CN103815051A - Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil - Google Patents
Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil Download PDFInfo
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- CN103815051A CN103815051A CN201410080183.2A CN201410080183A CN103815051A CN 103815051 A CN103815051 A CN 103815051A CN 201410080183 A CN201410080183 A CN 201410080183A CN 103815051 A CN103815051 A CN 103815051A
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- oil
- peony
- peony seeds
- peony seed
- seed oil
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- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 97
- 239000003921 oil Substances 0.000 title claims abstract description 37
- 235000019198 oils Nutrition 0.000 title claims abstract description 37
- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 33
- 239000008157 edible vegetable oil Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000000203 mixture Substances 0.000 title abstract 6
- 235000007340 Hordeum vulgare Nutrition 0.000 title abstract 3
- 240000005979 Hordeum vulgare Species 0.000 title 1
- 244000170916 Paeonia officinalis Species 0.000 title 1
- 241000736199 Paeonia Species 0.000 claims abstract description 96
- 239000010779 crude oil Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000007670 refining Methods 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 241000209140 Triticum Species 0.000 claims description 24
- 235000021307 Triticum Nutrition 0.000 claims description 24
- 239000000843 powder Substances 0.000 claims description 23
- 239000012266 salt solution Substances 0.000 claims description 22
- 238000005119 centrifugation Methods 0.000 claims description 11
- 230000008014 freezing Effects 0.000 claims description 10
- 238000007710 freezing Methods 0.000 claims description 10
- 230000010355 oscillation Effects 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 2
- 239000004519 grease Substances 0.000 abstract description 6
- 241000209219 Hordeum Species 0.000 abstract 2
- 238000010298 pulverizing process Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 240000005001 Paeonia suffruticosa Species 0.000 description 1
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 229930003451 Vitamin B1 Natural products 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- AOJZSYZUFZULLN-UHFFFAOYSA-N hexylcyclopropane Chemical compound CCCCCCC1CC1 AOJZSYZUFZULLN-UHFFFAOYSA-N 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000010734 process oil Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
Abstract
The invention provides a blend edible oil of peony seed oil and barley oil and a preparation method of the blend edible oil. The blend edible oil is prepared through the following steps: taking shelled peony seeds, conducting physical squeezing to prepare peony seed crude oil after the shelled peony seeds are processed; refining the peony seed crude oil to prepare refined peony seed oil; blending the refined peony seed oil and barley oil sold in market according to the weight ratio of 1:(0.1-0.5), so that the blend edible oil is obtained. According to the invention, after the shelled peony seeds are subjected to a series of processing, the cell structure is destroyed, and the water content of the cells is reduced, so that grease in the cells can be separated from the cells in the process of squeezing conveniently, thereby improving the oil yield.
Description
Technical field
The present invention relates to edible oil field, specifically a kind of peony seed oil and large wheat oil blending edible oil and preparation method thereof.
Background technology
Peony seed oil is edible oil emerging, that have edible health double effects, take from peony seed, wherein be rich in the elements such as protein, fat, potassium, calcium, magnesium, phosphorus, selenium and vitamin B1, B2, carrotene etc., and contain odd-carbon fatty acid that active anticancer is very strong as C15, C17 etc., the aliphatic acid that contains in addition a small amount of circulus is as sad in 2-hexyl cyclopropane, is widely used in medicine, health care, food, superior cosmetics, lubricated wet goods industry.
Two kinds of modes and pluses and minuses separately that peony seed oil is produced are as follows:
1) extract technology: the residue tree peony seedcake after squeezing, leaches peony seed oil with chemical solvent.Advantage: oil yield is high, output is large, saves cost.Shortcoming: nutritional labeling reduces, belongs to chemical industry.
2) squeezing process: industrialization squeezing peony seed oil on the basis of ancient method.Advantage: the low temperature of controlling well can retain all original nutritional labelings of peony seed oil, physical squeezing.Shortcoming: oil yield is low, cost is high.
Summary of the invention
The object of the invention is to overcome the low problem of oil yield of traditional milling process, and then utilize commercially available large wheat oil that a kind of peony seed oil and large wheat oil blending edible oil and preparation method thereof are provided, the ready-mixed oil of preparing by the method is nutritious and balanced, overcome the low problem of traditional squeezing process oil yield, made the squeezing oil yield of peony seed oil exceed 10% left and right than the oil yield of traditional milling process.
The technical scheme that the present invention takes is for achieving the above object: a kind of peony seed oil and large wheat oil blending edible oil, be in harmonious proportion and form by weight the ratio of 0.1-0.5:1 by the peony seed oil of large wheat oil and refining.
Preparing above-mentioned peony seed oil with the method for large wheat oil blending edible oil is: remove shell peony seeds and carry out after treatment physical squeezing and make peony seeds crude oil, again the refining peony seed oil obtaining after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio and make product, wherein, the processing of peony seeds of shelling described in comprises the following steps:
1) peony seeds after shelling is added to the water soak after 2-5h and drains, and to put into immediately temperature be-45 ℃ of following freezing 15-20h of environment, then in sub-zero low temperature environment, be ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) the peony seeds powder of step 1) taken out and under the environment temperature of 20-25 ℃, joined in the salt solution that mass concentration is 15-18%, leaving standstill 17-24h after then passing into wherein supersonic oscillations 3-5min, for subsequent use;
3) adopt centrifugation to make step 2) in peony seeds powder separate with salt solution, then under temperature is the condition of 65-70 ℃, dry to moisture content and be less than 5%, afterwards peony seeds powder is squeezed.
Described step 2) condition of supersonic oscillations is: the ultrasonic wave of the corresponding 120-150W of salt solution of every kilogram, hyperacoustic frequency is 80-110KHz.
In described step 3), the rotating speed of centrifugation is 2500-4000r/min.
The salt solution of isolating in described step 3) after peony seeds powder is isolated peony seeds crude oil by distillation procedure.
In the present invention, first peony seeds is soaked in water is that cell in order to make peony seeds fully absorbs water, then after freezing in the freezing environment below-45 ℃ and put into salt solution under the environment temperature of 20-25 ℃, destroyed like this eucaryotic cell structure, be convenient in when squeezing fuel-displaced;
Meanwhile, peony seeds powder is placed in to the salt solution that mass concentration is 15-18%, can makes the cell dehydration of peony seeds, cell volume dwindles, and is not only convenient to follow-up oven dry, and has eliminated unnecessary moisture in cell, has improved squeezing oil yield; In this process, introduce supersonic oscillations, not only play stirring action, and can play the cyto-architectural effect that destroys; In follow-up centrifugation, also can make the grease of cell interior move to skin, be convenient to be extracted in expressing process.
In the present invention, by freezing peony seeds rear pulverizing, granularity is less, is more conducive to post-processed and improves oil yield, still, in crushing process, have part grease and be extracted, the particle of pulverizing is less, and the grease of crushing process loss is more, consider above factor, the particle diameter after pulverizing is that 1-2mm is advisable; And, be compared to directly and pulverize, in sub-zero low temperature environment, pulverize immediately after freezing in the freezing environment below-45 ℃, can effectively reduce the loss of grease in crushing process.
Beneficial effect: the present invention will shell peony seeds after a series of processing, has destroyed eucaryotic cell structure and has reduced the water content of cell, is convenient to so intracellular grease and from cell, separates in expressing process, thereby improved oil yield.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
Embodiment 1
A kind of peony seed oil and large wheat oil blending edible oil, be in harmonious proportion and form by weight the ratio of 0.1:1 by the peony seed oil of commercially available large wheat oil and refining;
Its preparation method is, removing shell peony seeds carries out after treatment physical squeezing and makes peony seeds crude oil, again the refining peony seed oil obtaining after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio and make product, wherein, described in the shell processing of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak after 2h and drains, and to put into immediately temperature be-45 ℃ of following freezing 15h of environment, then in sub-zero low temperature environment, be ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) the peony seeds powder of step 1) being taken out and join mass concentration under the environment temperature of 20-25 ℃ is in 15% salt solution, then after passing into wherein supersonic oscillations 3min, leave standstill 17h, hyperacoustic frequency is 80KHz, and the ultrasonic wave of every kilogram of corresponding 120W power of salt solution is for subsequent use;
3) adopt centrifugation to make step 2) in peony seeds powder separate with salt solution, the rotating speed of centrifugation is 2500r/min, then under temperature is the condition of 65 ℃, dries to moisture content and is less than 5%, afterwards peony seeds powder is squeezed;
4) salt solution after separation distills, and isolates the peony seeds crude oil wherein containing.
Embodiment 2
A kind of peony seed oil and large wheat oil blending edible oil, be in harmonious proportion and form by weight the ratio of 0.5:1 by the peony seed oil of commercially available large wheat oil and refining;
Its preparation method is, removing shell peony seeds carries out after treatment physical squeezing and makes peony seeds crude oil, again the refining peony seed oil obtaining after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio and make product, wherein, described in the shell processing of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak after 5h and drains, and to put into immediately temperature be-45 ℃ of following freezing 20h of environment, then in sub-zero low temperature environment, be ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) the peony seeds powder of step 1) being taken out and join mass concentration under the environment temperature of 20-25 ℃ is in 18% salt solution, then after passing into wherein supersonic oscillations 5min, leave standstill 24h, hyperacoustic frequency is 110KHz, and the ultrasonic wave of every kilogram of corresponding 150W power of salt solution is for subsequent use;
3) adopt centrifugation to make step 2) in peony seeds powder separate with salt solution, the rotating speed of centrifugation is 4000r/min, then under temperature is the condition of 70 ℃, dries to moisture content and is less than 5%, afterwards peony seeds powder is squeezed;
4) salt solution after separation distills, and isolates the peony seeds crude oil wherein containing.
Embodiment 3
A kind of peony seed oil and large wheat oil blending edible oil, be in harmonious proportion and form by weight the ratio of 0.3:1 by the peony seed oil of commercially available large wheat oil and refining;
Its preparation method is, removing shell peony seeds carries out after treatment physical squeezing and makes peony seeds crude oil, again the refining peony seed oil obtaining after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio and make product, wherein, described in the shell processing of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak after 3.5h and drains, and to put into immediately temperature be-45 ℃ of following freezing 18h of environment, then in sub-zero low temperature environment, be ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) the peony seeds powder of step 1) being taken out and join mass concentration under the environment temperature of 20-25 ℃ is in 17% salt solution, then after passing into wherein supersonic oscillations 4min, leave standstill 20h, hyperacoustic frequency is 95KHz, and the ultrasonic wave of every kilogram of corresponding 135W power of salt solution is for subsequent use;
3) adopt centrifugation to make step 2) in peony seeds powder separate with salt solution, the rotating speed of centrifugation is 3300r/min, then under temperature is the condition of 68 ℃, dries to moisture content and is less than 5%, afterwards peony seeds powder is squeezed;
4) salt solution after separation distills, and isolates the peony seeds crude oil wherein containing.
Claims (5)
1. peony seed oil and a large wheat oil blending edible oil, is characterized in that: the peony seed oil by commercially available large wheat oil and refining is in harmonious proportion and forms by weight the ratio of 0.1-0.5:1.
2. the method for preparation peony seed oil as claimed in claim 1 and large wheat oil blending edible oil, removing shell peony seeds carries out after treatment physical squeezing and makes peony seeds crude oil, again the refining peony seed oil obtaining after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion and make product in ratio claimed in claim 1, it is characterized in that: described in the shell processing of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak after 2-5h and drains, and to put into immediately temperature be-45 ℃ of following freezing 15-20h of environment, then in sub-zero low temperature environment, be ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) the peony seeds powder of step 1) taken out and under the environment temperature of 20-25 ℃, joined in the salt solution that mass concentration is 15-18%, leaving standstill 17-24h after then passing into wherein supersonic oscillations 3-5min, for subsequent use;
3) adopt centrifugation to make step 2) in peony seeds powder separate with salt solution, then under temperature is the condition of 65-70 ℃, dry to moisture content and be less than 5%, afterwards peony seeds powder is squeezed.
3. the method for preparing peony seed oil and large wheat oil blending edible oil according to claim 2, is characterized in that: described step 2) condition of supersonic oscillations is: the ultrasonic wave of the corresponding 120-150W of salt solution of every kilogram, hyperacoustic frequency is 80-110KHz.
4. the method for preparing peony seed oil and large wheat oil blending edible oil according to claim 2, is characterized in that: in described step 3), the rotating speed of centrifugation is 2500-4000r/min.
5. the method for preparing peony seed oil and large wheat oil blending edible oil according to claim 2, is characterized in that: the salt solution of isolating in described step 3) after peony seeds powder is isolated peony seeds crude oil by distillation procedure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410080183.2A CN103815051B (en) | 2014-03-06 | 2014-03-06 | Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410080183.2A CN103815051B (en) | 2014-03-06 | 2014-03-06 | Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil |
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| Publication Number | Publication Date |
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| CN103815051A true CN103815051A (en) | 2014-05-28 |
| CN103815051B CN103815051B (en) | 2015-06-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410080183.2A Expired - Fee Related CN103815051B (en) | 2014-03-06 | 2014-03-06 | Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1960639A (en) * | 2004-06-14 | 2007-05-09 | 卡拉皮利·佛罗伦萨公开股份有限公司 | Cereal and fruit oil |
| CN101653174A (en) * | 2009-09-07 | 2010-02-24 | 兰州牡丹园艺开发公司 | Method for preparing blend oil and cold-pressing and extracting peony seed oil |
| CN103493908A (en) * | 2013-10-11 | 2014-01-08 | 河南科技大学 | Nut blend oil with lipid lowering and blood glucose reducing effects and preparation method thereof |
-
2014
- 2014-03-06 CN CN201410080183.2A patent/CN103815051B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1960639A (en) * | 2004-06-14 | 2007-05-09 | 卡拉皮利·佛罗伦萨公开股份有限公司 | Cereal and fruit oil |
| CN101653174A (en) * | 2009-09-07 | 2010-02-24 | 兰州牡丹园艺开发公司 | Method for preparing blend oil and cold-pressing and extracting peony seed oil |
| CN103493908A (en) * | 2013-10-11 | 2014-01-08 | 河南科技大学 | Nut blend oil with lipid lowering and blood glucose reducing effects and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103815051B (en) | 2015-06-17 |
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Effective date of registration: 20180306 Address after: No. 4, unit 2, No. 7, courtyard No. 2, Yucai street, old city city, Henan Province, 702 Patentee after: Yang Panpan Address before: 471003 Henan province Luoyang Xigong Mill Road Wangcheng Avenue on the west side of Mill Road 89, two floor No. 01-02001 Patentee before: LUOYANG CHUNKUI AGRICULTURAL DEVELOPMENT Co.,Ltd. |
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