CN103865314B - A kind of printing ink washing agent and preparation method thereof - Google Patents
A kind of printing ink washing agent and preparation method thereof Download PDFInfo
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- CN103865314B CN103865314B CN201410067417.XA CN201410067417A CN103865314B CN 103865314 B CN103865314 B CN 103865314B CN 201410067417 A CN201410067417 A CN 201410067417A CN 103865314 B CN103865314 B CN 103865314B
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- diethylene glycol
- auxiliary agent
- acid
- printing ink
- butyl
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- 238000007639 printing Methods 0.000 title claims abstract description 16
- 238000005406 washing Methods 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 13
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000003350 kerosene Substances 0.000 claims abstract description 9
- 239000002253 acid Substances 0.000 claims abstract description 8
- CRWNQZTZTZWPOF-UHFFFAOYSA-N 2-methyl-4-phenylpyridine Chemical compound C1=NC(C)=CC(C=2C=CC=CC=2)=C1 CRWNQZTZTZWPOF-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims abstract description 7
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims abstract description 7
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 7
- 229940028356 diethylene glycol monobutyl ether Drugs 0.000 claims abstract description 7
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims abstract description 7
- JCGNDDUYTRNOFT-UHFFFAOYSA-N oxolane-2,4-dione Chemical compound O=C1COC(=O)C1 JCGNDDUYTRNOFT-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- RYCLIXPGLDDLTM-UHFFFAOYSA-J tetrapotassium;phosphonato phosphate Chemical compound [K+].[K+].[K+].[K+].[O-]P([O-])(=O)OP([O-])([O-])=O RYCLIXPGLDDLTM-UHFFFAOYSA-J 0.000 claims abstract description 7
- IVKNZCBNXPYYKL-UHFFFAOYSA-N 2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[4-(2,4,4-trimethylpentan-2-yl)phenoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethanol Chemical compound CC(C)(C)CC(C)(C)C1=CC=C(OCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO)C=C1 IVKNZCBNXPYYKL-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- XDLMVUHYZWKMMD-UHFFFAOYSA-N 3-trimethoxysilylpropyl 2-methylprop-2-enoate Chemical compound CO[Si](OC)(OC)CCCOC(=O)C(C)=C XDLMVUHYZWKMMD-UHFFFAOYSA-N 0.000 claims description 6
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 6
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 230000008878 coupling Effects 0.000 claims description 6
- 238000010168 coupling process Methods 0.000 claims description 6
- 238000005859 coupling reaction Methods 0.000 claims description 6
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 6
- 229960003656 ricinoleic acid Drugs 0.000 claims description 6
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 6
- 229910000077 silane Inorganic materials 0.000 claims description 6
- KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 5
- 230000000254 damaging effect Effects 0.000 abstract description 2
- 239000002761 deinking Substances 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 231100000419 toxicity Toxicity 0.000 abstract description 2
- 230000001988 toxicity Effects 0.000 abstract description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 239000003502 gasoline Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 1
- 229940043350 citral Drugs 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 230000002522 swelling effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of printing ink washing agent, it is characterized in that, be made up of the raw material of following weight part: disodium ethylene diamine tetraacetate 3-4, OP-10? 3-4, kerosene 20-24, potassium pyrophosphate 3-4, diethylene glycol monobutyl ether 10-12, citric acid 3-4, oxysuccinic acid 4-5, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate 2-3, auxiliary agent 4-5, water 100-110; The present invention adds auxiliary agent, improves the processing performance of clean-out system, reduces its toxic side effect and the pollution to environment; Cleaning performance of the present invention is good, and speed is fast, and do not need heating during deinking, volatility is little, and toxicity is extremely low, and to human body fanout free region, environmental pollution is little, and little to printing equipment damaging action, easy to use.
Description
Technical field
The present invention relates to printing cleaning technique field, particularly a kind of printing ink washing agent and preparation method thereof.
Background technology
What often use now in printing industry has the element purge of ink to be clean with organic solvents such as gasoline, kerosene, acetone, alcohol for printing machinery forme, rubber roll, blanket etc.; Such clean-out system also exists inflammable, explosive, contaminate environment, harm bedding sack is healthy, and to cleaning part, as: glue rod, blanket surface burn into swelling action, to parts damages, work-ing life shortens widely, simultaneously to the workman's skin of hand burn into injury using solvent, this solvent cleaning weak effect, gasoline, coal are the products of petroleum refining, and present ballooning oil prices can cause the waste of Nonrenewable resources petroleum-based energy like this.At present, the widely used clean-out system in market, be not be exactly in alkalescence in acidity, can have a strong impact on original true qualities and smooth finish in acid clean-out system, the clean-out system in alkalescence can permeate cleaning objects, causes object to corrode, even comes off.
Chinese patent 200510122330.9 discloses a kind of natural plant type detergent, it is characterized in that by limonene 60 ~ 80 parts, 10 ~ 20 parts, turps, propylene glycol phenylate 10 ~ 15 parts, Terpineol 350 5 ~ 10 parts, citral 1 ~ 3 part, the natural plant solvent that Homogeneous phase mixing is formulated and emulsifying agent mixing composition.But this clean-out system is not invented for cleaning printing-ink, so the effect of its cleaning printing-ink is also short of to some extent.
Summary of the invention
The object of this invention is to provide a kind of printing ink washing agent and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of printing ink washing agent, is made up of the raw material of following weight part: disodium ethylene diamine tetraacetate 3-4, OP-103-4, kerosene 20-24, potassium pyrophosphate 3-4, diethylene glycol monobutyl ether 10-12, citric acid 3-4, oxysuccinic acid 4-5, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate 2-3, auxiliary agent 4-5, water 100-110;
Described auxiliary agent is made up of the raw material of following weight part: Silane coupling reagent KH-570 2-3, ricinolic acid 2-3, tea-polyphenol 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, oxidation inhibitor 10351-2, ethanol 15-18; Preparation method is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 60-70 DEG C, stirs after 20-30 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minutes, to obtain final product.
Printing ink washing agent of the present invention, be made up of following concrete steps:
(1) at room temperature kerosene, potassium pyrophosphate, diethylene glycol monobutyl ether, citric acid, oxysuccinic acid are added in mixing kettle, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, be stirred to and dissolve completely;
(2) disodium ethylene diamine tetraacetate, OP-10, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-6 minute with the speed of 1300-1400 rev/min;
(3) finally auxiliary agent and all the other remaining components are added in mixing kettle, stir, naturally cooling.
Excellent effect of the present invention is: the present invention adds auxiliary agent, improves the processing performance of clean-out system, reduces its toxic side effect and the pollution to environment; Cleaning performance of the present invention is good, and speed is fast, and do not need heating during deinking, volatility is little, and toxicity is extremely low, and to human body fanout free region, environmental pollution is little, and little to printing equipment damaging action, easy to use.
Embodiment
Below by specific examples, the present invention is described in detail.
A kind of printing ink washing agent, is made up of the raw material of following weight part (kilogram): disodium ethylene diamine tetraacetate 3, OP-103, kerosene 20, potassium pyrophosphate 3, diethylene glycol monobutyl ether 10, citric acid 3, oxysuccinic acid 4, diethylene glycol dibutyl ether 4, butyl (tetra) titanate 2, auxiliary agent 4, water 100;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): Silane coupling reagent KH-570 3, ricinolic acid 2, tea-polyphenol 2, glyceryl monostearate 4, neopentyl glycol 2, p-tert-butyl benzoic acid 4, oxidation inhibitor 10351, ethanol 15; Preparation method is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 60-70 DEG C, stirs after 20-30 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minutes, to obtain final product.
Printing ink washing agent of the present invention, be made up of following concrete steps:
(1) at room temperature kerosene, potassium pyrophosphate, diethylene glycol monobutyl ether, citric acid, oxysuccinic acid are added in mixing kettle, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, be stirred to and dissolve completely;
(2) disodium ethylene diamine tetraacetate, OP-10, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-6 minute with the speed of 1300-1400 rev/min;
(3) finally auxiliary agent and all the other remaining components are added in mixing kettle, stir, naturally cooling.
Be applied to by ink on the stainless steel metal thin slice of certain mass, dry under state of nature, steel disc is placed in the beaker filling clean-out system, soak after 5 minutes at 25 DEG C, more at the uniform velocity vibrate 5 minutes, obtaining clean dirt rate is 93.4%, and cleansing power is good.With this clean-out system with compared with gasoline, kerosene, rubber cloth increases the service life 2 years, and ink roller can increase the service life 3 years.
Claims (1)
1. a printing ink washing agent, it is characterized in that, be made up of the raw material of following weight part: disodium ethylene diamine tetraacetate 3-4, OP-103-4, kerosene 20-24, potassium pyrophosphate 3-4, diethylene glycol monobutyl ether 10-12, citric acid 3-4, oxysuccinic acid 4-5, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate 2-3, auxiliary agent 4-5, water 100-110;
Described auxiliary agent is made up of the raw material of following weight part: Silane coupling reagent KH-570 2-3, ricinolic acid 2-3, tea-polyphenol 2-3, glyceryl monostearate 4-5, neopentyl glycol 2-3, p-tert-butyl benzoic acid 3-4, oxidation inhibitor 10351-2, ethanol 15-18; The preparation method of described auxiliary agent is by Silane coupling reagent KH-570, ricinolic acid, ethanol mixing, is heated to 60-70 DEG C, stirs after 20-30 minute, then add other remaining component, be warming up to 80-85 DEG C, stir 30-40 minutes, to obtain final product;
Described printing ink washing agent, be made up of following concrete steps:
(1) at room temperature kerosene, potassium pyrophosphate, diethylene glycol monobutyl ether, citric acid, oxysuccinic acid are added in mixing kettle, add in mixing kettle after the water of half amount is heated to 65-75 DEG C, be stirred to and dissolve completely;
(2) disodium ethylene diamine tetraacetate, OP-10, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate are added in mixing kettle, add the water being heated to 80-90 DEG C of surplus, stir 4-6 minute with the speed of 1300-1400 rev/min;
(3) finally auxiliary agent is added in mixing kettle, stir, naturally cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410067417.XA CN103865314B (en) | 2014-02-27 | 2014-02-27 | A kind of printing ink washing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410067417.XA CN103865314B (en) | 2014-02-27 | 2014-02-27 | A kind of printing ink washing agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103865314A CN103865314A (en) | 2014-06-18 |
| CN103865314B true CN103865314B (en) | 2016-04-27 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410067417.XA Active CN103865314B (en) | 2014-02-27 | 2014-02-27 | A kind of printing ink washing agent and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN103865314B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104830141B (en) * | 2015-04-30 | 2017-04-12 | 南京信息工程大学 | Microemulsion printing ink cleaner and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088952A (en) * | 1992-12-26 | 1994-07-06 | 化工部北京化工研究院 | Emulsion type high-efficiency non-toxic ink remover |
| CN103525161A (en) * | 2013-10-23 | 2014-01-22 | 合肥环照高分子材料厂 | High-efficiency printing ink cleaning agent and preparation method thereof |
-
2014
- 2014-02-27 CN CN201410067417.XA patent/CN103865314B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088952A (en) * | 1992-12-26 | 1994-07-06 | 化工部北京化工研究院 | Emulsion type high-efficiency non-toxic ink remover |
| CN103525161A (en) * | 2013-10-23 | 2014-01-22 | 合肥环照高分子材料厂 | High-efficiency printing ink cleaning agent and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103865314A (en) | 2014-06-18 |
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| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
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Address after: Seven road 236112 Anhui city in Fuyang Province Economic Development Zone No. 99 Ying Ying Patentee after: ANHUI YINGMEI TECHNOLOGY CO.,LTD. Address before: Seven road 236112 Anhui city in Fuyang Province Economic Development Zone No. 99 Ying Ying Patentee before: ANHUI YINGMEI COLOR PRINTING & PACKAGING Co.,Ltd. |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A printing ink cleaning agent and its preparation method Granted publication date: 20160427 Pledgee: Fuyang City Yingzhou financing Company limited by guarantee Pledgor: ANHUI YINGMEI TECHNOLOGY CO.,LTD. Registration number: Y2024980032966 |