CN103897882A - Preparation method of fruit and vegetable washing agent - Google Patents
Preparation method of fruit and vegetable washing agent Download PDFInfo
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- CN103897882A CN103897882A CN201210582950.0A CN201210582950A CN103897882A CN 103897882 A CN103897882 A CN 103897882A CN 201210582950 A CN201210582950 A CN 201210582950A CN 103897882 A CN103897882 A CN 103897882A
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Abstract
The invention discloses a preparation method of a fruit and vegetable washing agent. The preparation method comprises the steps: adding the following raw materials in parts by weight: 25-35 parts of alkylolamides type non-ionic surface active agent, 3-5 parts of cocoalkanoylamido propyl betaine and 8-10 parts of ethylene glycol in a reaction kettle, with a filling rate is 20-25 ml/min, and stirring after filling, with a stirring speed of 35 revolutions/min; standing for 35-45 min after stirring; and cooling at a temperature of less than 10 DEG C and a rate of 15 revolutions/min in a standing process. The fruit and vegetable washing agent produced by adopting the preparation method is capable of removing pesticide residual hazards in the surface of foods such as vegetables and fruits, and also eliminating pesticide residual hazards entering the foods, and has no toxic and side effects.
Description
Technical field
The preparation method who the present invention relates to a kind of fruits and vegetables washing composition, belongs to filed of daily-use chemical industry.
Background technology
At present, because agricultural chemicals, chemical fertilizer use in a large number in the planting process of vegetables, fruit tree, make the accumulation in a large number in these vegetable and fruits of agricultural chemicals, chemical fertilizer residual hazard, these agricultural chemicals, chemical fertilizer contain the toxic substances such as a large amount of toxic heavy metals, organophosphorus and organosulfur, the food such as the edible this vegetable and fruit that contains a large amount of agricultural chemicals, chemical fertilizer residual hazard of people, very harmful to health, threaten people's life.The method of eliminating now the residual toxicity in the food such as vegetables, fruit is to clean with the washing composition that contains alkaline matter, part residual toxicity that can only cleaning food surface, can not remove the agricultural chemicals, the chemical fertilizer residual hazard that enter in vegetables, fresh fruit cell, the alkaline matter in dawn washing composition is also poisonous to human body.
Summary of the invention
The deficiency existing for prior art, technical problem to be solved by this invention is to provide a kind of preparation method of fruits and vegetables washing composition, the agriculture chemical residual hazard of the washing composition vegetable and fruit remained on surface capable of washing of making, and with low cost, operational safety.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is that a kind of preparation method of fruits and vegetables washing composition, comprises the following steps:
(1) following material is added in reactor by weight: alkylol amide type nonionogenic tenside 25-35 part, AMONYL 380LC 3-5 part and ethylene glycol 8-10 part, filling speed is 20-25ml/ minute, after filling, stir, stirring velocity is 35 revs/min;
(2) after stirring, leave standstill, time of repose is 35-45 minute;
(3) leave standstill and carry out in process coolingly, cooling temperature, lower than 10 degrees Celsius, stirs in process of cooling, and stirring velocity is 15 revs/min;
(4) in the composition stirring later, add the material of following weight part: Sumizyme MP 2-6 part, xylene monosulfonic acid sodium solution 10-15 part, add fashionable stirring, when stirring, heat Heating temperature 45-60 degree Celsius, rate of heating 5 degrees celsius/minute;
(5) add the material of following weight part after stirring: 25 parts of vinylformic acid C1-C4 alkyl ester 10-15 part, ethylene glycol 8-10 part, 15 parts of glycerine and deionized waters, leave standstill after adding;
(6) stir after leaving standstill, stirring velocity 45-50 rev/min, carries out coolingly after stirring, and cooling temperature is lower than 5 degrees Celsius;
(7) cooled and filtered, leaves standstill and is greater than 35 minutes after filtering.
Optimize, the preparation method of above-mentioned fruits and vegetables washing composition, in its step (7), dwell temperature is less than 30 degrees Celsius.
The washing composition that method of the present invention is produced can be removed the residual toxicity in the food surfaces such as vegetables, fruit, also can remove the residual toxicity having entered in food, uses washing composition without any Side effect simultaneously.
Embodiment
embodiment 1
The present invention is a kind of preparation method of fruits and vegetables washing composition, comprises the following steps:
(1) following material is added in reactor by weight: 8 parts of 25 parts of alkylol amide type nonionogenic tensides, 3 parts of AMONYL 380LC and ethylene glycol, filling speed is 20ml/ minute, after filling, stir, stirring velocity is 35 revs/min;
(2) after stirring, leave standstill, time of repose is 35 minutes;
(3) leave standstill and carry out in process coolingly, cooling temperature, lower than 10 degrees Celsius, stirs in process of cooling, and stirring velocity is 15 revs/min;
(4) in the composition stirring later, add the material of following weight part: 2 parts of Sumizyme MPs, 10 parts of xylene monosulfonic acid sodium solutions, add fashionable stirring, when stirring, heat 45 degrees Celsius of Heating temperatures, rate of heating 5 degrees celsius/minute;
(5) add the material of following weight part after stirring: 25 parts of 10 parts of vinylformic acid C1-C4 alkyl esters, 8 parts of ethylene glycol, 15 parts of glycerine and deionized waters, leave standstill after adding;
(6) stir after leaving standstill, 45 revs/min of stirring velocitys, carry out coolingly after stirring, and cooling temperature is lower than 5 degrees Celsius;
(7) cooled and filtered, leaves standstill and is greater than 35 minutes after filtering, and in its step (7), dwell temperature is less than 30 degrees Celsius.
embodiment 2
The present invention is a kind of preparation method of fruits and vegetables washing composition, comprises the following steps:
(1) following material is added in reactor by weight: 10 parts of 35 parts of alkylol amide type nonionogenic tensides, 5 parts of AMONYL 380LC and ethylene glycol, filling speed is 25ml/ minute, after filling, stir, stirring velocity is 35 revs/min;
(2) after stirring, leave standstill, time of repose is 45 minutes;
(3) leave standstill and carry out in process coolingly, cooling temperature, lower than 10 degrees Celsius, stirs in process of cooling, and stirring velocity is 15 revs/min;
(4) in the composition stirring later, add the material of following weight part: 6 parts of Sumizyme MPs, 15 parts of xylene monosulfonic acid sodium solutions, add fashionable stirring, when stirring, heat 60 degrees Celsius of Heating temperatures, rate of heating 5 degrees celsius/minute;
(5) add the material of following weight part after stirring: 25 parts of 15 parts of vinylformic acid C1-C4 alkyl esters, 10 parts of ethylene glycol, 15 parts of glycerine and deionized waters, leave standstill after adding;
(6) stir after leaving standstill, 50 revs/min of stirring velocitys, carry out coolingly after stirring, and cooling temperature is lower than 5 degrees Celsius;
(7) cooled and filtered, leaves standstill and is greater than 35 minutes after filtering, and in its step (7), dwell temperature is less than 30 degrees Celsius.
The washing composition that method of the present invention is produced can be removed the residual toxicity in the food surfaces such as vegetables, fruit, also can remove the residual toxicity having entered in food, uses washing composition without any Side effect simultaneously.
Certainly, above-mentioned explanation is not limitation of the present invention, and the present invention is also not limited to above-mentioned giving an example; those skilled in the art; in essential scope of the present invention, variation, remodeling, interpolation or the replacement made, all should belong to protection scope of the present invention.。
Claims (2)
1. a preparation method for fruits and vegetables washing composition, comprises the following steps:
(1) following material is added in reactor by weight: alkylol amide type nonionogenic tenside 25-35 part, AMONYL 380LC 3-5 part and ethylene glycol 8-10 part, filling speed is 20-25ml/ minute, after filling, stir, stirring velocity is 35 revs/min;
(2) after stirring, leave standstill, time of repose is 35-45 minute;
(3) leave standstill and carry out in process coolingly, cooling temperature, lower than 10 degrees Celsius, stirs in process of cooling, and stirring velocity is 15 revs/min;
(4) in the composition stirring later, add the material of following weight part: Sumizyme MP 2-6 part, xylene monosulfonic acid sodium solution 10-15 part, add fashionable stirring, when stirring, heat Heating temperature 45-60 degree Celsius, rate of heating 5 degrees celsius/minute;
(5) add the material of following weight part after stirring: 25 parts of vinylformic acid C1-C4 alkyl ester 10-15 part, ethylene glycol 8-10 part, 15 parts of glycerine and deionized waters, leave standstill after adding;
(6) stir after leaving standstill, stirring velocity 45-50 rev/min, carries out coolingly after stirring, and cooling temperature is lower than 5 degrees Celsius;
(7) cooled and filtered, leaves standstill and is greater than 35 minutes after filtering.
2. the preparation method of fruits and vegetables washing composition according to claim 1, is characterized in that: in described step (7), dwell temperature is less than 30 degrees Celsius.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210582950.0A CN103897882A (en) | 2012-12-28 | 2012-12-28 | Preparation method of fruit and vegetable washing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210582950.0A CN103897882A (en) | 2012-12-28 | 2012-12-28 | Preparation method of fruit and vegetable washing agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103897882A true CN103897882A (en) | 2014-07-02 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210582950.0A Pending CN103897882A (en) | 2012-12-28 | 2012-12-28 | Preparation method of fruit and vegetable washing agent |
Country Status (1)
| Country | Link |
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| CN (1) | CN103897882A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021140390A1 (en) | 2020-01-06 | 2021-07-15 | Vinay Bhalchandra PARANJPE | A vegetable and fruit wash composition and uses thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5500143A (en) * | 1993-11-01 | 1996-03-19 | The Procter & Gamble Company | Cleaning compositions for produce |
| CN1405288A (en) * | 2001-08-20 | 2003-03-26 | 潘灿平 | Detergent composition |
| CN1865422A (en) * | 2006-03-30 | 2006-11-22 | 中国日用化学工业研究院 | Detergent for washing dishware with hand and its preparation method |
| CN101649258A (en) * | 2009-08-31 | 2010-02-17 | 广州立白企业集团有限公司 | Tableware detergent with enzyme and preparation method thereof |
| CN102382727A (en) * | 2010-07-19 | 2012-03-21 | 罗门哈斯公司 | Polymers for laundry detergents |
-
2012
- 2012-12-28 CN CN201210582950.0A patent/CN103897882A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5500143A (en) * | 1993-11-01 | 1996-03-19 | The Procter & Gamble Company | Cleaning compositions for produce |
| CN1405288A (en) * | 2001-08-20 | 2003-03-26 | 潘灿平 | Detergent composition |
| CN1865422A (en) * | 2006-03-30 | 2006-11-22 | 中国日用化学工业研究院 | Detergent for washing dishware with hand and its preparation method |
| CN101649258A (en) * | 2009-08-31 | 2010-02-17 | 广州立白企业集团有限公司 | Tableware detergent with enzyme and preparation method thereof |
| CN102382727A (en) * | 2010-07-19 | 2012-03-21 | 罗门哈斯公司 | Polymers for laundry detergents |
Non-Patent Citations (2)
| Title |
|---|
| 徐宝财、周雅文、韩富: "《家用洗涤剂生产及配方》", 31 May 2008, article "洗涤剂生产工艺", pages: 116 - 5 * |
| 王慎敏、刘莹、姜文勇: "《洗涤剂配方设计、制备工艺与配方实例》", 30 April 2003, article "液体洗涤剂制备", pages: 183-184 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021140390A1 (en) | 2020-01-06 | 2021-07-15 | Vinay Bhalchandra PARANJPE | A vegetable and fruit wash composition and uses thereof |
| US11744269B2 (en) | 2020-01-06 | 2023-09-05 | Vinay Bhalchandra PARANJPE | Vegetable and fruit wash formulation and uses thereof |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140702 |