CN103898769B - The preparation method of cotton-spinning fabric scouring agent - Google Patents
The preparation method of cotton-spinning fabric scouring agent Download PDFInfo
- Publication number
- CN103898769B CN103898769B CN201410110163.5A CN201410110163A CN103898769B CN 103898769 B CN103898769 B CN 103898769B CN 201410110163 A CN201410110163 A CN 201410110163A CN 103898769 B CN103898769 B CN 103898769B
- Authority
- CN
- China
- Prior art keywords
- parts
- mass
- agitator
- cotton
- take
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 18
- 238000009991 scouring Methods 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000009987 spinning Methods 0.000 title claims abstract description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 36
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 108010059892 Cellulase Proteins 0.000 claims abstract description 11
- 229940106157 cellulase Drugs 0.000 claims abstract description 11
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 10
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims abstract description 10
- ZZGUZQXLSHSYMH-UHFFFAOYSA-N ethane-1,2-diamine;propanoic acid Chemical compound NCCN.CCC(O)=O.CCC(O)=O ZZGUZQXLSHSYMH-UHFFFAOYSA-N 0.000 claims abstract description 10
- 125000001924 fatty-acyl group Chemical group 0.000 claims abstract description 10
- 239000011734 sodium Substances 0.000 claims abstract description 10
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 10
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 9
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 9
- 239000001110 calcium chloride Substances 0.000 claims abstract description 9
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 9
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 9
- 239000000344 soap Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 230000000694 effects Effects 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 7
- 229920000742 Cotton Polymers 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 5
- 239000008367 deionised water Substances 0.000 abstract description 4
- 229910021641 deionized water Inorganic materials 0.000 abstract description 4
- 239000001814 pectin Substances 0.000 abstract description 4
- 229920001277 pectin Polymers 0.000 abstract description 4
- 235000010987 pectin Nutrition 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract description 3
- 239000012752 auxiliary agent Substances 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract description 2
- 238000013019 agitation Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000009472 formulation Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to a kind of preparation method of cotton-spinning fabric scouring agent; material comprises: cellulase, alkaline pectase, trimethylolpropane, polyethylene glycol, two fatty acyl group ethylene diamine dipropionic acid sodium, sodium hydroxide solution, calcium chloride, hydrogen peroxide, soap flakes, deionized water; material grouping is poured in agitator according to formulation order and adds thermal agitation, naturally after cooling.The process conditions of the inventive method, as adding of material puts forward sequence, the rotating speed of agitator and temperature and control, all that inventor experienced by long-term practice, continuous summary improves thus obtains, the auxiliary agent of preparation participates in the concise of cotton fabric, cotton fiber except pectin effect and cleaning effect all very good, fabric softening is improved.
Description
Technical field
The present invention relates to a kind of weaving scouring agent, particularly a kind of preparation method of cotton-spinning fabric scouring agent.
Background technology
The preparation of tradition scouring agent is all generally that all materials are all mixed stirring, cool after being heated to uniform temperature, owing to may react between some material, therefore the order put upside down needs to redesign according to actual material composition, and mixing speed and temperature control also very important, there is certain influence to the final properties of product obtained.
Summary of the invention
The object of the invention is to: the defect overcoming above-mentioned prior art, propose a kind of preparation method of cotton-spinning fabric scouring agent.
In order to achieve the above object, the preparation method of the cotton-spinning fabric scouring agent that the present invention proposes, comprises the steps:
Step 1, take the sodium hydroxide solution of 16-25 parts by mass, the calcium chloride of 5-9 parts by mass, the soap flakes of 5-6 parts by mass, the trimethylolpropane of 5-6 parts by mass is together poured in agitator, be under the condition of 30-40 rev/min at speed of agitator, temperature is slowly risen to 20-25 DEG C;
Step 2, take the polyethylene glycol of 2-3 parts by mass, the hydrogen peroxide of 9-10 parts by mass, pour in agitator, mixing speed is increased to 40-50 rev/min, and temperature slowly rises to 30-35 DEG C;
Step 3, take two fatty acyl group ethylene diamine dipropionic acid sodium of 3-4 parts by mass, the ionized water of 60-70 parts by mass, pours in agitator, and agitator speed controls at 40-50 rev/min, and temperature slowly rises to 40-45 DEG C;
Step 4, take the cellulase of 0.2-0.3 parts by mass, the alkaline pectase of 0.9-1.2 parts by mass, pours in agitator, and mixing speed keeps 45-50 rev/min, and temperature slowly rises to 55-60 DEG C, and keeps 15-20 minute;
Step 5, be placed under normal temperature and naturally cool.
The preparation method of cotton-spinning fabric scouring agent of the present invention also has following improvement:
1, the mass percent concentration of described sodium hydroxide solution is: 15-16%.
2, in described hydrogen peroxide, the concentration of volume percent mark of hydrogen peroxide is 25-26%.
3, described cellulase is 0.2 part, and alkaline pectase is 0.9 part, and trimethylolpropane is 5 parts, and polyethylene glycol is 2 parts; two fatty acyl group ethylene diamine dipropionic acid sodium is 3 parts, and sodium hydroxide solution is 16 parts, and calcium chloride is 5 parts; hydrogen peroxide is 9 parts, and soap flakes are 5 parts, and deionized water is 60 parts.
4, described cellulase is 0.3 part, and alkaline pectase is 1.2 parts, and trimethylolpropane is 6 parts, and polyethylene glycol is 3 parts; two fatty acyl group ethylene diamine dipropionic acid sodium is 4 parts, and sodium hydroxide solution is 25 parts, and calcium chloride is 9 parts; hydrogen peroxide is 10 parts, and soap flakes are 6 parts, and deionized water is 70 parts.
5, described cellulase is 0.25 part; alkaline pectase is 1 part; trimethylolpropane is 5.5 parts; polyethylene glycol is 2.6 parts, and two fatty acyl group ethylene diamine dipropionic acid sodium is 3.4 parts, and sodium hydroxide solution is 20 parts; calcium chloride is 8 parts; hydrogen peroxide is 9.5 parts, and soap flakes are 5.5 parts, and deionized water is 65 parts.
Preparation method of the present invention, add alkaline pectase, the pectin removing effect of scouring agent to cellulose surface can be improved, and add a small amount of cellulase, improve fabric softening, and the trimethylolpropane added is on the one hand as the promoter of alkaline pectase, improves the heat resistance of cellulase on the other hand, extend its survival half-life, kill two birds with one stone.In addition, the two fatty acyl group ethylene diamine dipropionic acid sodium added in scouring agent are as a kind of novel Gemini surface active, and have excellent alkaline-resisting and resistance to stabilized hydrogen peroxide feature, emulsibility is good, and foaming power is strong, improves scouring result.
The process conditions of the inventive method, as adding of material puts forward sequence, the rotating speed of agitator and temperature and control, all that inventor experienced by long-term practice, continuous summary improves thus obtains, the auxiliary agent of preparation participates in the concise of cotton fabric, cotton fiber except pectin effect and cleaning effect all very good, fabric softening is improved.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described.
Embodiment one
The preparation method of the present embodiment cotton-spinning fabric scouring agent, comprises the steps:
Step 1, take the sodium hydroxide solution of 16 parts by mass, the calcium chloride of 5 parts by mass, the soap flakes of 5 parts by mass, the trimethylolpropane of 5 parts by mass is together poured in agitator, is under the condition of 30 revs/min, temperature is slowly risen to 20 DEG C at speed of agitator;
Step 2, take the polyethylene glycol of 2 parts by mass, the hydrogen peroxide of 9 parts by mass, pours in agitator, and mixing speed is increased to 40 revs/min, and temperature slowly rises to 30 DEG C;
Step 3, take two fatty acyl group ethylene diamine dipropionic acid sodium of 3 parts by mass, the ionized water of 60 parts by mass, pours in agitator, and agitator speed controls at 40 revs/min, and temperature slowly rises to 40 DEG C;
Step 4, take the cellulase of 0.2 parts by mass, the alkaline pectase of 0.9 parts by mass, pours in agitator, and mixing speed keeps 45 revs/min, and temperature slowly rises to 55 DEG C, and keeps 15 minutes;
Step 5, be placed under normal temperature and naturally cool.
Wherein, the mass percent concentration of sodium hydroxide solution is: 15%, and in hydrogen peroxide, the concentration of volume percent mark of hydrogen peroxide is 25%.
Embodiment two
The preparation method of the present embodiment cotton-spinning fabric scouring agent, comprises the steps:
Step 1, take the sodium hydroxide solution of 25 parts by mass, the calcium chloride of 9 parts by mass, the soap flakes of 6 parts by mass, the trimethylolpropane of 6 parts by mass is together poured in agitator, is under the condition of 40 revs/min, temperature is slowly risen to 25 DEG C at speed of agitator;
Step 2, take the polyethylene glycol of 3 parts by mass, the hydrogen peroxide of 10 parts by mass, pours in agitator, and mixing speed is increased to 50 revs/min, and temperature slowly rises to 35 DEG C;
Step 3, take two fatty acyl group ethylene diamine dipropionic acid sodium of 4 parts by mass, the ionized water of 70 parts by mass, pours in agitator, and agitator speed controls at 50 revs/min, and temperature slowly rises to 45 DEG C;
Step 4, take the cellulase of 0.3 parts by mass, the alkaline pectase of 1.2 parts by mass, pours in agitator, and mixing speed keeps 50 revs/min, and temperature slowly rises to 60 DEG C, and keeps 20 minutes;
Step 5, be placed under normal temperature and naturally cool.
Embodiment three
The preparation method of the present embodiment cotton-spinning fabric scouring agent, comprises the steps:
Step 1, take the sodium hydroxide solution of 20 parts by mass, the calcium chloride of 8 parts by mass, the soap flakes of 5.5 parts by mass, the trimethylolpropane of 5.5 parts by mass is together poured in agitator, is under the condition of 35 revs/min, temperature is slowly risen to 20-25 DEG C at speed of agitator;
Step 2, take the polyethylene glycol of 2.6 parts by mass, the hydrogen peroxide of 9.5 parts by mass, pours in agitator, and mixing speed is increased to 45 revs/min, and temperature slowly rises to 35 DEG C;
Step 3, take two fatty acyl group ethylene diamine dipropionic acid sodium of 3.4 parts by mass, the ionized water of 65 parts by mass, pours in agitator, and agitator speed controls at 45 revs/min, and temperature slowly rises to 43 DEG C;
Step 4, take the cellulase of 0.25 parts by mass, the alkaline pectase of 0.5 parts by mass, pours in agitator, and mixing speed keeps 48 revs/min, and temperature slowly rises to 58 DEG C, and keeps 18 minutes;
Step 5, be placed under normal temperature and naturally cool.
Our experiments show that, use above-mentioned three embodiment techniques to prepare scouring agent and participate in cotton fabric concise as additive, cotton fiber except pectin effect and cleaning effect all very good, fabric softening is improved.
In addition to the implementation, the present invention can also have other embodiments.All employings are equal to the technical scheme of replacement or equivalent transformation formation, all drop on the protection domain of application claims.
Claims (1)
1. a preparation method for cotton-spinning fabric scouring agent, comprises the steps:
Step 1, take the sodium hydroxide solution of 16-25 parts by mass, the calcium chloride of 5-9 parts by mass, the soap flakes of 5-6 parts by mass, the trimethylolpropane of 5-6 parts by mass is together poured in agitator, be under the condition of 30-40 rev/min at speed of agitator, temperature is slowly risen to 20-25 DEG C; The mass percent concentration of described sodium hydroxide solution is: 15-16%;
Step 2, take the polyethylene glycol of 2-3 parts by mass, the hydrogen peroxide of 9-10 parts by mass, pour in agitator, mixing speed is increased to 40-50 rev/min, and temperature slowly rises to 30-35 DEG C; In described hydrogen peroxide, the concentration of volume percent mark of hydrogen peroxide is 25-26%;
Step 3, take two fatty acyl group ethylene diamine dipropionic acid sodium of 3-4 parts by mass, the ionized water of 60-70 parts by mass, pours in agitator, and agitator speed controls at 40-50 rev/min, and temperature slowly rises to 40-45 DEG C;
Step 4, take the cellulase of 0.2-0.3 parts by mass, the alkaline pectase of 0.9-1.2 parts by mass, pours in agitator, and mixing speed keeps 45-50 rev/min, and temperature slowly rises to 55-60 DEG C, and keeps 15-20 minute;
Step 5, be placed under normal temperature and naturally cool.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410110163.5A CN103898769B (en) | 2014-03-24 | 2014-03-24 | The preparation method of cotton-spinning fabric scouring agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410110163.5A CN103898769B (en) | 2014-03-24 | 2014-03-24 | The preparation method of cotton-spinning fabric scouring agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103898769A CN103898769A (en) | 2014-07-02 |
| CN103898769B true CN103898769B (en) | 2016-03-02 |
Family
ID=50990327
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410110163.5A Expired - Fee Related CN103898769B (en) | 2014-03-24 | 2014-03-24 | The preparation method of cotton-spinning fabric scouring agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103898769B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104294612A (en) * | 2014-10-20 | 2015-01-21 | 苏州富美纺织科技有限公司 | Scouring agent for silk-cotton blended fabrics |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51149976A (en) * | 1975-06-17 | 1976-12-23 | Kogyo Gijutsuin | Enzymatic scouring of vegetable fiber |
| CN1528972A (en) * | 2003-10-02 | 2004-09-15 | 江南大学 | Full-cotton woven fabric bioenzyme continuous padding and decatizing pretreatment process |
| CN1712631A (en) * | 2005-07-06 | 2005-12-28 | 江南大学 | Pre-treatment of cotton fabrics by rolling and piling up of enzyme |
| CN101255655A (en) * | 2008-04-02 | 2008-09-03 | 苏州大学 | Silk broadcloth scouring agent |
| CN102978960A (en) * | 2012-12-26 | 2013-03-20 | 东华大学 | Low-alkali pretreatment method for in-situ catalytic degradation of impurities in cotton and cotton fabrics |
-
2014
- 2014-03-24 CN CN201410110163.5A patent/CN103898769B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51149976A (en) * | 1975-06-17 | 1976-12-23 | Kogyo Gijutsuin | Enzymatic scouring of vegetable fiber |
| CN1528972A (en) * | 2003-10-02 | 2004-09-15 | 江南大学 | Full-cotton woven fabric bioenzyme continuous padding and decatizing pretreatment process |
| CN1712631A (en) * | 2005-07-06 | 2005-12-28 | 江南大学 | Pre-treatment of cotton fabrics by rolling and piling up of enzyme |
| CN101255655A (en) * | 2008-04-02 | 2008-09-03 | 苏州大学 | Silk broadcloth scouring agent |
| CN102978960A (en) * | 2012-12-26 | 2013-03-20 | 东华大学 | Low-alkali pretreatment method for in-situ catalytic degradation of impurities in cotton and cotton fabrics |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103898769A (en) | 2014-07-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103898734B (en) | A kind of preparation method of silk flosssilk wadding BLENDED FABRIC scouring agent | |
| CN103911850B (en) | A kind of scouring agent being applicable to cotton-spinning fabric | |
| CN106393370A (en) | Treatment method for osier for wickerwork | |
| CN107164120A (en) | A kind of pure plant hair soap and preparation method thereof | |
| CN103898770B (en) | A kind of silk flosssilk wadding BLENDED FABRIC scouring agent | |
| CN103898769B (en) | The preparation method of cotton-spinning fabric scouring agent | |
| CN104479934A (en) | Marine alga enzyme detergent | |
| CN102660397B (en) | A kind of for washing composition cleaning underwear and preparation method thereof | |
| CN110903917A (en) | High-efficiency cleaning paste | |
| CN104650726A (en) | Thermal insulation high-elasticity waterproof paint and preparation method thereof | |
| CN107892998A (en) | A kind of washing powder of strong dirt-removing stain | |
| CN103938469A (en) | Method for preparing reactive dyeing and printing paste of linen fabric | |
| CN106751089A (en) | A kind of shock resistance high temperature resistant polystyrene cable material | |
| CN104531385A (en) | Enzyme-containing peroxide bleacher | |
| CN110257182A (en) | A kind of hyperconcetration fabric washing coagulates pearl and preparation method | |
| CN107447527A (en) | A kind of scouring agent for wollen fabrics | |
| CN108531318A (en) | A kind of preparation process of the soap containing paris polyphylla extract | |
| CN109679780A (en) | One kind is exempted to wipe seamless car washing liquid entirely | |
| CN109401861A (en) | A kind of detergent not damaging dress material with effect of color protection | |
| CN104003912B (en) | A kind of preparation method of body wash type α olefin sulfonate and application thereof | |
| CN103882773B (en) | A kind of shitosan wet strength agent and preparation method thereof | |
| CN106221956A (en) | A kind of soft detergent | |
| CN107046858A (en) | A kind of cotton seeds lint acid solution and preparation method thereof | |
| CN108795593A (en) | A kind of anti-antibacterial honeysuckle liquid detergent | |
| CN104611111A (en) | Environment-friendly cutting fluid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160302 |