CN103976466A - Abelmoschus manilhot seed extractive and application in cigarette - Google Patents
Abelmoschus manilhot seed extractive and application in cigarette Download PDFInfo
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- CN103976466A CN103976466A CN201410212642.8A CN201410212642A CN103976466A CN 103976466 A CN103976466 A CN 103976466A CN 201410212642 A CN201410212642 A CN 201410212642A CN 103976466 A CN103976466 A CN 103976466A
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- cigarette
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- yellow hollyhock
- hollyhock seed
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Abstract
The invention relates to abelmoschus manilhot seed extractive. The extractive is obtained through the following steps: purified, dried and pulverized abelmoschus manilhot seeds are put into solvent for extraction, the extracting solution after extraction is subjected to decompression concentration and dried, and crude extractive is obtained; the crude extractive is dissolved in absolute ethyl alcohol and stands still for 4-12 hours at the temperature of 0 to minus 20 DEG C, and then the crude extractive is subjected to vacuum filtration or centrifugal separation, and the extracting solution is subjected to decompression concentration again, so that the abelmoschus manilhot seed extractive is obtained. As the abelmoschus manilhot seed extractive is added to cigarettes on the premises that the original property and processing technique of cigarettes are not changed, the fine degree and mild degree of smoke are remarkably improved, the impurity odor and irritation of smoke are reduced, the aroma volume and sensory comfort are improved, and the overall smoking quality of the cigarette is improved.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of yellow hollyhock seed extract and the application in cigarette as the tobacco aromatics using in cigarette additive thereof.
Background technology
In tobacco product, the fragrance of tobacco and jealous be vital.Along with the reduction of tar content in cigarette in recent years, low-coke tar cigarette exists smoke thin out, and fragrance weakens, and cigarette product style and features weakens, and is difficult to the problem of being accepted by consumer.So Harm reduction techniques fall burnt in, cigarette flavouring and to improve flue gas concentration be key issue.Perfuming cigarette is reinforced is one of core technology of tobacco industry, mode by flavoring and casing can make up the insufficient fragrance on cigarette tobacco leaf formulation, eliminates assorted gas, makes the cigarette perfume (or spice) of cigarette product more abundant, sufficient, thereby inhaling taste, smell on perfume (or spice) and there is individual style, strengthen the feature of cigarette product.
Vast territory and abundant resources in China, and floristics is various, and the composition of contained active ingredient also respectively has feature, for the exploitation of natural perfume material provides rich in natural resources.Can to effective ingredients in plant, extract separation by different modes method, and for the feature of cigarette product, extract is applied in cigarette with multi-form, to improving the overall quality of cigarette.
Sunset Abelmoschus Root [Abelmoschus manihot (Linn.) Medicus] has another name called gumbo, is the annual or herbaceos perennial of Malvaceae Abelmoschus.Originate in south China, existing extensively cultivation in all parts of the country, how for ornamental plantation.Sunset abelmoschus stem or bark hide fiber can and be manufactured synthetic cotton for fiber crops; Root contains mucilaginous substance, can make papermaking thickener; That its seed, root, flower can be done is medicinal (Feng Guomei. Chinese Plants will, the 49th volume the second fascicle, [M].Editorial board of Chinese Academy of Sciences's " Chinese Plants will ", Science Press: Beijing, 1984; P 53.).Seed is for constipation, difficult urination, oedema, lithangiuria, alactation.Yellow hollyhock seed is rich in fat oil, and more than content reaches 30 %, its main component is: linoleic acid, oleic acid, palmitic acid, stearic acid, leukotrienes etc., high linoleic acid low linolenic is the feature of yellow hollyhock seed fatty acid oil composition.In addition, yellow hollyhock seed also contain several amino acids and mineral element (Chen Jinling, etc. the research of yellow hollyhock seed form and chemical composition thereof [J] for Lin Wenqun, Chen Zhong. research and development of natural products. 2002,14 (3): 41-44.).
In recent years to the research of Sunset Abelmoschus Root mainly concentrate on chemical composition analysis and mensuration, pharmacological action, cultivate and breed, the aspect such as quality standard, less about the report of yellow hollyhock seed extract, and do not find its application in tobacco.
Summary of the invention
The object of the invention is to provide a kind of yellow hollyhock seed extract and the application in cigarette as tobacco aromatics using thereof, can improve suction quality and the sense organ comfort level of cigarette.
To achieve these goals, the present invention adopts following technical scheme:
Yellow hollyhock seed extract, it is obtained by following step: removal of impurities, oven dry the yellow hollyhock seed pulverized are put into solvent and extract, extract and finish rear extract reduced pressure concentration (in order to except desolventizing) and dry to obtain crude extract; Crude extract with after anhydrous alcohol solution in 0～-20 ℃ place 4～12 hours (freezing dewaxing, with so that insoluble matter fully separate out), then vacuum filtration or centrifugation, filtrate is reduced pressure concentration and get final product again.Gained yellow hollyhock seed extract is at room temperature yellow or brown color oily liquids or liquid extract, is soluble in ethanol.
The addition of absolute ethyl alcohol is preferably 5～10 times of crude extract weight.
Concrete, described solvent can be benzinum, ethyl acetate, 95 % ethanol or absolute ethyl alcohol etc., during extraction, solid-liquid ratio is preferably 1g:4～15ml.During extraction, can adopt following various ways to carry out: 1) Soxhlet is extracted 1～2 time, each 4～8 hours.2) heating and refluxing extraction is 1～2 time, each 1～3 hour.3) ultrasonic wave assisted extraction, ultrasonic frequency 30～60 kHz, power 100～1000 W, extraction times 30～60 min, extracts 25～50 ℃ of temperature.Also can adopt Microwave-assisted Extraction other this area routine techniques such as to get.
The application of above-mentioned yellow hollyhock seed extract in cigarette.Can be specifically: after yellow hollyhock seed ethanol for extract (preferably 95v% ethanol) dilution is dissolved, be evenly sprayed onto on pipe tobacco, after naturally drying or toasting, technique is made cigarette routinely; Wherein, the addition of yellow hollyhock seed extract is 0.01 of pipe tobacco weight～0.1 ‰.Can be used alone or be deployed into essence with other spices and use.
Innovative point of the present invention is: provide a kind of and take yellow hollyhock seed and be that raw material extracts the yellow hollyhock seed extract of preparation, and it is applied on cigarette as cigarette additive.Do not changing on the original performance of cigarette and processing technology basis, the yellow hollyhock seed extract adding can be coordinated with cigarette is fragrant, significantly improves the fine and smooth soften of flue gas, reduces assorted gas and the excitant of flue gas, improve the sense organ comfort level of perfume quantity and cigarette, improved the integral suction quality of cigarette.In addition, yellow hollyhock seed is rich and easy to get, and production technology is simple to operation, and production cost is lower, therefore has more actual production meaning and value.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is described further, but protection scope of the present invention is not limited to this.
embodiment 1
A kind of yellow hollyhock seed extract, it is obtained by following step: yellow hollyhock seed is removed after impurity, being placed in 40 ℃ of baking ovens dries, pulverize, then put into the ethyl acetate heating and refluxing extraction 2h of 8 times of yellow hollyhock seed weight, after extraction finishes, extract reduced pressure concentration is removed solvent ethyl acetate, then in vacuum drying chamber, dries and obtains crude extract.To the abundant stirring and dissolving of absolute ethyl alcohol of adding 8 times of crude extract weight in crude extract, in refrigerator-freezer-5 ℃ standing 12 hours.Vacuum filtration immediately after taking-up, filtrate is reduced pressure concentration and get final product again.
Take the above-mentioned yellow hollyhock seed extract of 0.1g and be diluted to 10g with 95v% ethanol, mix, standby.Pipe tobacco is evenly divided into two parts, and portion accounts for 0.02 ‰ of pipe tobacco weight by yellow hollyhock seed extract and on pipe tobacco, evenly sprays the ethanolic solution (being designated as test cigarette) containing yellow hollyhock seed extract; Another part pressed 0.02 ‰ of pipe tobacco weight and evenly sprayed 95 % ethanol pipe tobacco in contrast.Then, roll into respectively cigarette.Test cigarette and contrast cigarette are put into respectively to constant temperature (22 ± 1 ℃), constant humidity (relative humidity 60 ± 2 %) more than case inner equilibrium 48 h.Through the above judging panel of 7 people, smoke panel test, the results are shown in Table 1.As seen from Table 1: add the test cigarette after yellow hollyhock seed extract, flue gas free from extraneous odour, fragrance is coordinated, and perfume quantity increases, and assorted gas and excitant alleviate, and pleasant impression is comfortable, and whole sucking quality is improved.
The aesthetic quality of table 1, contrast cigarette and test cigarette contrasts smoking result
embodiment 2
A kind of yellow hollyhock seed extract, it is obtained by following step: yellow hollyhock seed is removed after impurity, being placed in 40 ℃ of baking ovens dries, pulverize, then put into the benzinum Soxhlet of 4 times of yellow hollyhock seed weight and extract 8h, after extraction finishes, extract reduced pressure concentration, except desolventizing benzinum, is then dried and is obtained crude extract in vacuum drying chamber.To the abundant stirring and dissolving of absolute ethyl alcohol of adding 10 times of crude extract weight in crude extract, in refrigerator-freezer-10 ℃ standing 12 hours.Vacuum filtration immediately after taking-up, filtrate is reduced pressure concentration and get final product again.
Take the above-mentioned yellow hollyhock seed extract of 0.1g and be diluted to 10g with 95v% ethanol, mix, standby.Pipe tobacco is evenly divided into two parts, and portion accounts for 0.01 ‰ of pipe tobacco weight by yellow hollyhock seed extract and on pipe tobacco, evenly sprays the ethanolic solution (being designated as test cigarette) containing yellow hollyhock seed extract; Another part pressed 0.01 ‰ of pipe tobacco weight and evenly sprayed 95 % ethanol pipe tobacco in contrast.Then, roll into respectively cigarette.Test cigarette and contrast cigarette are put into respectively to constant temperature (22 ± 1 ℃), constant humidity (relative humidity 60 ± 2 %) more than case inner equilibrium 48 h.Through the above judging panel of 7 people, smoke panel test, the results are shown in Table 2.As seen from Table 2: add the test cigarette after yellow hollyhock seed extract, flue gas free from extraneous odour, fragrance matter promotes, and perfume quantity increases, and assorted gas, excitant alleviate, and pleasant impression is clean.
The aesthetic quality of table 2, contrast cigarette and test cigarette contrasts smoking result
embodiment 3
A kind of yellow hollyhock seed extract, it is obtained by following step: yellow hollyhock seed is removed after impurity, being placed in 40 ℃ of baking ovens dries, pulverize, then put into 95 v% ethanol of 15 times of yellow hollyhock seed weight in the ultrasonic extraction of ultrasonic circulation extractor 50min, ultrasonic frequency 40 kHz, power 750 W, ultrasonic time and interval time are 2 s/1 s, mixing speed 1300 rpm.After extraction finishes, extract is evaporated to without alcohol taste, then in vacuum drying chamber, dries and obtains crude extract.To the abundant stirring and dissolving of absolute ethyl alcohol of adding 5 times of crude extract weight in crude extract, in refrigerator-freezer 0 ℃ standing 12 hours.Vacuum filtration immediately after taking-up, filtrate is evaporated to again without alcohol taste, obtains.
Take the above-mentioned yellow hollyhock seed extract of 0.020 g, with 95v % ethanol, be diluted to 1.000 g, mix.Adopting perfuming cigarette injector is 0.05 ‰ to injecting 2 μ L(perfuming amounts in every blank cigarette), be designated as test cigarette.Separately get the blank cigarette of part, inject 2 μ L 95v % ethanol cigarette in contrast for every.Test cigarette and contrast cigarette are put into respectively to constant temperature (22 ± 1 ℃), constant humidity (relative humidity 60 ± 2 %) more than case inner equilibrium 48 h.Through the above judging panel of 7 people, smoke panel test, the results are shown in Table 3.As seen from Table 3: add the test cigarette after yellow hollyhock seed extract: fragrance matter and perfume quantity all have lifting, assorted gas and excitant reduce, and flue gas exquisiteness is soft, has significantly improved the suction quality of cigarette.
The aesthetic quality of table 3, contrast cigarette and test cigarette contrasts smoking result
。
Claims (4)
1. yellow hollyhock seed extract, is characterized in that, by following step, is obtained: removal of impurities, oven dry the yellow hollyhock seed pulverized are put into solvent and extract, extract and finish rear extract reduced pressure concentration and dry to obtain crude extract; Crude extract is with placing 4～12 hours in 0～-20 ℃ after anhydrous alcohol solution, then vacuum filtration or centrifugation, and filtrate is reduced pressure concentration and get final product again.
2. yellow hollyhock seed extract as claimed in claim 1, is characterized in that, described solvent is benzinum, ethyl acetate, 95 % ethanol or absolute ethyl alcohols, and during extraction, solid-liquid ratio is 1g:4～15ml.
3. the application of yellow hollyhock seed extract in cigarette described in claim 1 or 2.
4. the application of yellow hollyhock seed extract in cigarette as claimed in claim 3, is characterized in that, after yellow hollyhock seed extract is dissolved with ethanol dilution, is evenly sprayed onto on pipe tobacco, and after naturally drying or toasting, technique is made cigarette routinely; Wherein, the addition of yellow hollyhock seed extract is 0.01 of pipe tobacco weight～0.1 ‰.
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| CN201410212642.8A CN103976466B (en) | 2014-05-20 | 2014-05-20 | The application of yellow hollyhock seed extract in cigarette |
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| CN201410212642.8A CN103976466B (en) | 2014-05-20 | 2014-05-20 | The application of yellow hollyhock seed extract in cigarette |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6174567A (en) * | 1984-09-19 | 1986-04-16 | 日本たばこ産業株式会社 | Flavor and smoking taste modifier for tobacco |
| CN101386634A (en) * | 2008-09-05 | 2009-03-18 | 周春晓 | Hyperin extraction method and preparation and use thereof |
| CN102319275A (en) * | 2011-09-15 | 2012-01-18 | 江苏苏中药业集团股份有限公司 | Flos abelmoschi manihot extract, preparation and preparation method thereof |
| CN102731597A (en) * | 2012-01-20 | 2012-10-17 | 天津中医药大学 | Abelmoschus manihot extract and novel application of chemical components thereof |
| CN103054041A (en) * | 2013-01-20 | 2013-04-24 | 湖南奇异生物科技有限公司 | Preparation process of okra extractive dry powder |
| CN103739732A (en) * | 2013-12-27 | 2014-04-23 | 新疆奇康哈博维药有限公司 | Method for extracting hollyhock seed polysaccharide |
-
2014
- 2014-05-20 CN CN201410212642.8A patent/CN103976466B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6174567A (en) * | 1984-09-19 | 1986-04-16 | 日本たばこ産業株式会社 | Flavor and smoking taste modifier for tobacco |
| CN101386634A (en) * | 2008-09-05 | 2009-03-18 | 周春晓 | Hyperin extraction method and preparation and use thereof |
| CN102319275A (en) * | 2011-09-15 | 2012-01-18 | 江苏苏中药业集团股份有限公司 | Flos abelmoschi manihot extract, preparation and preparation method thereof |
| CN102731597A (en) * | 2012-01-20 | 2012-10-17 | 天津中医药大学 | Abelmoschus manihot extract and novel application of chemical components thereof |
| CN103054041A (en) * | 2013-01-20 | 2013-04-24 | 湖南奇异生物科技有限公司 | Preparation process of okra extractive dry powder |
| CN103739732A (en) * | 2013-12-27 | 2014-04-23 | 新疆奇康哈博维药有限公司 | Method for extracting hollyhock seed polysaccharide |
Non-Patent Citations (3)
| Title |
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| 叶超凡等: ""烟用天然植物增香保润技术的研究进展"", 《农产品加工•学刊》 * |
| 叶超凡等: ""烟用天然植物增香保润技术的研究进展"", 《农产品加工•学刊》, no. 3, 22 May 2012 (2012-05-22) * |
| 李颖等: "桑葚多糖抗氧化作用的研究", 《中国酿造》 * |
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Address after: 450000 Yulin South Road, Henan, Zheng Dong, No. 16 South Road, Zhengzhou Patentee after: China Tobacco Henan Industrial Co., Ltd. Patentee after: Zhengzhou Tobacco Research Institute of CNTC Address before: 450000 Zhengzhou agricultural road, Henan, No. 29 Patentee before: China Tobacco Henan Industrial Co., Ltd. Patentee before: Zhengzhou Tobacco Research Institute of CNTC |