CN103948839A - Semen coicis prepared decoction pieces and preparation method thereof - Google Patents
Semen coicis prepared decoction pieces and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the field of traditional Chinese medicine decoction pieces, and particularly relates to semen coicis prepared decoction pieces and a preparation method thereof. The semen coicis prepared decoction pieces are prepared from semen coicis and edible oil. The preparation method of the semen coicis prepared decoction pieces comprises the following steps: cleaning the semen coicis, enabling the semen coicis to pass through 30-40 mesh sieve pores, and putting the semen coicis in 1-5L of drinking water, so that the semen coicis are swelled by soaking; fishing up the swelled semen coicis, draining off surface moisture of the semen coicis, adding the edible oil, uniformly stirring, steaming for 3-4 hours by using moderate heat till cores of the semen coicis are well-done, taking out the steamed semen coicis, airing till the surfaces of the semen coicis are bright and the semen coicis is transparent, putting the semen coicis in the sun, and slightly drying the semen coicis till the semen coicis has hardness by holding with hands; and frying for 2-5 minutes by using moderate heat till the semen coicis is popcorn-shaped, taking out, screening to remove sand, and cooling, thus obtaining the semen coicis prepared decoction pieces. The semen coicis prepared decoction pieces have the advantages that effective components in cells of the semen coicis prepared decoction pieces are rapidly dissolved out, the effects of clinically reducing blood glucose and resisting tumors are enhanced, and the irritation is reduced. The processing technology of the semen coicis prepared decoction pieces has the advantages of high efficiency, standardization, energy conservation, environmental protection and the like.
Description
Technical field
The present invention relates to prepared slices of Chinese crude drugs field, particularly a kind of Semen Coicis legal system decoction pieces and preparation method thereof.
Background technology
Modern study shows: Semen Coicis has the effects such as blood sugar lowering, antitumor, raising immunity, is mainly used in clinically edema, beriberi, dysuria, diarrhea due to hypofunction of the spleen, arthralgia chiefly caused by damp pathogen contracture, lung abscess, acute appendicitis, wart, the diseases such as cancerous protuberance.
The existing concocting method of Semen Coicis is to get clean Semen Coicis, and the wheat bran that drops into parch container stirs rapidly, fries and to surface, is micro-yellow, obtains.But by after said method parch, in use, the effect that Semen Coicis has been given play to is faint, is difficult to produce a desired effect.
Summary of the invention
The object of the present invention is to provide a kind of Semen Coicis legal system decoction pieces and preparation method thereof, can effectively improve the content of the effective ingredient triolein in Semen Coicis, make it in application, it is more obvious that the effect of Semen Coicis is brought into play.
The object of the present invention is achieved like this, and a kind of Semen Coicis legal system decoction pieces is made by following material composition:
Semen Coicis and edible oil.
Count by weight 2.5～6 parts of described Semen Coicis 150-300 part, described edible oil.
Preferably, 200 parts of described Semen Coiciss, 4～6 parts of described edible oil.
A preparation method for Semen Coicis legal system decoction pieces, comprises the following steps:
Step 1, by Semen Coicis Ex-all, by 30～40 mesh sieve holes, enters 1～5L and drinks the swollen 24～48h of water logging;
Wherein, soak time is difference to some extent according to the difference in season, preferably, soaks 46-50 hour winter, soaks 20-28 hour summer.
Preferably, every 1g Semen Coicis adds 1～5mL drinking water.
Step 2, picks up and soaks swollen Semen Coicis, drains surface moisture, adds edible oil and mixes thoroughly, with moderate heat, steams 3～4h, to the well-done heart, takes out and dries to surface-brightening, color transparently, puts under the sun micro-solarization to holding tool hardness;
Wherein, preferably, the addition of described edible oil is that every 100kg Semen Coicis is mixed thoroughly with edible oil 1～3kg.
The time of drying is preferably 1～2 day.
Step 3, with moderate heat stir-baking with sand 3～5min, flower-shaped to rice krispies, take out, sieve shakeout, cools, and obtains.Wherein, final yield is 60%～70%.
A kind of Semen Coicis legal system decoction pieces provided by the invention and preparation method thereof, can make the rapid stripping of the intracellular effective ingredient of Semen Coicis decoction pieces, strengthen the effects such as clinical blood sugar lowering, antitumor, and reduce zest, reach the advantages such as method italian-jobi jen process of preparing technique is efficient, standard, standard, energy-saving and environmental protection.Meanwhile, adopt Three factors-levels L9 (3
4) orthogonal test comes standard method preparation method of semen coicis and technical parameter, set up its normalized processing procedure, conventional process techniques and modern scientific theory are organically combined, and effective ingredient triolein is obviously raise, bring into play due curative effect, guarantee the safe and effective of common people's medication.
Simultaneously can improve Semen Coicis process of preparing technological level, make that it is efficient to realizing, the modern pharmaceutical technology of standard, standard, energy-saving and environmental protection strides forward major step.
The present invention adopts Three factors-levels L9 (3
4) orthogonal test comes standard method preparation method of semen coicis and technical parameter, sets up its normalized processing procedure, conventional process techniques and modern scientific theory organically combined, and effective ingredient triolein is obviously raise, and brings into play due curative effect.
Accompanying drawing explanation
Fig. 1 is the preparation method flow chart of a kind of Semen Coicis legal system decoction pieces provided by the invention.
The specific embodiment
Below by specific embodiment, also by reference to the accompanying drawings the present invention is described in further detail.
A Semen Coicis legal system decoction pieces, by following material composition, made:
Semen Coicis and edible oil.
Count by weight 2.5～6 parts of described Semen Coicis 150-300 part, described edible oil.
Preferably, 200 parts of described Semen Coiciss, 4～6 parts of described edible oil.
A preparation method for Semen Coicis legal system decoction pieces, as shown in Figure 1, comprises the following steps:
Step 1, by Semen Coicis Ex-all, by 30～40 mesh sieve holes, enters 1～5L and drinks the swollen 24～48h of water logging;
Wherein, soak time is difference to some extent according to the difference in season, preferably, soaks 46-50 hour winter, soaks 20-28 hour summer.
Preferably, every 1g Semen Coicis adds 1～5mL drinking water.
Step 2, picks up and soaks swollen Semen Coicis, drains surface moisture, adds edible oil and mixes thoroughly, with moderate heat, steams 3～4h, to the well-done heart, takes out and dries to surface-brightening, color transparently, puts under the sun micro-solarization to holding tool hardness;
Wherein, preferably, the addition of described edible oil is that every 100kg Semen Coicis is mixed thoroughly with edible oil 1～3kg.
The time of drying is preferably 1～2 day.
Step 3, with moderate heat stir-baking with sand 3～5min, flower-shaped to rice krispies, take out, sieve shakeout, cools, and obtains.Wherein, final yield is 60%～70%.
A kind of Semen Coicis legal system decoction pieces provided by the invention and preparation method thereof, can make the rapid stripping of the intracellular effective ingredient of Semen Coicis decoction pieces, strengthen the effects such as clinical blood sugar lowering, antitumor, and reduce zest, reach the advantages such as method italian-jobi jen process of preparing technique is efficient, standard, standard, energy-saving and environmental protection.Meanwhile, adopt Three factors-levels L9 (3
4) orthogonal test comes standard method preparation method of semen coicis and technical parameter, set up its normalized processing procedure, conventional process techniques and modern scientific theory are organically combined, and effective ingredient triolein is obviously raise, bring into play due curative effect, guarantee the safe and effective of common people's medication.
Simultaneously can improve Semen Coicis process of preparing technological level, make that it is efficient to realizing, the modern pharmaceutical technology of standard, standard, energy-saving and environmental protection strides forward major step.
The present invention adopts Three factors-levels L9 (3
4) orthogonal test comes standard method preparation method of semen coicis and technical parameter, sets up its normalized processing procedure, conventional process techniques and modern scientific theory organically combined, and effective ingredient triolein is obviously raise, and brings into play due curative effect.
The content balance table of the effective ingredient triolein in the Semen Coicis that below different concocting methods are made:
Result Semen Coicis is after distinct methods is concocted, the content of triolein is obviously inconsistent, that is: method Semen Coicis > fries the clean Semen Coicis of Semen Coicis > parching with earth Semen Coicis > Semen Coicis (parched with bran) >, and method Semen Coicis and fry content recruitment higher than other concocting method, embodies legal system Semen Coicis with the obvious advantage.
Embodiment 1
Get Semen Coicis 200g, Ex-all, by 30～40 mesh sieve holes, enters 3L and drinks the swollen 24～48h of water logging.Pick up and drain surface moisture, add edible oil 6g and mix thoroughly, with moderate heat, steam 3～4h, to the well-done heart, take out dry to surface-brightening, color transparent, micro-solarization.With 140 ℃ of-190 ℃ of moderate heat stir-baking with sand 3～5min, flower-shaped to rice krispies, take out, sieve shakeout, cools, and obtains.
According to process of preparation method quality standard, detect finished product, concrete detection is as follows:
[discriminating]
(1) the light off-white color of microscopical identification this product powder or yellow-white.Main is gelatinized starch grain, the visible oil droplet in parenchyma cell surface, accidental stone cell.
(2) thin layer chromatography is differentiated and is got this product powder 1g, adds petroleum ether (60～90 ℃) 10mL, and supersound process 30 minutes filters, filtrate evaporate to dryness, and residue adds petroleum ether (60～90 ℃) 1mL to be made to dissolve, as need testing solution.Separately get Semen Coicis control medicinal material 1g, be made in the same way of control medicinal material solution.According to thin layer chromatography test, draw each 10 μ L of above-mentioned two kinds of solution, put respectively on same silica gel g thin-layer plate, petroleum ether (60～90 ℃)-ethyl acetate-acetic acid (10:3:0.1) of take are developing solvent, launch, and take out, dry, put under ultra-violet lamp (365nm) and inspect.In test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, the fluorescence speckle of micro-aobvious same color.
(3) high performance liquid chromatography is differentiated and is got Semen Coicis oil reference extract, triolein reference substance, and the mobile phase adding under (assay) item is made respectively every 1mL containing the solution of 1mg, 0.14mg, in contrast extract, reference substance solution.According to the chromatographic condition test under (assay) item, draw respectively need testing solution, reference substance solution and above-mentioned reference extract, each 10 μ L of reference substance solution under (assay) item, injection liquid chromatography.The chromatographic peak that test sample chromatogram is consistent with reference substance retention time; And present 7 the main chromatographic peaks consistent with reference extract chromatographic peak retention time.
[extractum] measured according to the hot dipping under ethanol-soluble extractives algoscopy (appendix X A of Chinese Pharmacopoeia version in 2010) item, with dehydrated alcohol, makes solvent, and result is 7.4%.
[assay] measured according to high performance liquid chromatography (appendix VI D).
Chromatographic condition and system suitability be take octadecylsilane chemically bonded silica as filler; Acetonitrile-the dichloromethane (65:35) of take is mobile phase; Evaporative light scattering detector detects.Number of theoretical plate calculates and should be not less than 5000 by triolein peak.
It is appropriate that triolein reference substance is got in the preparation of reference substance solution, accurately weighed, adds mobile phase and make every 1ml containing the solution of 0.14mg, obtains.
The about 0.6g of this product powder (crossing sieve No. three) is got in the preparation of need testing solution, accurately weighed, puts in tool plug conical flask, precision adds mobile phase 50ml, and weighed weight is soaked 2 hours, supersound process (power 300W, frequency 50kHz) 30 minutes, lets cool, weighed weight again, the weight of supplying less loss by mobile phase, shakes up, and filters, get subsequent filtrate, obtain.
Algoscopy is accurate reference substance solution 5 μ l, the 10 μ l of drawing respectively, need testing solution 5～10 μ l, and injection liquid chromatography, measures, and with external standard two-point method logarithmic equation, calculates, and obtains.
This product is pressed dry product and is calculated, containing triolein (C
57h
104o
6) be 0.90%.
Embodiment 2
Get Semen Coicis 250g, Ex-all, by 30～40 mesh sieve holes, enters 4L and drinks the swollen 24～48h of water logging.Pick up and drain surface moisture, add edible oil 5g and mix thoroughly, with moderate heat, steam 3～4h, to the well-done heart, take out dry to surface-brightening, color transparent, micro-solarization.With moderate heat (140 ℃-190 ℃) stir-baking with sand 3～5min, flower-shaped to rice krispies, take out, sieve shakeout, cools, and obtains.
Detect (detection method is identical with embodiment 1).
[discriminating] (1) light off-white color of microscopical identification this product powder or yellow-white.Main is gelatinized starch grain, the visible oil droplet in parenchyma cell surface, accidental stone cell.
(2) Semen Coicis control medicinal material check: in test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, the fluorescence speckle of micro-aobvious same color.
(3) Semen Coicis oil reference extract, the check of triolein reference substance: the chromatographic peak that test sample chromatogram is consistent with reference substance retention time; And present 7 the main chromatographic peaks consistent with reference extract chromatographic peak retention time.
[extractum] measured according to the hot dipping under ethanol-soluble extractives algoscopy (appendix X A of Chinese Pharmacopoeia version in 2010) item, with dehydrated alcohol, makes solvent, and result is 7.8%.
[assay] this product is pressed dry product and is calculated, containing triolein (C
57h
104o
6) be 0.92%.
Embodiment 3
Get Semen Coicis 300g, Ex-all, by 30～40 mesh sieve holes, enters 5L and drinks the swollen 24～48h of water logging; Pick up and drain surface moisture, add edible oil 4g and mix thoroughly, with moderate heat, steam 3～4h, to the well-done heart, take out dry to surface-brightening, color transparent, micro-solarization; With moderate heat (140 ℃-190 ℃) stir-baking with sand 3～5min, flower-shaped to rice krispies, take out, sieve shakeout, cools, and obtains.
Detect (detection method is identical with embodiment 1).
[discriminating] (1) light off-white color of microscopical identification this product powder or yellow-white.Main is gelatinized starch grain, the visible oil droplet in parenchyma cell surface, accidental stone cell.
(2) Semen Coicis control medicinal material check: in test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, the fluorescence speckle of micro-aobvious same color.
(3) Semen Coicis oil reference extract, the check of triolein reference substance: the chromatographic peak that test sample chromatogram is consistent with reference substance retention time; And present 7 the main chromatographic peaks consistent with reference extract chromatographic peak retention time.
[extractum] measured according to the hot dipping under ethanol-soluble extractives algoscopy (appendix X A of Chinese Pharmacopoeia version in 2010) item, with dehydrated alcohol, makes solvent, and result is 8.0%.
[assay] this product is pressed dry product and is calculated, containing triolein (C
57h
104o
6) be 0.97%.
The former concocting method product quality of this concocting method comparison sheet:
From upper table result, learn, the decoction pieces product of concocting method of the present invention is compared every test item with former concocting method product and is all reached requirement, and effective ingredient triolein content is apparently higher than former concocting method.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (8)
1. a Semen Coicis legal system decoction pieces, is characterized in that, by following material composition, is made:
Semen Coicis and edible oil.
2. a kind of Semen Coicis legal system decoction pieces according to claim 1, is characterized in that, counts by weight 2.5～6 parts of described Semen Coicis 150-300 part, described edible oil.
3. the preparation method of a kind of Semen Coicis legal system decoction pieces according to claim 1 and 2, is characterized in that, comprises the following steps:
Step 1, by Semen Coicis Ex-all, by 30～40 mesh sieve holes, enters 1～5L and drinks the swollen 24～48h of water logging;
Step 2, picks up and soaks swollen Semen Coicis, drains surface moisture, adds edible oil and mixes thoroughly, with moderate heat, steams 3～4h, to the well-done heart, takes out and dries to surface-brightening, color transparently, puts under the sun micro-solarization to holding tool hardness;
Step 3, with moderate heat stir-baking with sand 2～5min, flower-shaped to rice krispies, take out, sieve shakeout, cools, and obtains.
4. the preparation method of a kind of Semen Coicis legal system decoction pieces according to claim 3, is characterized in that:
In described step 1, described in enter 1～5L and drink the swollen 24～48h of water logging and specifically comprise:
Soak 46-50 hour winter, soak 20-28 hour summer.
5. the preparation method of a kind of Semen Coicis legal system decoction pieces according to claim 4, is characterized in that:
Described step 1, in every 1g Semen Coicis add 1～5mL drinking water.
6. the preparation method of a kind of Semen Coicis legal system decoction pieces according to claim 3, is characterized in that:
In described step 2, the addition of described edible oil is that every 100kg Semen Coicis is mixed thoroughly with edible oil 1～3kg.
7. the preparation method of a kind of Semen Coicis legal system decoction pieces according to claim 6, is characterized in that:
In described step 2, the time of drying is 1～2 day.
8. the preparation method of a kind of Semen Coicis legal system decoction pieces according to claim 3, is characterized in that:
In described step 2 and step 3, the temperature of described moderate heat is 140 ℃-190 ℃.
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Cited By (8)
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| CN105105020A (en) * | 2015-09-18 | 2015-12-02 | 福建农林大学 | Coix lacryma-jobi instant tablets rich in EGCG and coix seed grease |
| CN108939031A (en) * | 2018-09-20 | 2018-12-07 | 江西景德中药股份有限公司 | Chinese medicine composition of strengthening spleen and nourishing blood and its preparation method and application |
| CN108982741A (en) * | 2018-09-13 | 2018-12-11 | 江西景德中药股份有限公司 | The discrimination method of method semen coicis based on thin-layer chromatography |
| CN108969688A (en) * | 2018-09-20 | 2018-12-11 | 江西景德中药股份有限公司 | Invigorating spleen for diuresis, Chinese medicine composition of detumescence and apocenosis and its preparation method and application |
| CN108992601A (en) * | 2018-09-13 | 2018-12-14 | 江西景德中药股份有限公司 | Semen coicis legal system medicine materical crude slice and preparation method thereof |
| CN110063497A (en) * | 2019-06-04 | 2019-07-30 | 四川星河云海科技有限公司 | A kind of semen coicis food and its processing method |
| CN110151930A (en) * | 2019-05-27 | 2019-08-23 | 王茂泓 | A kind of processing method of Chinese medicine preparation |
| CN113058008A (en) * | 2021-04-09 | 2021-07-02 | 建昌帮药业有限公司 | Fried semen coicis and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105020A (en) * | 2015-09-18 | 2015-12-02 | 福建农林大学 | Coix lacryma-jobi instant tablets rich in EGCG and coix seed grease |
| CN105105020B (en) * | 2015-09-18 | 2018-08-17 | 福建农林大学 | A kind of Job's tears fast food piece rich in EGCG and coix seed grease |
| CN108982741A (en) * | 2018-09-13 | 2018-12-11 | 江西景德中药股份有限公司 | The discrimination method of method semen coicis based on thin-layer chromatography |
| CN108992601A (en) * | 2018-09-13 | 2018-12-14 | 江西景德中药股份有限公司 | Semen coicis legal system medicine materical crude slice and preparation method thereof |
| CN108992601B (en) * | 2018-09-13 | 2021-10-29 | 江西景德中药股份有限公司 | Decoction pieces prepared from Coicis semen and its preparation method |
| CN108939031A (en) * | 2018-09-20 | 2018-12-07 | 江西景德中药股份有限公司 | Chinese medicine composition of strengthening spleen and nourishing blood and its preparation method and application |
| CN108969688A (en) * | 2018-09-20 | 2018-12-11 | 江西景德中药股份有限公司 | Invigorating spleen for diuresis, Chinese medicine composition of detumescence and apocenosis and its preparation method and application |
| CN110151930A (en) * | 2019-05-27 | 2019-08-23 | 王茂泓 | A kind of processing method of Chinese medicine preparation |
| CN110063497A (en) * | 2019-06-04 | 2019-07-30 | 四川星河云海科技有限公司 | A kind of semen coicis food and its processing method |
| CN113058008A (en) * | 2021-04-09 | 2021-07-02 | 建昌帮药业有限公司 | Fried semen coicis and preparation method thereof |
| CN113058008B (en) * | 2021-04-09 | 2022-05-20 | 建昌帮药业有限公司 | Fried semen coicis and preparation method thereof |
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