CN103860395A - Preparation method of skin smearing shower gel containing enteromorpha polysaccharide - Google Patents

Preparation method of skin smearing shower gel containing enteromorpha polysaccharide Download PDF

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Publication number
CN103860395A
CN103860395A CN201410096650.0A CN201410096650A CN103860395A CN 103860395 A CN103860395 A CN 103860395A CN 201410096650 A CN201410096650 A CN 201410096650A CN 103860395 A CN103860395 A CN 103860395A
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China
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skin
powder
parts
entermorpha
enteromorpha
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CN201410096650.0A
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CN103860395B (en
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李霞
刘玉凤
郝再彬
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Guilin University of Technology
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Guilin University of Technology
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Abstract

The invention discloses a preparation method of skin smearing shower gel containing enteromorpha polysaccharide. The preparation method comprises the following steps: (1) cleaning and drying enteromorpha; grinding and sieving the enteromorpha through a 100-mesh sieve; (2) adding distilled water which is 20ml/g of mass of the enteromorpha; refluxing and extracting at 90 DEG C for 2 hours, filtering, and separating residue from the extracting solution; (3) processing the residue (4) according to the step (2) twice; (4) mixing the extracting solutions, condensing and freeze-drying to obtain enteromorpha polysaccharide powder; (5) mixing the following raw materials in parts by weight: 1-5 parts of olive oil, 1-5 parts of glycerol and 1-5 parts of rosemary essential oil, to obtain a mixed solution; (6) heating 70-90 parts by weight of distilled water to 70-90 DEG C, adding 1-10 parts by weight of enteromorpha polysaccharide powder, dropwise adding the mixed solution, regulating pH value to 5.5-6.5 through citric acid, and condensing. The shower gel disclosed by the invention has functions of resisting bacteria, nourishing and protecting skin, replenishing skin water, regulating metabolic balance of skin cells so that the skin is glossy, fine, smooth and elastic and the functions of losing weight, resisting ultraviolet rays and the like are also achieved.

Description

A kind of preparation method containing sea grass polysaccharide skin film bath foam
Technical field
The present invention relates to a kind of special bath foam technical field, particularly a kind of preparation method of the bath foam containing sea grass polysaccharide, belongs to the research and development of health care product.
Background technology
Entermorpha is the wild chlorella in the beach of coastal waters, and its natural propagation ability is strong especially, and output is huge.It is distributed in river mouth, middle damp marsh of being with widely, also can grow nonparasitically upon another plant on the frond of tangleweed.Entermorpha is a kind of important economical alga of Chlorophyta Ulvaceae, sea grass polysaccharide be the important pharmacological active substance of marine algae it.Sea grass polysaccharide is mainly made up of monosaccharide such as rhamnose, xylose, glucoses (a small amount of mannose, galactose, arabinose), and contains alduronic acid and sulfate, and polysaccharide main chain contains multiple connection of bonding.
The nutritive value of Entermorpha is higher, record according to " occupying diet spectrum with breath ": Entermorpha " gallbladder that disappears, the scrofula goiter that disappears, let out swollen, reduce phlegm, control being not acclimatized ", coastal spreading so far controlled acute and chronic gastroenteritis with the decoction of ulva class, and relieve summer heating Detoxication beverage is made Entermorpha in Guangdong.Medicinal part: Quan Zao.Nature,taste and action: salty, cold, hard masses softening and resolving, heat-clearing and toxic substances removing.Cure mainly: paronychia, lymphonodi cervicales are swollen, carbuncle on the back, furuncle.Modern pharmacology proves that sea grass polysaccharide has the effects such as antitumor, antioxidation, anticoagulation, antibacterial, antiviral, adjusting immunity and anti-inflammatory activity, blood fat reducing, moisturizing.
Because sea grass polysaccharide has viscosity, the debita spissitudo under tepid state can form green environmental friendly coatings, it is coated in to skin surface by the form of taking a shower and forms thin film, and other active effective ingredient of polysaccharide and compatibility thereof is absorbed by the skin, enters blood lentamente; Dissolve simultaneously polysaccharide the supply of moisture slow release ground skin, arrive skin moistening object.This patent is especially applicable to skin nursing, the maintenance under dry environment.
Bath foam is to pass through temperature, utilize the several functions such as imperial heresy, secretion, absorption, infiltration, excretion, sensation of skin, act on skin, muscle, joint, improve three metabolism, strengthen its function, and the absorption by skin to medicine, keep healthy for part and whole body, mediation whole body QI and blood, has no side effect.
Through retrieval, all do not contain at present the skin skin film bath foam of sea grass polysaccharide as raw material both at home and abroad.
Summary of the invention
The object of the invention is to provide a kind of preparation method of the skin film bath foam containing sea grass polysaccharide.
Selecting sea grass polysaccharide is primary raw material, is equipped with Fructus Canarii albi wet goods adjuvant, and be processed into through science there is antibacterial, nutrition protection skin, and for supplementing skin moisture; The metabolic balance of regulation of skin cell, makes skin gloss exquisiteness and high resilience; Also contribute to the multi-efficiencies such as fat-reducing and ultraviolet rays resistance.
Concrete steps are:
(1) Entermorpha is cleaned, dried to constant weight; Pulverize, cross 100 mesh sieves, obtain Entermorpha powder.
(2) in step (1) gained Entermorpha powder, add distilled water in the quality 20mL/g of Entermorpha powder, 90 DEG C of reflux, extract, 2 hours, filter, and separate residue and extracting solution.
(3) the residue replacement Entermorpha powder of getting step (2) repeats the step of (2).
(4) the residue replacement Entermorpha powder of getting step (3) repeats the step of (2).
(5) merge said extracted liquid, remove part water through vacuum concentration, after lyophilization, obtain sea grass polysaccharide powder, save backup in 4 DEG C.
(6) weight portion is respectively: the raw material of olive oil 1-5, glycerol 1-5 and rosemary ethereal oil 1-5 is mixed to get mixed liquor.
(7) distilled water that is 70-90 by weight portion is warming up to 70-90 DEG C, adding weight portion is the sea grass polysaccharide powder of step (5) gained of 1-10, stirring makes it all be uniformly dissolved rear dropping step (6) gained mixed liquor, make it form stable solution, then use Fructus Citri Limoniae acid for adjusting pH to 5.5-6.5, stir, concentrated, must contain sea grass polysaccharide skin film bath foam, be distributed into multiple aliquots under aseptic.
The obtained sea grass polysaccharide skin film bath foam sea grass polysaccharide content that contains is not less than 1%, and polyoses content detects and carries out according to national standard or industry standard, optical analysis or high performance liquid chromatography.
The invention has the beneficial effects as follows: there is antibacterial, nutrition protection skin, and for supplementing skin moisture; The metabolic balance of regulation of skin cell, makes skin gloss exquisiteness and high resilience; Also contribute to the multi-efficiencies such as fat-reducing and ultraviolet rays resistance.
Product of the present invention is in ensureing sea grass polysaccharide special efficacy, is furnished with multiple natural materials, effective ingredient is wherein under the heating power of hot water, penetrate into skin, absorbed by blood capillary, enter blood circulation of human body system, thereby reach the effect of improving body constitution, blood circulation promoting, be a kind of well health care product, allow consumer there is more selection, be suitable for and promote the use of.
Detailed description of the invention
Embodiment:
(1) Entermorpha raw material is cleaned, dried to constant weight; Pulverize, cross 100 mesh sieves, obtain Entermorpha powder.
(2) in 6.5 kilograms of steps (1) gained Entermorpha powder, add the distilled water of 13000mL, 90 DEG C of reflux, extract, 2 hours, filter, and separate residue and extracting solution.
(3) the residue replacement Entermorpha powder of getting step (2) repeats the step of (2).
(4) the residue replacement Entermorpha powder of getting step (3) repeats the step of (2).
(5) merge said extracted liquid, remove part water through vacuum concentration, realize the preparation of concentrated solution; After concentrated solution lyophilization sea grass polysaccharide powder, save backup sea grass polysaccharide yield 12% in 4 DEG C.
(6) 0.1 kilogram of olive oil, 0.1 kilogram of glycerol and 0.1 kilogram of rosemary ethereal oil mix homogeneously are obtained to mixed liquor.
(7) 10 kilograms of distilled water are warming up to 90 DEG C, add step (5) gained sea grass polysaccharide powder, stirring makes it all be uniformly dissolved the mixed liquor of rear dropping step (6) gained, make it form stable solution, then use Fructus Citri Limoniae acid for adjusting pH to 6.0, stir, be concentrated into 10 kilograms, must contain sea grass polysaccharide skin film bath foam, be distributed under aseptic 4 parts for subsequent use.

Claims (1)

1. containing a preparation method for sea grass polysaccharide skin film bath foam, it is characterized in that concrete steps are:
(1) Entermorpha is cleaned, dried to constant weight; Pulverize, cross 100 mesh sieves, obtain Entermorpha powder;
(2) in step (1) gained Entermorpha powder, add distilled water in the quality 20mL/g of Entermorpha powder, 90 DEG C of reflux, extract, 2 hours, filter, and separate residue and extracting solution;
(3) the residue replacement Entermorpha powder of getting step (2) repeats the step of (2);
(4) the residue replacement Entermorpha powder of getting step (3) repeats the step of (2);
(5) merge said extracted liquid, remove part water through vacuum concentration, after lyophilization, obtain sea grass polysaccharide powder, save backup in 4 DEG C;
(6) weight portion is respectively: the raw material of olive oil 1-5, glycerol 1-5 and rosemary ethereal oil 1-5 is mixed to get mixed liquor;
(7) distilled water that is 70-90 by weight portion is warming up to 70-90 DEG C, adding weight portion is the sea grass polysaccharide powder of step (5) gained of 1-10, stirring makes it all be uniformly dissolved rear dropping step (6) gained mixed liquor, make it form stable solution, then use Fructus Citri Limoniae acid for adjusting pH to 5.5-6.5, stir, concentrated, must contain sea grass polysaccharide skin film bath foam.
CN201410096650.0A 2014-03-17 2014-03-17 A kind of preparation method containing sea grass polysaccharide skin film bath foam Expired - Fee Related CN103860395B (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101697944A (en) * 2007-12-18 2010-04-28 王春霞 Biological chitosan activin antibacterial bath cream
CN103396499A (en) * 2013-08-14 2013-11-20 上海海洋大学 Enteromorpha prolifera polysaccharide, and extraction method and application thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101697944A (en) * 2007-12-18 2010-04-28 王春霞 Biological chitosan activin antibacterial bath cream
CN103396499A (en) * 2013-08-14 2013-11-20 上海海洋大学 Enteromorpha prolifera polysaccharide, and extraction method and application thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
赵素芬 等: "三种绿藻多糖的提取及理化性质和活性比较", 《台湾海峡》 *

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