Multistage combined heat regulation ultrapure water continuous generator is dividing an application of invention " multistage combined secondary distillation heat regulation ultrapure water continuous generator ".Original application day: on April 22nd, 2016, application number: 2014100450588, former invention and created name: multistage combined secondary distillation heat regulation ultrapure water continuous generator.
Summary of the invention
For the defect of prior art, one of object of the application:
Be to adopt multistage distillation to prepare high purity water in complete totally enclosed system, avoid secondary pollution;
Two of the application's object:
Be to provide a kind of multistage distillation of continuous supplementation feed liquor to prepare high-purity hydrophone, alleviate and need the scientific research personnel of high purity water tired;
Three of the application's object:
Be to provide the bubble-free high-efficiency multi-stage distillation preparation of a kind of prolong high-purity hydrophone.
For guaranteeing that above-mentioned purpose realization also should possess:
1, the distillation amount of primary and secondary distiller wants consistent, the two balance;
2, each interlayer, for avoiding hypertonia to occur the unexpected explosion of glass pot, also will keep the internal and external pressure balance in each interlayer;
3, air enters and brings impurity effect pure water quality into;
4, glass pot also will bear certain pressure, avoids the breakage of the accidental collision in packed and transported use procedure.
For achieving the above object, the application by the following technical solutions:
1, multistage combined heat regulation ultrapure water continuous generator, comprises elementary prolong outlet pipe 1-1, elementary V-arrangement prolong 2-1, elementary quartz heating-pipe 3-1, primary distillation device 4-1, elementary prolong inlet tube 5-1, elementary prolong inlet tube water seal 6-1, the elementary liquid funnel 7-1 that holds, elementary filler neck 8-1, secondary prolong outlet pipe 1-2, secondary V-arrangement prolong 2-2, secondary quartz heating-pipe 3-2, secondary distiller 4-2, secondary prolong inlet tube 5-2, secondary prolong inlet tube water seal 6-2, the secondary liquid funnel 7-2 that holds, secondary filler neck 8-2, high purity water outlet pipe 9, silica glass valve 9-1, pressure compensation opening 10, high-order glass pot 11, glass valves 12, first water feed liquor flexible pipe 13, first water fluid inlet 14, support 15, high purity water storage chamber 16, upper interlayer 17-1, lower interlayer 17-2, distiller back cover 18, distiller main body 19, distiller end socket 20, primary air filter 21-1, secondary air strainer 21-2, storage chamber air filter 21-3, primary electrical heated filament 22-1, secondary electrical heated filament 22-2, voltate regulator 23,
It is characterized in that: high-order glass pot 11 bottoms connect glass valves 12, and glass valves 12 connects first water feed liquor flexible pipe 13, and first water feed liquor flexible pipe 13 connects first water fluid inlet 14, and pressure compensation opening 10 is equipped with at high-order glass pot 11 tops;
Distiller main body 19 is right cylinder, and distiller main body 19 is divided into three regions by upper interlayer 17-1 and lower interlayer 17-2, that is: primary distillation device 4-1, secondary distiller 4-2 and high purity water storage chamber 16; It is the isometrical circular glass sheet of right cylinder, the inwall bonding connection of upper interlayer 17-1 and lower interlayer 17-2 circumferential edge and distiller main body 19 that upper interlayer 17-1 and lower interlayer 17-2 are with distiller main body 19;
Distiller main body 19 top bonding connection distiller end sockets 20, distiller main body 19 bottom adhesive connect distiller back cover 18;
Described primary distillation device 4-1 is positioned at distiller main body 19 tops, and primary distillation device 4-1 comprises elementary prolong outlet pipe 1-1, elementary V-arrangement prolong 2-1, elementary quartz heating-pipe 3-1, elementary prolong inlet tube 5-1, elementary prolong inlet tube water seal 6-1, elementary liquid funnel 7-1, elementary filler neck 8-1, upper interlayer 17-1, primary air filter 21-1, the primary electrical heated filament 22-1 of holding; Elementary V-arrangement prolong 2-1 is positioned at primary distillation device 4-1 top; Elementary prolong outlet pipe 1-1 and elementary prolong inlet tube 5-1 lean out respectively outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Elementary quartz heating-pipe 3-1 is U-shaped pipe, inside has primary electrical heated filament 22-1, and elementary quartz heating-pipe 3-1U type opening end leans out outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Elementaryly hold the below that liquid funnel 7-1 is positioned at primary distillation device 4-1 bottom elementary V-arrangement prolong 2-1, face " V " font bottom of elementary V-arrangement prolong 2-1;
First water fluid inlet 14 is positioned at primary distillation device 4-1 bottom one side, the tube wall surrounding of first water fluid inlet 14 and bonding the linking together of upper interlayer 17-1 through upper interlayer 17-1;
The elementary liquid funnel 7-1 bottom of holding is elementary filler neck 8-1, and elementary filler neck 8-1 is positioned at primary distillation device 4-1 bottom center, and through upper interlayer 17-1, the outer wall of elementary filler neck 8-1 is together with upper interlayer 17-1 bonding connection; The outlet of elementary filler neck 8-1 is arranged in secondary distiller 4-2;
Described secondary distiller 4-2 is positioned at distiller main body 19 middle parts, and secondary distiller 4-2 comprises secondary prolong outlet pipe 1-2, secondary V-arrangement prolong 2-2, secondary quartz heating-pipe 3-2, secondary prolong inlet tube 5-2, secondary prolong inlet tube water seal 6-2, secondary liquid funnel 7-2, secondary filler neck 8-2, upper interlayer 17-2, secondary air strainer 21-2, the secondary electrical heated filament 22-2 of holding;
Secondary V-arrangement prolong 2-2 is positioned at secondary distiller 4-2 top; Secondary prolong outlet pipe 1-2 and secondary prolong inlet tube 5-2 lean out respectively outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Secondary quartz heating-pipe 3-2 is U-shaped, inside has secondary electrical heated filament 22-2, departs from the central authorities of distiller main body 19 at the bottom of " V " font of secondary quartz heating-pipe 3-2; (its objective is and make the secondary liquid funnel 7-2 elementary filler neck 8-1 that staggers that holds) secondary quartz heating-pipe 3-2U type opening end leans out outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Described secondary electrical heated filament 22-2 connects voltate regulator 23; For thyristor regulating depressor, (adjustment is added to the voltage on nichrome wire to described voltate regulator 23, controls heating power; Regulate voltate regulator 23 to reduce voltage the heating intensity of secondary electrical heated filament 22-2 is reduced, make the distillation amount of secondary distiller 4-2 and the distillation amount of primary distillation device 4-1 keep balance, avoid secondary distiller 4-2 distillation speed too fast, evaporate to dryness burns out);
Secondaryly hold the below that liquid funnel 7-2 is positioned at secondary distiller 4-2 bottom secondary V-arrangement prolong 2-2, face " V " font bottom of secondary V-arrangement prolong 2-2;
The secondary liquid funnel 7-2 bottom of holding is secondary filler neck 8-2, and secondary filler neck 8-2 is positioned at secondary distiller 4-2 bottom, and through lower interlayer 17-2, the outer wall of secondary filler neck 8-2 is together with lower interlayer 17-2 bonding connection; The outlet of secondary filler neck 8-2 is arranged in high purity water store chamber 16;
Described high purity water store chamber 16 bottoms connect high purity water band valve outlet port pipe 9.
2, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: described elementary prolong inlet tube 5-1 connects elementary prolong inlet tube water seal 6-1.
3, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: described secondary prolong inlet tube 5-2 connects secondary prolong inlet tube water seal 6-2.
4, described multistage combined heat regulation ultrapure water continuous generator, it is characterized in that: described support 15 is identical three of equidistant shape, three supports 15 are positioned at distiller back cover 18 housing bottoms, three support 15 spacing equate, support multistage combined heat regulation ultrapure water continuous generator.
5, described multistage combined heat regulation ultrapure water continuous generator, it is characterized in that: described elementary prolong outlet pipe 1-1, elementary V-arrangement prolong 2-1, elementary quartz heating-pipe 3-1, primary distillation device 4-1, elementary prolong inlet tube 5-1, the elementary liquid funnel 7-1 that holds, elementary filler neck 8-1, secondary prolong outlet pipe 1-2, secondary V-arrangement prolong 2-2, secondary quartz heating-pipe 3-2, secondary distiller 4-2, secondary prolong inlet tube 5-2, the secondary liquid funnel 7-2 that holds, secondary filler neck 8-2, high purity water outlet pipe 9, silica glass valve 9-1, first water fluid inlet 14, high purity water storage chamber 16, upper interlayer 17-1, lower interlayer 17-2, distiller back cover 18, distiller main body 19, distiller end socket 20 is silica glass material, (avoiding the pollution of simple glass to distilled water at different levels).
6, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: described distiller back cover 18 and distiller end socket 20 are the ellipsoid of evagination.(avoiding using or transporting and damage distiller by accidental impact).
7, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: primary air filter 21-1 is housed on distiller end socket 20.
8, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: on top side portion distiller main body 19 walls of secondary distiller 4-2, secondary air strainer 21-2 is housed.
9, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: on the 16 top side portion walls of high purity water storage chamber, storage chamber air filter 21-3 is housed.(air filter can effectively avoid other impurity such as airborne micronic dust, bacterium to enter).
10, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: silica glass valve 9-1 is housed on described high purity water outlet pipe 9.(while stopping using, close glass valves 9-1, can avoid airborne impurity to waft in high purity water storage chamber 16)
Beneficial effect
1, boil after the series connection of high purity water distiller in the multistage quartzy Asia of solution prior art, is non-closed system, avoids causing the problem of secondary pollution;
2, multistage combined heat regulation ultrapure water continuous generator, because multistage distillation device is combined, the second distillation water temp of elementary condensation is high, continues the fast heat utilization rate of heating evaporation high;
3, multistage combined heat regulation ultrapure water continuous generator combine volume little, take up room littlely, cost is low;
4, adopt the water seal of prolong inlet tube to enter prolong by Anti-bubble, elementary V-arrangement prolong and secondary V-arrangement prolong inlet tube enter without bubble, and prolong utilization ratio is high, improves cooling efficiency, reduces water of condensation consumption, saving water resource;
5, in multistage combined heat regulation ultrapure water continuous generator, by regulating high purity water outlet pipe 9 to install silica glass valve 9-1 additional, in used time not, to close, the impurity that prevents air enters high purity water storage chamber 16 and pollutes high purity waters;
6, by the adjustment to the first water feed liquor amount of glass valves 12, can realize the running balance of flooding quantity and high purity water liquid outlet quantity, therefore can alleviate the fatigue that operator's long-time observation causes, and avoid because flooding quantity deficiency causes that instrument dryouies, bursts, damage instrument, even bring harm;
7, in elementary, secondary distiller and high purity water storage chamber, installing air filter additional can effectively avoid other impurity such as airborne micronic dust, bacterium to enter;
8, described glass pot 4 main bodys are cylindrical, and glass pot 4 tops and bottom are the arch of evagination, and top and bottom bearing resistance are high.
9, adopt voltate regulator 23, the Heating temperature of secondary quartz heating-pipe in adjustable secondary distiller, make distillation amount in primary distillation device and the distillation amount in secondary distiller realize running balance, avoid redistilled water in secondary distiller because temperature is higher than the single flash water temp being entered by outside in primary distillation device, the fast evaporate to dryness of distillation speed, the problem burning out.
Embodiment
Embodiment 1
1, multistage combined heat regulation ultrapure water continuous generator, comprises elementary prolong outlet pipe 1-1, elementary V-arrangement prolong 2-1, elementary quartz heating-pipe 3-1, primary distillation device 4-1, elementary prolong inlet tube 5-1, elementary prolong inlet tube water seal 6-1, the elementary liquid funnel 7-1 that holds, elementary filler neck 8-1, secondary prolong outlet pipe 1-2, secondary V-arrangement prolong 2-2, secondary quartz heating-pipe 3-2, secondary distiller 4-2, secondary prolong inlet tube 5-2, secondary prolong inlet tube water seal 6-2, the secondary liquid funnel 7-2 that holds, secondary filler neck 8-2, high purity water outlet pipe 9, silica glass valve 9-1, pressure compensation opening 10, high-order glass pot 11, glass valves 12, first water feed liquor flexible pipe 13, first water fluid inlet 14, support 15, high purity water storage chamber 16, upper interlayer 17-1, lower interlayer 17-2, distiller back cover 18, distiller main body 19, distiller end socket 20, primary air filter 21-1, secondary air strainer 21-2, storage chamber air filter 21-3, primary electrical heated filament 22-1, secondary electrical heated filament 22-2, voltate regulator 23,
It is characterized in that: high-order glass pot 11 bottoms connect glass valves 12, and glass valves 12 connects first water feed liquor flexible pipe 13, and first water feed liquor flexible pipe 13 connects first water fluid inlet 14, and pressure compensation opening 10 is equipped with at high-order glass pot 11 tops;
Distiller main body 19 is right cylinder, and distiller main body 19 is divided into three regions by upper interlayer 17-1 and lower interlayer 17-2, that is: primary distillation device 4-1, secondary distiller 4-2 and high purity water storage chamber 16; It is the isometrical circular glass sheet of right cylinder, the inwall bonding connection of upper interlayer 17-1 and lower interlayer 17-2 circumferential edge and distiller main body 19 that upper interlayer 17-1 and lower interlayer 17-2 are with distiller main body 19;
Distiller main body 19 top bonding connection distiller end sockets 20, distiller main body 19 bottom adhesive connect distiller back cover 18;
Described primary distillation device 4-1 is positioned at distiller main body 19 tops, and primary distillation device 4-1 comprises elementary prolong outlet pipe 1-1, elementary V-arrangement prolong 2-1, elementary quartz heating-pipe 3-1, elementary prolong inlet tube 5-1, elementary prolong inlet tube water seal 6-1, elementary liquid funnel 7-1, elementary filler neck 8-1, upper interlayer 17-1, primary air filter 21-1, the primary electrical heated filament 22-1 of holding; Elementary V-arrangement prolong 2-1 is positioned at primary distillation device 4-1 top; Elementary prolong outlet pipe 1-1 and elementary prolong inlet tube 5-1 lean out respectively outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Elementary quartz heating-pipe 3-1 is U-shaped pipe, inside has primary electrical heated filament 22-1, and elementary quartz heating-pipe 3-1U type opening end leans out outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Elementaryly hold the below that liquid funnel 7-1 is positioned at primary distillation device 4-1 bottom elementary V-arrangement prolong 2-1, face " V " font bottom of elementary V-arrangement prolong 2-1;
First water fluid inlet 14 is positioned at primary distillation device 4-1 bottom one side, the tube wall surrounding of first water fluid inlet 14 and bonding the linking together of upper interlayer 17-1 through upper interlayer 17-1;
The elementary liquid funnel 7-1 bottom of holding is elementary filler neck 8-1, and elementary filler neck 8-1 is positioned at primary distillation device 4-1 bottom center, and through upper interlayer 17-1, the outer wall of elementary filler neck 8-1 is together with upper interlayer 17-1 bonding connection; The outlet of elementary filler neck 8-1 is arranged in secondary distiller 4-2.
Described secondary distiller 4-2 is positioned at distiller main body 19 middle parts, and secondary distiller 4-2 comprises secondary prolong outlet pipe 1-2, secondary V-arrangement prolong 2-2, secondary quartz heating-pipe 3-2, secondary prolong inlet tube 5-2, secondary prolong inlet tube water seal 6-2, secondary liquid funnel 7-2, secondary filler neck 8-2, upper interlayer 17-2, secondary air strainer 21-2, the secondary electrical heated filament 22-2 of holding;
Secondary V-arrangement prolong 2-2 is positioned at secondary distiller 4-2 top; Secondary prolong outlet pipe 1-2 and secondary prolong inlet tube 5-2 lean out respectively outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Secondary quartz heating-pipe 3-2 is U-shaped, inside has secondary electrical heated filament 22-2, departs from the central authorities of distiller main body 19 at the bottom of " V " font of secondary quartz heating-pipe 3-2; (its objective is and make the secondary liquid funnel 7-2 elementary filler neck 8-1 that staggers that holds) secondary quartz heating-pipe 3-2U type opening end leans out outside distiller main body 19 wall walls, and tube wall and distiller main body 19 walls are bonded together;
Described secondary electrical heated filament 22-2 connects voltate regulator 23; For thyristor regulating depressor, (adjustment is added to the voltage on nichrome wire to described voltate regulator 23, controls heating power; Regulate voltate regulator 23 to reduce voltage the heating intensity of secondary electrical heated filament 22-2 is reduced, make the distillation amount of secondary distiller 4-2 and the distillation amount of primary distillation device 4-1 keep balance, avoid secondary distiller 4-2 distillation speed too fast, evaporate to dryness burns out);
Secondaryly hold the below that liquid funnel 7-2 is positioned at secondary distiller 4-2 bottom secondary V-arrangement prolong 2-2, face " V " font bottom of secondary V-arrangement prolong 2-2;
The secondary liquid funnel 7-2 bottom of holding is secondary filler neck 8-2, and secondary filler neck 8-2 is positioned at secondary distiller 4-2 bottom, and through lower interlayer 17-2, the outer wall of secondary filler neck 8-2 is together with lower interlayer 17-2 bonding connection; The outlet of secondary filler neck 8-2 is arranged in high purity water store chamber 16;
Described high purity water store chamber 16 bottoms connect high purity water band valve outlet port pipe 9.
2, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: described elementary prolong inlet tube 5-1 connects elementary prolong inlet tube water seal 6-1.
3, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: described secondary prolong inlet tube 5-2 connects secondary prolong inlet tube water seal 6-2.
4, described multistage combined heat regulation ultrapure water continuous generator, it is characterized in that: described support 15 is identical three of equidistant shape, three supports 15 are positioned at distiller back cover 18 housing bottoms, three support 15 spacing equate, support multistage combined heat regulation ultrapure water continuous generator.
5, described multistage combined heat regulation ultrapure water continuous generator, it is characterized in that: described elementary prolong outlet pipe 1-1, elementary V-arrangement prolong 2-1, elementary quartz heating-pipe 3-1, primary distillation device 4-1, elementary prolong inlet tube 5-1, the elementary liquid funnel 7-1 that holds, elementary filler neck 8-1, secondary prolong outlet pipe 1-2, secondary V-arrangement prolong 2-2, secondary quartz heating-pipe 3-2, secondary distiller 4-2, secondary prolong inlet tube 5-2, the secondary liquid funnel 7-2 that holds, secondary filler neck 8-2, high purity water outlet pipe 9, silica glass valve 9-1, first water fluid inlet 14, high purity water storage chamber 16, upper interlayer 17-1, lower interlayer 17-2, distiller back cover 18, distiller main body 19, distiller end socket 20 is silica glass material, (avoiding the pollution of simple glass to distilled water at different levels).
6, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: described distiller back cover 18 and distiller end socket 20 are the ellipsoid of evagination.(avoiding using or transporting and damage distiller by accidental impact).
7, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: primary air filter 21-1 is housed on distiller end socket 20.
8, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: on top side portion distiller main body 19 walls of secondary distiller 4-2, secondary air strainer 21-2 is housed.
9, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: on the 16 top side portion walls of high purity water storage chamber, storage chamber air filter 21-3 is housed.(air filter can effectively avoid other impurity such as airborne micronic dust, bacterium to enter).
10, described multistage combined heat regulation ultrapure water continuous generator, is characterized in that: silica glass valve 9-1 is housed on described high purity water outlet pipe 9.(while stopping using, close glass valves 9-1, can avoid airborne impurity to waft in high purity water storage chamber 16).