CN103979932A - Black ceramic plate and making method thereof - Google Patents
Black ceramic plate and making method thereof Download PDFInfo
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- CN103979932A CN103979932A CN201410192421.9A CN201410192421A CN103979932A CN 103979932 A CN103979932 A CN 103979932A CN 201410192421 A CN201410192421 A CN 201410192421A CN 103979932 A CN103979932 A CN 103979932A
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Abstract
The invention discloses a black ceramic plate and a making method thereof. Raw materials composing the black ceramic plate comprise bentonite, kaolin, clay, vanadium tailings, granite stone wastes, manganese mine and a plasticizer. The making method of the black ceramic plate comprises the following steps: 1, crushing all the raw materials, and mixing to form a raw material mixture; 2, mixing the raw materials with water in a stirrer to prepare a wet material; 3, sending the wet material to a pug mill, and mixing to prepare a mud material; 4, sending the mud material to a vacuum extruder, molding through a die mouth, and cutting to make a wet green body; 5, drying the wet green body to make a dry green body; and 6, sending the dry green body to a calcining kiln, and calcining to make the black ceramic plate. In the invention, the low-cost steel enterprise waste vanadium tailings are used as a main raw material and a chromophoric raw material, low-cost clay and granite stone industry waste powder are added, the black ceramic plate with different hues by adding different amounts of the clay and the powder, and the black ceramic plate has the advantages of high quality, low cost and low energy consumption.
Description
Technical field
The present invention relates to a kind of black pottery plate and preparation method thereof.
Background technology
In the materials and manufacture craft of existing black pottery plate, mainly there is following defect: the one, need in raw material, add cobalt black or without cobalt black ceramic pigment, addition is larger, thereby cause cost very high; The 2nd, the iron-holder of the basic raw materials such as requirement clay, feldspar is low, causes the raw-material price of plinth high, has correspondingly increased production cost; The 3rd, firing temperature is up to more than 1150 DEG C, and energy consumption is large; Above 3 cause the market sale price of existing black pottery plate high.
Summary of the invention
One of object of the present invention is to provide the black pottery plate that a kind of production cost is low.
In order to realize foregoing invention object, the technical solution used in the present invention is as follows:
Technical scheme one: the raw material composition of making black pottery plate comprises by weight: wilkinite 10-20 part, kaolin 10-20 part, clay 10-20 part, tailings in vanadium extraction 25-60 part, granite building material waste residue 20-30 part, manganese ore 0.1-3 part, softening agent 0.1-3 part.
Technical scheme two: the raw material composition of making black pottery plate comprises by weight: 15 parts of wilkinites, 12 parts of kaolin, 17 parts of clays, 50 parts of tailings in vanadium extraction, 21 parts, granite building material waste residue, 1 part of manganese ore, 0.5 part, softening agent.
Two of object of the present invention is to provide a kind of preparation method of black pottery plate.
In order to realize foregoing invention object, processing method of the present invention comprises the following steps:
(1), by proportioning, get the each raw material except softening agent described in technique scheme one or two and by more than each raw material pulverizing to 250 order, the then each raw material formation mixing raw material after co-grinding;
(2) account for the proportion relation of the 15.5-18.5% of mixing raw material quality by water, mixing raw material, softening agent and water are mixed in stirrer, thereby make wet feed;
(3) above-mentioned wet feed is sent into pug mill carry out mixing, thereby make the pug that plasticity index is 8-12;
(4) above-mentioned pug is sent into vacuum-extruder and carry out moulding through die orifice, then cut into the specification that meets design requirements, thereby make wet base substrate;
(5) will wet base substrate under temperature 120-150 DEG C condition, dry 4-8 hour, thus make dry tenacity and reach the dry body body of 1.5-3.5Mpa;
(6) dry body body is sent in calcining kiln, under temperature 1100-1140 DEG C condition, after 2.5-5 hour burns till, just made black pottery plate.
Described in the present invention in raw material, softening agent is that modified starch is the binding agent that is dry mixed of main component, for example can adopt this product of Guangdong Feng Lin glaze company production, can certainly adopt the like product of other producer, softening agent plays increases plasticity and lubricated effect; Wilkinite, kaolin, clay, granite building material waste residue are pottery board substrate material; Tailings in vanadium extraction, manganese ore are body material and chromonic materials.
The equipment such as the present invention's stirrer used, pug mill and pulverizer, are all currently available products.
The invention has the advantages that: utilize low cost iron and steel enterprise waste material tailings in vanadium extraction for main raw material and as color development raw material, add the waste residue powder of clay and granite building material industry cheaply, the black pottery plate that can produce different form and aspect according to addition difference, quality product is high, cost is low, energy consumption is low.
Embodiment
Further illustrate by the following examples technical solution of the present invention; these embodiment are only for representing in detail technical conceive of the present invention and exploitativeness thereof; be not limiting the scope of the invention, the equivalence replacement that utilizes the technology of the present invention to conceive to make and accommodation are still within protection scope of the present invention.
Embodiment 1
1. proportioning raw materials
Making the raw material composition of black pottery plate counts by weight: 15 parts of wilkinites, 12 parts of kaolin, 17 parts of clays, 50 parts of tailings in vanadium extraction, 21 parts, granite building material waste residue, 1 part of manganese ore, 0.5 part, softening agent.
2. preparation method
(1), by proportioning, get each raw material except softening agent and by each raw material pulverizing to 250 order, then the each raw material after co-grinding forms mixing raw material;
(2) account for 15.5% proportion relation of mixing raw material quality by water, mixing raw material, softening agent and water are mixed in stirrer, thereby make wet feed;
(3) above-mentioned wet feed being sent into pug mill and carried out mixingly, is 9 pug thereby make plasticity index;
(4) above-mentioned pug is sent into vacuum-extruder and carry out moulding through die orifice, then cut into the specification that meets design requirements, thereby make wet base substrate;
(5) will wet base substrate under 120 DEG C of conditions of temperature, dry 8 hours, thus make dry tenacity and reach the dry body body of 2.4Mpa;
(6) dry body body is sent in calcining kiln, under 1100 DEG C of conditions of temperature, after 5 hours burn till, just made black pottery plate.
Embodiment 2
1. proportioning raw materials
Making the raw material composition of black pottery plate counts by weight: 10 parts of wilkinites, 10 parts of kaolin, 10 parts of clays, 25 parts of tailings in vanadium extraction, 20 parts, granite building material waste residue, 0.1 part of manganese ore, 0.1 part, softening agent.
2. preparation method
(1), by proportioning, get each raw material except softening agent and by each raw material pulverizing to 300 order, then the each raw material after co-grinding forms mixing raw material;
(2) account for 16.5% proportion relation of mixing raw material quality by water, mixing raw material, softening agent and water are mixed in stirrer, thereby make wet feed;
(3) above-mentioned wet feed being sent into pug mill and carried out mixingly, is 10 pug thereby make plasticity index;
(4) above-mentioned pug is sent into vacuum-extruder and carry out moulding through die orifice, then cut into the specification that meets design requirements, thereby make wet base substrate;
(5) will wet base substrate under 130 DEG C of conditions of temperature, dry 7 hours, thus make dry tenacity and reach the dry body body of 2.6Mpa;
(6) dry body body is sent in calcining kiln, under 1110 DEG C of conditions of temperature, after 4 hours burn till, just made black pottery plate.
Embodiment 3
1. proportioning raw materials
Making the raw material composition of black pottery plate counts by weight: 17 parts of wilkinites, 16 parts of kaolin, 13 parts of clays, 40 parts of tailings in vanadium extraction, 25 parts, granite building material waste residue, 1.5 parts of manganese ores, 1.5 parts, softening agent.
2. preparation method
(1), by proportioning, get each raw material except softening agent and by each raw material pulverizing to 350 order, then the each raw material after co-grinding forms mixing raw material;
(2) account for 17.5% proportion relation of mixing raw material quality by water, mixing raw material, softening agent and water are mixed in stirrer, thereby make wet feed;
(3) above-mentioned wet feed being sent into pug mill and carried out mixingly, is 11 pug thereby make plasticity index;
(4) above-mentioned pug is sent into vacuum-extruder and carry out moulding through die orifice, then cut into the specification that meets design requirements, thereby make wet base substrate;
(5) will wet base substrate under 140 DEG C of conditions of temperature, dry 5.5 hours, thus make dry tenacity and reach the dry body body of 2.8Mpa;
(6) dry body body is sent in calcining kiln, under 1130 DEG C of conditions of temperature, after 3 hours burn till, just made black pottery plate.
Embodiment 4
1. proportioning raw materials
Making the raw material composition of black pottery plate counts by weight: 20 parts of wilkinites, 20 parts of kaolin, 20 parts of clays, 60 parts of tailings in vanadium extraction, 30 parts, granite building material waste residue, 3 parts of manganese ores, 3 parts, softening agent.
2. preparation method
(1), by proportioning, get each raw material except softening agent and by each raw material pulverizing to 400 order, then the each raw material after co-grinding forms mixing raw material;
(2) account for 18.5% proportion relation of mixing raw material quality by water, mixing raw material, softening agent and water are mixed in stirrer, thereby make wet feed;
(3) above-mentioned wet feed being sent into pug mill and carried out mixingly, is 12 pug thereby make plasticity index;
(4) above-mentioned pug is sent into vacuum-extruder and carry out moulding through die orifice, then cut into the specification that meets design requirements, thereby make wet base substrate;
(5) will wet base substrate under 150 DEG C of conditions of temperature, dry 4 hours, thus make dry tenacity and reach the dry body body of 3.2Mpa;
(6) dry body body is sent in calcining kiln, under 1140 DEG C of conditions of temperature, after 2.5 hours burn till, just made black pottery plate.
The black pottery plate of making thickness 18mm by the batching of above-described embodiment 1-4 and method, then carries out testing performance index, and test result is in table 1.
Table 1 testing performance index result table
From the performance index of upper table, can find out, black pottery plate provided by the present invention has reached the requirement of national standard completely; That is to say, the present invention's plate of making pottery taking waste materials such as tailings in vanadium extraction and granite building material waste residues as main material production black, has not only reduced production cost, and has solved the difficult and problem of environmental pollution that brings of above-mentioned waste disposal.
Claims (3)
1. a black pottery plate, is characterized in that its raw material composition comprises by weight: wilkinite 10-20 part, kaolin 10-20 part, clay 10-20 part, tailings in vanadium extraction 25-60 part, granite building material waste residue 20-30 part, manganese ore 0.1-3 part, softening agent 0.1-3 part.
2. black pottery plate according to claim 1, is characterized in that its raw material composition comprises by weight: 15 parts of wilkinites, 12 parts of kaolin, 17 parts of clays, 50 parts of tailings in vanadium extraction, 21 parts, granite building material waste residue, 1 part of manganese ore, 0.5 part, softening agent.
3. a method of preparing the black pottery plate described in claim 1 or 2, is characterized in that comprising the following steps:
(1), by proportioning, get the each raw material except softening agent described in claim 1 or 2 and by more than each raw material pulverizing to 250 order, the then each raw material formation mixing raw material after co-grinding;
(2) account for the proportion relation of the 15.5-18.5% of mixing raw material quality by water, mixing raw material, softening agent and water are mixed in stirrer, thereby make wet feed;
(3) above-mentioned wet feed is sent into pug mill carry out mixing, thereby make the pug that plasticity index is 8-12;
(4) above-mentioned pug is sent into vacuum-extruder and carry out moulding through die orifice, then cut into the specification that meets design requirements, thereby make wet base substrate;
(5) will wet base substrate under temperature 120-150 DEG C condition, dry 4-8 hour, thus make dry tenacity and reach the dry body body of 1.5-3.5Mpa;
(6) dry body body is sent in calcining kiln, under temperature 1100-1140 DEG C condition, after 2.5-5 hour burns till, just made black pottery plate.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106381972A (en) * | 2016-08-29 | 2017-02-08 | 瑞高(浙江)建筑系统有限公司 | Travertine gold ceramic plate |
| CN109231955A (en) * | 2018-08-10 | 2019-01-18 | 瑞高（浙江）环保新材料科技有限公司 | The wear-resisting ceramic plate of a kind of nanometer of dry granular and preparation process |
| CN110028304A (en) * | 2019-05-10 | 2019-07-19 | 成林山 | A kind of production method and its processing unit (plant) of rock pottery |
| CN110510991A (en) * | 2019-10-09 | 2019-11-29 | 山东雅美特新材料科技股份有限公司 | A kind of white ceramic plate and preparation method thereof |
| CN110521536A (en) * | 2019-08-14 | 2019-12-03 | 杨文明 | A kind of high-carbon ceramic plate for officinal dendrobium stem plantation |
| CN110590331A (en) * | 2019-10-10 | 2019-12-20 | 山东雅美特新材料科技股份有限公司 | Low-cost yellow ceramic plate and preparation method thereof |
| CN111410513A (en) * | 2020-04-20 | 2020-07-14 | 福建省乐普陶板制造有限公司 | Thin microporous composite ceramic plate with high porosity and preparation method thereof |
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| CN101718131A (en) * | 2009-12-01 | 2010-06-02 | 西安交通大学 | Ceramic plate for curtain wall decoration and preparation method thereof |
| CN102910892A (en) * | 2012-09-28 | 2013-02-06 | 新嘉理（江苏）陶瓷有限公司 | Black ceramic plate prepared by natural minerals and extracted vanadium tailings and preparation method of black ceramic plate |
| CN103011876A (en) * | 2012-11-23 | 2013-04-03 | 佛山欧神诺陶瓷股份有限公司 | Heat-insulation foamed ceramic plate and preparation method thereof |
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2014
- 2014-05-08 CN CN201410192421.9A patent/CN103979932B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101718131A (en) * | 2009-12-01 | 2010-06-02 | 西安交通大学 | Ceramic plate for curtain wall decoration and preparation method thereof |
| CN102910892A (en) * | 2012-09-28 | 2013-02-06 | 新嘉理（江苏）陶瓷有限公司 | Black ceramic plate prepared by natural minerals and extracted vanadium tailings and preparation method of black ceramic plate |
| CN103011876A (en) * | 2012-11-23 | 2013-04-03 | 佛山欧神诺陶瓷股份有限公司 | Heat-insulation foamed ceramic plate and preparation method thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106381972A (en) * | 2016-08-29 | 2017-02-08 | 瑞高(浙江)建筑系统有限公司 | Travertine gold ceramic plate |
| CN109231955A (en) * | 2018-08-10 | 2019-01-18 | 瑞高（浙江）环保新材料科技有限公司 | The wear-resisting ceramic plate of a kind of nanometer of dry granular and preparation process |
| CN110028304A (en) * | 2019-05-10 | 2019-07-19 | 成林山 | A kind of production method and its processing unit (plant) of rock pottery |
| CN110521536A (en) * | 2019-08-14 | 2019-12-03 | 杨文明 | A kind of high-carbon ceramic plate for officinal dendrobium stem plantation |
| CN110510991A (en) * | 2019-10-09 | 2019-11-29 | 山东雅美特新材料科技股份有限公司 | A kind of white ceramic plate and preparation method thereof |
| CN110590331A (en) * | 2019-10-10 | 2019-12-20 | 山东雅美特新材料科技股份有限公司 | Low-cost yellow ceramic plate and preparation method thereof |
| CN111410513A (en) * | 2020-04-20 | 2020-07-14 | 福建省乐普陶板制造有限公司 | Thin microporous composite ceramic plate with high porosity and preparation method thereof |
| CN111410513B (en) * | 2020-04-20 | 2020-11-24 | 福建省乐普陶板制造有限公司 | Thin microporous composite ceramic plate with high porosity and preparation method thereof |
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| CN103979932B (en) | 2015-12-02 |
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Address after: 276800 Rizhao North Economic Development Zone, Shandong Patentee after: Shandong yameite new materials Polytron Technologies Inc. Address before: 262306 Shandong province Rizhao City Wulian County Industrial Park (Chao he Zhen Liu Guan Cun XI) Patentee before: ASIAN ELEGANT ADVANCE CERAMIC CO.,LTD. |
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Effective date of registration: 20230627 Address after: 221400 No. 9, industrial concentration zone, Qipan Town, Xinyi City, Xuzhou City, Jiangsu Province Patentee after: Jiangsu Pantai New Material Technology Co.,Ltd. Address before: 276800 Rizhao North Economic Development Zone, Shandong Province Patentee before: Shandong yameite new materials Polytron Technologies Inc. |
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