CN103980544A - Fire retardation non-metal powder - Google Patents
Fire retardation non-metal powder Download PDFInfo
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- CN103980544A CN103980544A CN201410149508.8A CN201410149508A CN103980544A CN 103980544 A CN103980544 A CN 103980544A CN 201410149508 A CN201410149508 A CN 201410149508A CN 103980544 A CN103980544 A CN 103980544A
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Abstract
The present invention discloses fire retardation non-metal powder, which is prepared from the following raw materials by weight: 50-55 parts of hydrotalcite powder, 10-20 parts of diatomite, 15-20 parts of a compound fire retardation agent, 10-15 parts of shell powder, 1-2 parts of triethyl phosphate, 0.8-1.2 parts of tartaric acid, 1-2 parts of dioctyl adipate, 2-4 parts of a silane coupling agent DL171, 1-2 parts of alkylethoxyglucoside, 1-2 parts of magnesium naphthenate, and 0.3-0.5 part of barium petroleum sulfonate. According to the present invention, the formula is reasonable, the preparation process is simple and easy-performing, and the fire retardation non-metal powder has a good fire retardation performance through addition of the compound fire retardation agent, and can be widely applied in the fields of plastic reinforcing agents, coating material fillers and the like.
Description
Technical field
The present invention relates to multiple modified non-metallic powder field, is exactly a kind of fire-retardant non-metallic powder.
Background technology
The material that non-metallic material are made up of non-metallic element or compound.Since 19th century, along with producing and scientific and technical progress, especially inorganic chemistry and organic chemistry industrial expansion, the mankind are taking natural mineral, plant, oil etc. as raw material, manufacture and synthesized many novel metalloid materials, as cement, synthetic graphite, special cermacis, synthetic rubber, synthetic resins (plastics), synthon etc.These non-metallic material are because having the performance of various excellences, for natural non-metallic material and some metallic substance can't be obtained, thereby the purposes in the modern industry constantly expands, and develops rapidly.
Non-metallic powder is widely used in the industry such as coating, plastics, papermaking, printing-ink, chemical fibre, rubber, makeup.
Summary of the invention
The object of the present invention is to provide a kind of fire-retardant non-metallic powder.
Above-mentioned purpose realizes by following scheme:
A kind of fire-retardant non-metallic powder, it is characterized in that: it is to be made by the raw material of following weight parts: neatly stone flour 50-55, diatomite 10-20, compound flame retardant 15-20, oyster shell whiting 10-15, triethyl phosphate 1-2, tartrate 0.8-1.2, Octyl adipate 1-2, silane coupling agent DL171 2-4, alcohol ether glucoside 1-2, magnesium naphthenate 1-2, barium mahogany sulfonate 0.3-0.5;
Described compound flame retardant is made by the raw material of following weight parts:
Silane coupling agent KH550 1-2, polynite 50-60, nanometer silver 1-2, magnesium hydroxide 40-50, Leyden blue 2-5, citric acid 1-2, sodium lauryl sulphate 2-4, encapsulated red phosphorus 4-8, urea 1-2;
The preparation method of described compound flame retardant is:
Urea, polynite add in suitable quantity of water stirs 20-30 minute, after oven dry, after all the other raw material blendings, at 40-50 DEG C, stirs 30-50 minute, to obtain final product.
The preparation method of described fire-retardant non-metallic powder, is characterized in that: comprise the following steps:
(1) neatly stone flour is added in high-speed mixer, then add respectively diatomite and compound flame retardant, stir and heat up, in the time that temperature reaches 70-80 DEG C, be incubated 10-20 minute and anhydrate point to dry;
(2) add alcohol ether glucoside, triethyl phosphate, barium mahogany sulfonate again, be warming up to 140-150 DEG C, then be incubated 8-12 minute, be cooled to 60-70 DEG C, insulation 10-20 minute, then adds all the other raw materials, after stirring, cooling and get final product.
Beneficial effect of the present invention is: the present invention fills a prescription rationally, and preparation is simple, by making adding of compound flame retardant the present invention have good flame retardant properties, can be widely used in the field such as plastic reinforcing agent, coating weighting agent.
Embodiment
A kind of fire-retardant non-metallic powder, it is to be made by the raw material of following weight kg: neatly stone flour 55, diatomite 20, compound flame retardant 20, oyster shell whiting 15, triethyl phosphate 2, tartrate 1.2, Octyl adipate 2, silane coupling agent DL171 4, alcohol ether glucoside 2, magnesium naphthenate 2, barium mahogany sulfonate 0.5;
Described compound flame retardant is made by the raw material of following weight kg:
Silane coupling agent KH550 2, polynite 60, nanometer silver 2, magnesium hydroxide 50, Leyden blue 5, citric acid 2, sodium lauryl sulphate 4, encapsulated red phosphorus 8, urea 2;
The preparation method of described compound flame retardant is:
Urea, polynite add in suitable quantity of water stirs 30 minutes, after oven dry, after all the other raw material blendings, stirs 50 minutes at 50 DEG C, to obtain final product.
The preparation method of described fire-retardant non-metallic powder, comprises the following steps:
(1) neatly stone flour is added in high-speed mixer, then add respectively diatomite and compound flame retardant, stir and heat up, in the time that temperature reaches 80 DEG C, be incubated 20 minutes and anhydrate point to dry;
(2) add again alcohol ether glucoside, triethyl phosphate, barium mahogany sulfonate, be warming up to 150 DEG C, then be incubated 12 minutes, be cooled to 70 DEG C, be incubated 20 minutes, then add all the other raw materials, after stirring, cooling and get final product.
Add the prepared plastics of the present embodiment, its flame retardant rating reaches V1.
Claims (2)
1. a fire-retardant non-metallic powder, it is characterized in that: it is to be made by the raw material of following weight parts: neatly stone flour 50-55, diatomite 10-20, compound flame retardant 15-20, oyster shell whiting 10-15, triethyl phosphate 1-2, tartrate 0.8-1.2, Octyl adipate 1-2, silane coupling agent DL171 2-4, alcohol ether glucoside 1-2, magnesium naphthenate 1-2, barium mahogany sulfonate 0.3-0.5;
Described compound flame retardant is made by the raw material of following weight parts:
Silane coupling agent KH550 1-2, polynite 50-60, nanometer silver 1-2, magnesium hydroxide 40-50, Leyden blue 2-5, citric acid 1-2, sodium lauryl sulphate 2-4, encapsulated red phosphorus 4-8, urea 1-2;
The preparation method of described compound flame retardant is:
Urea, polynite add in suitable quantity of water stirs 20-30 minute, after oven dry, after all the other raw material blendings, at 40-50 DEG C, stirs 30-50 minute, to obtain final product.
2. a preparation method for fire-retardant non-metallic powder according to claim 1, is characterized in that: comprise the following steps:
(1) neatly stone flour is added in high-speed mixer, then add respectively diatomite and compound flame retardant, stir and heat up, in the time that temperature reaches 70-80 DEG C, be incubated 10-20 minute and anhydrate point to dry;
(2) add alcohol ether glucoside, triethyl phosphate, barium mahogany sulfonate again, be warming up to 140-150 DEG C, then be incubated 8-12 minute, be cooled to 60-70 DEG C, insulation 10-20 minute, then adds all the other raw materials, after stirring, cooling and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410149508.8A CN103980544B (en) | 2014-04-15 | 2014-04-15 | A kind of fire-retardant non-metallic powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410149508.8A CN103980544B (en) | 2014-04-15 | 2014-04-15 | A kind of fire-retardant non-metallic powder |
Publications (2)
| Publication Number | Publication Date |
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| CN103980544A true CN103980544A (en) | 2014-08-13 |
| CN103980544B CN103980544B (en) | 2016-05-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410149508.8A Active CN103980544B (en) | 2014-04-15 | 2014-04-15 | A kind of fire-retardant non-metallic powder |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108727668A (en) * | 2018-06-04 | 2018-11-02 | 芜湖同达新材料科技有限公司 | A kind of composite modified halogen-free flameproof pulvis and its preparation method and application |
| CN108912444A (en) * | 2018-06-04 | 2018-11-30 | 芜湖同达新材料科技有限公司 | A kind of environment friendly halogen-free fireproof master batch and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093525A (en) * | 2010-12-30 | 2011-06-15 | 苏州科技学院 | Method for preparing macromolecular flame retardant containing hydrotalcite-like compounds |
| CN102604246A (en) * | 2012-03-19 | 2012-07-25 | 上海锦湖日丽塑料有限公司 | Efficient-inflame-retardance styrene resin composition |
| CN102766471A (en) * | 2012-03-29 | 2012-11-07 | 广东省宜华木业股份有限公司 | Preparation method of mesoporous silica nanometer composite flame retardant |
| CN103074077A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Composite flame retardant |
| CN103265725A (en) * | 2013-06-13 | 2013-08-28 | 盐城工学院 | Low-smoke aluminum hypophosphite compounded fire retardant and preparation method thereof |
-
2014
- 2014-04-15 CN CN201410149508.8A patent/CN103980544B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102093525A (en) * | 2010-12-30 | 2011-06-15 | 苏州科技学院 | Method for preparing macromolecular flame retardant containing hydrotalcite-like compounds |
| CN102604246A (en) * | 2012-03-19 | 2012-07-25 | 上海锦湖日丽塑料有限公司 | Efficient-inflame-retardance styrene resin composition |
| CN102766471A (en) * | 2012-03-29 | 2012-11-07 | 广东省宜华木业股份有限公司 | Preparation method of mesoporous silica nanometer composite flame retardant |
| CN103074077A (en) * | 2012-12-30 | 2013-05-01 | 胶州市富田化工有限公司 | Composite flame retardant |
| CN103265725A (en) * | 2013-06-13 | 2013-08-28 | 盐城工学院 | Low-smoke aluminum hypophosphite compounded fire retardant and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108727668A (en) * | 2018-06-04 | 2018-11-02 | 芜湖同达新材料科技有限公司 | A kind of composite modified halogen-free flameproof pulvis and its preparation method and application |
| CN108912444A (en) * | 2018-06-04 | 2018-11-30 | 芜湖同达新材料科技有限公司 | A kind of environment friendly halogen-free fireproof master batch and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103980544B (en) | 2016-05-25 |
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