CN103815129B - The feed processing technology of sulphur resources in a kind of quick removal rapeseed dregs - Google Patents

The feed processing technology of sulphur resources in a kind of quick removal rapeseed dregs Download PDF

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Publication number
CN103815129B
CN103815129B CN201410069566.XA CN201410069566A CN103815129B CN 103815129 B CN103815129 B CN 103815129B CN 201410069566 A CN201410069566 A CN 201410069566A CN 103815129 B CN103815129 B CN 103815129B
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rapeseed dregs
rapeseed
dregs
sulphur
steam
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CN103815129A (en
Inventor
贺永惠
王清华
刘兴友
张慧辉
苗志国
崔艳红
王艳荣
刘保国
常新耀
魏刚才
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Henan Institute of Science and Technology
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Henan Institute of Science and Technology
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Abstract

Rapeseed dregs is the unconventional protein feed resource of one of aquaculture, and glucosinolate (being called for short sulphur glycosides) content is the bottleneck limiting its extensive use.The present invention utilizes a kind of new feed processing technology---Steam explosion treatment technology, the sulphur glycosides of the overwhelming majority in rapeseed dregs can be removed fast and efficiently.Pretreatment adds water to make rapeseed dregs aquation a period of time; Add pretreatment rapeseed dregs in the feed bin of steam blasting instrument, under specific pressure, process certain hour; The sulphur glycosides of in rapeseed dregs 87.2% can be removed after explosion.Compared with prior art, this technology has the features such as pretreatment is simple, the time is short, efficiency is high, pollution-free, is conducive to carrying out detoxification from rapeseed dregs raw material beginning of production.

Description

The feed processing technology of sulphur resources in a kind of quick removal rapeseed dregs
Technical field
The invention belongs to feed processing technology, be specifically related to a kind of feed processing technology removing glucosinolate in rapeseed dregs (being called for short sulphur glycosides) content fast.
Background technology
Protein feed resource shortage is the subject matter that China's animal husbandry and feed industrial development face, and supply demand gap is large, needs a large amount of import.China produces dregs of rapeseed cake per year and reaches more than 7,000,000 tons, but obtains 30% of the grouts inadequate resource total amount of efficiency utilization for a long time.There is very large gap in the actual demand of this situation and feedstuff industry, aquaculture and even agricultural development, therefore, is badly in need of carrying out rapeseed dregs efficiency utilization key technology research in a deep going way.The crude protein content of rapeseed dregs is higher, and reach about 34% ~ 38%, crude fiber content is higher, reaches about 12% ~ 13%.Poisonous and harmful element in rapeseed dregs is sulphur glucoside mainly, sulphur glucoside itself is nontoxic, its catabolite is isothiocyanates and oxazolidine thione mainly, the disorder of animal Thyroid Gland Swell, thyroxine secretion and liver enlargement can be caused, hepatosis, thus impact is grown and production performance, is even poisoned to death.In addition sulphur glucoside has acid, can reduce the appetite of animal, reduces the nutritive value of rapeseed dregs, thus limits its extensive use.
The method of the detoxification of rapeseed dregs mainly soil buries method, infusion method, alkali lye neutralisation, expanded method and fermentable process.Although these processing methods have certain effect, but virus elimination rate height differs, also exist: after detoxification, the loss of rapeseed dregs nutriment is larger, as caused protein denaturation, solubility reduces, protein digestibility declines, some water miscible nutriments run off, thermo-responsive nutriment is destroyed, mineral element loss etc. because of alkali effect; Waste liquid after detoxification easily causes water body environment pollution; Operating equipment relative complex, production cost is higher; After detoxification, the palatability of rapeseed dregs is poor, there is detoxifying agent residue problem.Although microbe fermentation method has the advantages such as detoxification efficiency is obvious, fermentation microorganism used therefor must meet the restriction of country to microorganism fodder, and the processing time is long, and there is excellent species and be difficult to problems such as cultivating, conservation is difficult.This area is in the urgent need to a kind of method overcoming sulphur resources in the quick removal rapeseed dregs of above-mentioned shortcoming.
Summary of the invention
The invention provides the method for glucosinolate content in a kind of quick removal rapeseed dregs, comprise the steps:
(1) in rapeseed dregs, add water, place until the abundant aquation of rapeseed dregs;
(2) steam regulation explosion instrument, after reaching specific steam pressure, by step 1) rapeseed dregs that obtains puts into the feed bin of steam blasting instrument, and dimension pressure 30 ~ 90 seconds, carries out explosion.
In one embodiment, said method also comprises the steps:
Collect described step 2) sample that obtains, it is dried and pulverization process, obtains virus-free rapeseed meal.
In a preferred embodiment, the amount adding water described in described step (1) is with 20 ~ 40% of described rapeseed dregs weighing scale.More preferably, the amount adding water described in described step (1) is with 25 ~ 30% of described rapeseed dregs weighing scale.
In a preferred embodiment, the time of placing described in described step (1) is 1 ~ 20 hour.More preferably, the time of placing described in described step (1) is 8 ~ 15 hours.
In a preferred embodiment, the steam pressure in described step (2) is 0.5 ~ 3.0MPa.More preferably, the steam pressure in described step (2) is 0.8 ~ 2.5MPa.Especially preferably, the steam pressure in described step (2) is 1.0 ~ 2.0MPa.
In a preferred embodiment, the Steam explosion treatment time in described step (2) is 15 seconds ~ 120 seconds.More preferably, the Steam explosion treatment time in described step (2) is 30 ~ 90 seconds.Especially preferably, the Steam explosion treatment time in described step (2) is 60 ~ 90 seconds.
In a preferred embodiment, the present invention can remove the sulphur glycosides of in rapeseed dregs 74%.More preferably, the sulphur glycosides of in rapeseed dregs 87.2% can be removed.
The present invention has the features such as pretreatment is simple, the time is short, efficiency is high, pollution-free, overcomes that virus elimination rate in prior art is low, the processing time is long, requires high, to reduce feed palatability, excellent species conservation difficulty, detoxification high in cost of production problem to the anticorrosive of equipment.Specifically, the present invention only needs the humidity adjusting rapeseed dregs with water, carry out the hydration process of some hours in room temperature, do not exist and pollute and corrosion, do not affect the palatability of feed, do not need to control fermentation temperature, Steam explosion treatment equipment needs disposable infusion of financial resources, and energy consumption only needs water, electricity, liquefied gas, only needs the processing time of about 1 minute, can remove the sulphur glycosides of in rapeseed dregs 87.2%, comprehensive benefit is the highest.
Accompanying drawing explanation
Fig. 1 provides the result of the test of embodiment 1.
Detailed description of the invention
In order to better the present invention is described, be convenient to understand technical scheme of the present invention, typical but non-limiting embodiment of the present invention is as follows:
Embodiment
In rapeseed dregs, add water to fully wetting, open QBS-80B steam blasting instrument, steam pressure is adjusted to required vapor pressure, wet-mixing rapeseed dregs is added feed bin, dimension pressure a period of time, carry out explosion; Collect the sample after explosion treatment, dry, pulverize, namely complete the detoxification treatment of rapeseed dregs.Fig. 1 gives the result of 6 process, and wherein ratio of water to material (weight ratio of water and rapeseed dregs) is followed successively by 10%, 20%, 25%, 30%, 40%; Hydration time is for being followed successively by 4,6,8,10,12,15 hours; Process pressure is followed successively by 0.8,1.0,1.5,1.8,2.0,2.5MPa; The dimension pressure time is followed successively by 15,30,60,90,120 seconds; NY/T1582-2007 method is adopted to detect the content of sulphur glycosides in virus-free rapeseed meal after process.Result shows, the inventive method can remove the sulphur resources of in rapeseed dregs 87.2%, and detoxification efficiency is obvious.
Applicant states, the present invention illustrates method detailed of the present invention by above-described embodiment, but the present invention is not limited to above-mentioned method detailed, does not namely mean that the present invention must rely on above-mentioned method detailed and could implement.Person of ordinary skill in the field should understand, any improvement in the present invention, to equivalence replacement and the interpolation of auxiliary element, the concrete way choice etc. of each raw material of product of the present invention, all drops within protection scope of the present invention and open scope.

Claims (4)

1. remove a method for sulphur resources in rapeseed dregs fast, be made up of following steps:
(1) add in rapeseed dregs with the water of described dish dregs of rice weighing scale 25 ~ 30%, place 8 ~ 15 hours until the abundant aquation of rapeseed dregs;
(2) steam regulation explosion instrument, after reaching 1.0 ~ 2.0MPa steam pressure, by step 1) rapeseed dregs that obtains puts into the feed bin of steam blasting instrument, and dimension pressure 60 seconds ~ 90 seconds, carries out explosion.
2. method according to claim 1, is characterized in that, also comprises the steps:
Collect the sample that described step (2) obtains, it is dried and pulverization process, obtains virus-free rapeseed meal.
3. method according to claim 2, is characterized in that, described technology can remove the sulphur glycosides of in rapeseed dregs 74%.
4. method according to claim 2, is characterized in that, described technology can remove the sulphur glycosides of in rapeseed dregs 87.2%.
CN201410069566.XA 2014-02-28 2014-02-28 The feed processing technology of sulphur resources in a kind of quick removal rapeseed dregs Expired - Fee Related CN103815129B (en)

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CN104054949A (en) * 2014-06-09 2014-09-24 四川国凤中科生物科技有限公司 Preparation process of chicken feed containing detoxified rapeseed meal
CN104068246A (en) * 2014-06-09 2014-10-01 四川国凤中科生物科技有限公司 Chicken feed containing detoxicated rapeseed meal
CN104920796A (en) * 2015-05-28 2015-09-23 河南双成生物科技有限公司 A method for reducing aflatoxin contents in feed raw materials
CN107095002A (en) * 2017-04-21 2017-08-29 安徽家壹味食品有限公司 A kind of rape cake preprocess method for being used to prepare poultry and livestock feed

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101401614A (en) * 2008-10-30 2009-04-08 河南省龙腾高科实业有限公司 Multi-bacterial fermentation production of protein feedstuff with steam exploration of vegetables dregs and cotton dregs and method thereof
CN101642187A (en) * 2009-09-02 2010-02-10 张培举 Protein feed rich in small peptides and multi-enzyme bacteria and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101401614A (en) * 2008-10-30 2009-04-08 河南省龙腾高科实业有限公司 Multi-bacterial fermentation production of protein feedstuff with steam exploration of vegetables dregs and cotton dregs and method thereof
CN101642187A (en) * 2009-09-02 2010-02-10 张培举 Protein feed rich in small peptides and multi-enzyme bacteria and preparation method thereof

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