-07-25 | 上海锦湖日丽塑料有限公司 | Efficient-inflame-retardance styrene resin composition |
| CN102766471A (en) * | 2012-03-29 | 2012-11-07 | 广东省宜华木业股份有限公司 | Preparation method of mesoporous silica nanometer composite flame retardant |
| CN103074077A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Composite flame retardant |
| CN103265725A (en) * | 2013-06-13 | 2013-08-28 | 盐城工学院 | Low-smoke aluminum hypophosphite compounded fire retardant and preparation method thereof |
-
2014
- 2014-04-15 CN CN201410149508.8A patent/CN103980544B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093525A (en) * | 2010-12-30 | 2011-06-15 | 苏州科技学院 | Method for preparing macromolecular flame retardant containing hydrotalcite-like compounds |
| CN102604246A (en) * | 2012-03-19 | 2012-07-25 | 上海锦湖日丽塑料有限公司 | Efficient-inflame-retardance styrene resin composition |
| CN102766471A (en) * | 2012-03-29 | 2012-11-07 | 广东省宜华木业股份有限公司 | Preparation method of mesoporous silica nanometer composite flame retardant |
| CN103074077A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Composite flame retardant |
| CN103265725A (en) * | 2013-06-13 | 2013-08-28 | 盐城工学院 | Low-smoke aluminum hypophosphite compounded fire retardant and preparation method thereof |
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| CN103980544A (en) | 2014-08-13 |
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