CN103937627A - Cleaning agent for chip capacitors - Google Patents

Cleaning agent for chip capacitors Download PDF

Info

Publication number
CN103937627A
CN103937627A CN201410123941.4A CN201410123941A CN103937627A CN 103937627 A CN103937627 A CN 103937627A CN 201410123941 A CN201410123941 A CN 201410123941A CN 103937627 A CN103937627 A CN 103937627A
Authority
CN
China
Prior art keywords
clean
out system
ethanol
patch capacitor
tensio
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201410123941.4A
Other languages
Chinese (zh)
Other versions
CN103937627B (en
Inventor
张海鹏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201410123941.4A priority Critical patent/CN103937627B/en
Publication of CN103937627A publication Critical patent/CN103937627A/en
Application granted granted Critical
Publication of CN103937627B publication Critical patent/CN103937627B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Detergent Compositions (AREA)

Abstract

The invention provides a cleaning agent for chip capacitors. The cleaning agent consists of the following components in percentage by weight: 40-60% of ethanol, 20-30% of diethyl glutarate, 10-20% of diethylene glycol monobutyl ether, 5-15% of isobutyl acetate, 3-8% of surfactant and 2-5% of dispersing agent. The cleaning agent solves the problems that an existing clip capacitor cleaning agent is high in volatility and is not environment-friendly.

Description

A kind of clean-out system for patch capacitor
Technical field
The present invention relates to patch capacitor technical field, particularly a kind of clean-out system for patch capacitor.
Background technology
Patch capacitor is the important electronic component in electronic product surface mounting technique, with the resistance slurry with certain resistivity, is printed onto on ceramic substrate and through sintering, forms.
Chip capacitor has been used the porcelain that contains tackiness agent in manufacture craft, it consists of macromolecule resin, solidifying agent, softening agent, dispersion agent, defoamer and porcelain, in making, sintering temperature is more than 1000 ℃, porcelain forms firm ceramic diaphragm, also can produce some residues simultaneously, residue thoroughly must be cleaned up to the temperature stability of guarantee patch capacitor, capacity stability and dielectric loss stability.Having used clean-out system main component is for many years trieline, methylene dichloride etc.But the toxicity of trieline is very big, methylene dichloride volatilization is too fast, in order to guarantee cleaning quality, just need constantly to add clean-out system, cause production cost to rise, in order to overcome the above-mentioned defect of clean-out system, provide a kind of cleaning force strong, the environment-friendly cleaning agent that volatility is low is very necessary.
Summary of the invention
For above-mentioned the deficiencies in the prior art, the invention provides a kind of clean-out system for patch capacitor, solve the problem of existing patch capacitor clean-out system high volatility, not environmental protection.
Technical scheme of the present invention is achieved in that a kind of clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 40~60%, ethyl glutarate 20~30%, Diethylene Glycol butyl ether 10~20%, isobutyl acetate 5~15%, tensio-active agent 3~8%, dispersion agent 2~5%.
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 45~52%, ethyl glutarate 22~28%, Diethylene Glycol butyl ether 12~18%, isobutyl acetate 6~12%, tensio-active agent 5~6%, dispersion agent 3~4%.Wherein, preferably, described tensio-active agent is Sodium dodecylbenzene sulfonate.
Wherein, preferably, described dispersion agent is trolamine.
Beneficial effect of the present invention:
1. clean-out system of the present invention has adopted alcohol, ester, ethers combination solvent, has greatly improved washing dynamics, and washing power reaches more than 99%.
2. in clean-out system of the present invention, added tensio-active agent, wherein, the Sodium dodecylbenzene sulfonate adding is senior tensio-active agent, has increased wettability and the perviousness of clean-out system, reduce the interfacial tension between clean-out system and selected object, contributed to peeling off of residue to come off.
3. clean-out system of the present invention adds dispersion agent, and dispersion agent can be scattered in scavenging solution peeling off cast, can not deposit again, has guaranteed to be cleaned the cleanliness factor of object.
Embodiment
Below the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only the present invention's part embodiment, rather than whole embodiment.Embodiment based in the present invention, those of ordinary skills, not making all other embodiment that obtain under creative work prerequisite, belong to the scope of protection of the invention.
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 40~60%, ethyl glutarate 20~30%, Diethylene Glycol butyl ether 10~20%, isobutyl acetate 5~15%, tensio-active agent 3~8%, dispersion agent 2~5%.
In the following embodiments, tensio-active agent is Sodium dodecylbenzene sulfonate, and dispersion agent is trolamine, and except above-mentioned substance, tensio-active agent and dispersion agent also can be other conventional tensio-active agent and dispersion agent in clean-out system.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 100-150r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 50-60r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 50-60r/min, stir, be clean-out system of the present invention.
Embodiment 1
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 45%, ethyl glutarate 25%, Diethylene Glycol butyl ether 12%, isobutyl acetate 8%, Sodium dodecylbenzene sulfonate 6%, trolamine 4%.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 120r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 55r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 55r/min, stir, be clean-out system of the present invention.
Embodiment 2
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 55%, ethyl glutarate 20%, Diethylene Glycol butyl ether 10%, isobutyl acetate 5%, Sodium dodecylbenzene sulfonate 5%, trolamine 5%.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 100r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 50r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 50r/min, stir, be clean-out system of the present invention.
Embodiment 3
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 40%, ethyl glutarate 30%, Diethylene Glycol butyl ether 18%, isobutyl acetate 7%, Sodium dodecylbenzene sulfonate 3%, trolamine 2%.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 150r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 60r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 60r/min, stir, be clean-out system of the present invention.
Embodiment 4
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 60%, ethyl glutarate 20%, Diethylene Glycol butyl ether 10%, isobutyl acetate 5%, Sodium dodecylbenzene sulfonate 3%, trolamine 2%.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 110r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 55r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 55r/min, stir, be clean-out system of the present invention.
Embodiment 5
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 40%, ethyl glutarate 24%, Diethylene Glycol butyl ether 20%, isobutyl acetate 10%, Sodium dodecylbenzene sulfonate 3%, trolamine 3%.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 130r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 58r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 52r/min, stir, be clean-out system of the present invention.
Embodiment 6
For a clean-out system for patch capacitor, composed of the following components by weight percentage: ethanol 40%, ethyl glutarate 28%, Diethylene Glycol butyl ether 10%, isobutyl acetate 12%, Sodium dodecylbenzene sulfonate 8%, trolamine 2%.
A preparation method for the clean-out system of patch capacitor, comprises the following steps:
1. ethanol, tensio-active agent are placed in to the reactor that band stirs, the speed with 140r/min under normal temperature is stirred to whole dissolvings;
2. pentanedioic acid diethyl ester, Diethylene Glycol butyl ether, ethanol isobutyl ester are added in the mixing solutions of step 1 gained, with the speed of 54r/min, be stirred to and mix;
3. trolamine is slowly splashed in the mixing solutions of step 2 gained, with the speed of 58r/min, stir, be clean-out system of the present invention.
Cleaning performance comparative test result
The pH value of clean-out system is 6.8-7.8, and washing power, higher than 99.3%, can meet the processing requirement that patch capacitor is made completely.
The foregoing is only preferred embodiment of the present invention, in order to limit the present invention, within the spirit and principles in the present invention not all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.

Claims (4)

1. for a clean-out system for patch capacitor, it is characterized in that, composed of the following components by weight percentage: ethanol 40~60%, ethyl glutarate 20~30%, Diethylene Glycol butyl ether 10~20%, isobutyl acetate 5~15%, tensio-active agent 3~8%, dispersion agent 2~5%.
2. a kind of clean-out system for patch capacitor according to claim 1, it is characterized in that, composed of the following components by weight percentage: ethanol 45~52%, ethyl glutarate 22~28%, Diethylene Glycol butyl ether 12~18%, isobutyl acetate 6~12%, tensio-active agent 5~6%, dispersion agent 3~4%.
3. a kind of clean-out system for patch capacitor according to claim 1 and 2, is characterized in that, described tensio-active agent is Sodium dodecylbenzene sulfonate.
4. a kind of clean-out system for patch capacitor according to claim 1 and 2, is characterized in that, described dispersion agent is trolamine.
CN201410123941.4A 2014-03-28 2014-03-28 A kind of cleaning agent for patch capacitor Expired - Fee Related CN103937627B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410123941.4A CN103937627B (en) 2014-03-28 2014-03-28 A kind of cleaning agent for patch capacitor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410123941.4A CN103937627B (en) 2014-03-28 2014-03-28 A kind of cleaning agent for patch capacitor

Publications (2)

Publication Number Publication Date
CN103937627A true CN103937627A (en) 2014-07-23
CN103937627B CN103937627B (en) 2017-10-10

Family

ID=51185508

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410123941.4A Expired - Fee Related CN103937627B (en) 2014-03-28 2014-03-28 A kind of cleaning agent for patch capacitor

Country Status (1)

Country Link
CN (1) CN103937627B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105296205A (en) * 2015-11-25 2016-02-03 济南昊泽环保科技有限公司 Cleaning agent for mechanical equipment, and preparation method of cleaning agent
WO2017140951A1 (en) * 2016-02-18 2017-08-24 Vauhti Speed Oy Composition for cleaning skin strips of skin skis

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1985217A (en) * 2004-07-15 2007-06-20 马林克罗特贝克公司 Non-aqueous microelectronic cleaning compositions containing fructose
CN101440332A (en) * 2008-12-30 2009-05-27 潘惠凯 Environment protection efficient water-based circuit board cleaning agent and preparation thereof
CN102191140A (en) * 2011-04-18 2011-09-21 宁波喜汉锡焊料有限公司 Electronic circuit board detergent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1985217A (en) * 2004-07-15 2007-06-20 马林克罗特贝克公司 Non-aqueous microelectronic cleaning compositions containing fructose
CN101440332A (en) * 2008-12-30 2009-05-27 潘惠凯 Environment protection efficient water-based circuit board cleaning agent and preparation thereof
CN102191140A (en) * 2011-04-18 2011-09-21 宁波喜汉锡焊料有限公司 Electronic circuit board detergent

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105296205A (en) * 2015-11-25 2016-02-03 济南昊泽环保科技有限公司 Cleaning agent for mechanical equipment, and preparation method of cleaning agent
WO2017140951A1 (en) * 2016-02-18 2017-08-24 Vauhti Speed Oy Composition for cleaning skin strips of skin skis
US10711226B2 (en) 2016-02-18 2020-07-14 Vauhti Speed Oy Composition for cleaning skin strips of skin skis

Also Published As

Publication number Publication date
CN103937627B (en) 2017-10-10

Similar Documents

Publication Publication Date Title
CN101728001B (en) Lead-free and low-silver photosensitive silver paste and preparation method thereof
CN103545012B (en) Filter conductive silver paste and preparation method thereof
CN102831949B (en) Efficient lead-free silver paste on back of solar cell and preparation method of silver paste
CN107962317B (en) Water-based cleaning-free soldering flux
WO2012108290A1 (en) Electroconductive paste and solar cell element obtained using the electroconductive paste
CN109326514B (en) Selective emitter solar cell phosphorus-doped slurry and preparation method thereof
CN103937627A (en) Cleaning agent for chip capacitors
TW436516B (en) Water cleanable silver composition
CN102855961A (en) Paste for formation of solar cell back electrodes and preparation method thereof
CN111105932B (en) Solid-state capacitance carbon foil nano conductive carbon paste and preparation method thereof
CN101354926B (en) Method for preparing conductor slurry containing carbon and silver
CN102831959B (en) Sliver paste for lead-free environment-friendly solar photovoltaic cells and preparation method of silver paste
CN104407735A (en) Touch screen leading wire conductive circuit, manufacturing method thereof, and touch screen mobile phone
CN104231325A (en) Preparation method of organic carrier
CN107868729B (en) Degumming composition and preparation method and application thereof
KR101368314B1 (en) Vehicle compositon and conductive composition using the same
CN103551762B (en) A kind of hot air leveling-up scaling powder of non-volatility organic matter and preparation method thereof
JP2014067492A (en) Composition for forming conductive part and manufacturing method of conductive part
CN104231713A (en) Paint remover and paint removing method thereof
CN115312230A (en) Conductive silver paste, and preparation method and application thereof
CN102831950B (en) Conductive lead-free silver paste mixed with copper powder and aluminum powder for solar cell and preparation method of conductive lead-free silver paste
CN104479464A (en) Water-based bacterial cellulose paint for lithium battery diaphragms
CN112289480A (en) Solar cell silver paste and preparation method thereof
CN112125301A (en) Graphene dispersing agent applied to change of graphene dispersion property
CN111128438A (en) Dip-soldering tin-free environment-friendly silver paste and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171010

Termination date: 20200328