CN1038096C - Preparation method of quick-acting panacea for adjusting the growth of plant - Google Patents
Preparation method of quick-acting panacea for adjusting the growth of plant Download PDFInfo
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- CN1038096C CN1038096C CN90107639A CN90107639A CN1038096C CN 1038096 C CN1038096 C CN 1038096C CN 90107639 A CN90107639 A CN 90107639A CN 90107639 A CN90107639 A CN 90107639A CN 1038096 C CN1038096 C CN 1038096C
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Abstract
The present invention relates to a preparation method for a quick acting medicine for adjusting the growth of plants. The preparation method comprises: salicylic acid or the salicylic acid and plant cytokinin, etc. are dissolved into a basic solution by ammonia water; citric acid or the citric acid and substances containing trace elements are dissolved into an acidic solution by water; the acidic solution and the basic solution are neutralized to be in a proper pH value. The preparation method has the advantages of simple process, little investment and low cost. The quick acting medicine prepared by the method can adjust the plants in various periods of the growth and the development of the plants, such as spraying leaves, soaking seeds, mixing seeds, pouring seeds, etc. The quick acting medicine has the advantage of rapid and obvious effect, and can be widely used for flowers, vegetables, wheat, maize, cotton, tobaccos and fruit trees.
Description
The present invention relates to the preparation method of a plant growth regulators, particularly a kind of is the preparation method of the plant growth regulating quick-acting panacea of primary raw material with salicylic acid, citric acid and phytocytomine, methyl.
In the existing plant growth regulator, the viscosity that has is little, sprays to meet rainwater behind the blade face and easily wash away and cause regulating effect poor, can not work to the differentiation of fringes such as wheat, paddy rice and corn; Have only with micro-coordinate plant growth, governing speed is slow; The using method that has is restricted, only is suitable for spraying the blade face; What have can only play regulating action in certain stage of plant growing.These have all influenced plant growth regulator in wider applying.
The object of the present invention is to provide a kind of to the plant growth regulation effect fast, significantly, the using method variation can both be played the preparation method of the multifunctional plant growth regulator of regulating action in each stage of plant growing.
Purpose of the present invention can reach by following measure.
A kind of preparation method of plant growth regulating quick-acting panacea, dissolving addition with proper ammonia in closed container is that 0.01-50% is (in weight %, as follows) salicylic acid alkalize solution, with suitable quantity of water dissolving addition is that the citric acid of 0.01-50% becomes acid solution, again described acidity and alkaline solution being neutralized and transfer to the solution pH value is 4-9, promptly make product plant growth regulating quick-acting panacea (abbreviation is planted and transferred spirit, and is as follows), carry out can at last, seal, pack.
The preparation method who also has a kind of plant growth regulating quick-acting panacea, employing is dissolved addition with proper ammonia in closed container be that 0.01-50% is (in weight %, as follows) salicylic acid and the addition methyl that is 3-22% and/or the addition phytocytomine alkalize solution that is 0.001-0.09%, is the citric acid of 0.01-50% and contains micro-material in right amount and become acid solution that more described alkalescence and acid solution being neutralized and transfer to the solution pH value is 4-9 with suitable quantity of water dissolving addition.
The addition of the above salicylic acid etc., all their addition accounts for the weight % of the total addition of various raw materials during assignment system plant growth regulating quick-acting panacea.
The used primary raw material salicylic acid of the present invention (molecular formula C
7H
6O
3, the formal name used at school septichen) and be a kind of special auxin.It can impel the plant cell activation among the present invention, thereby promote that plant grows fast, sprouting in advance, it is green and precocious to tell, improve plant survival rate, percentage of fertile fruit and seed and protect full degree, promote root system development, prevent plant pest, so it is called as the growth stimulator of plant, natural protective agent and chemical weapons.
Citric acid (molecular formula C
6H
8O
7H
2O, formal name used at school 2-hydroxy propane-1,2,3-tricarboxylic acids) also be one of primary raw material of the present invention.It mainly works the closure of the pore that impels plant leaf surface and cane, impel salicylic acid, phytocytomine, trace element and quick-acting chemical fertilizer etc. to enter plant corpus fast from the pore of plant leaf surface and footpath bar, intensify the plant cell activity, promote that plant grows fast, thereby reach the purpose of precocious volume increase.It also can regulate the physiological function of plant each side, and plays the pH value that coordinate plant growth is regulated quick-acting panacea.
Ammoniacal liquor is mainly used to dissolve salicylic acid, methyl, phytocytomine, borax etc. in the present invention, plays the pH value that coordinate plant growth is regulated quick-acting panacea simultaneously, increases the nutrition of plant instant nitrogenousfertilizer, promotes the luxuriant effect in blade face.Because ammonia is volatile, so ammonia solvent salicylic acid etc. should carry out in closed container, make ammoniacal liquor not volatile, prevent the pollution of air and be harmful to the healthy of human body, and keep the fertilizer efficiency of instant nitrogenousfertilizer.
The dissolving of citric acid water makes citric acid become acidic liquid, also makes the material that contains trace element that adds in the citric acid solution can fully be dissolved into the state that plant easily absorbs, and is beneficial to the plant fast Absorption.The concentration that water can also coordinate plant growth be regulated quick-acting panacea.
The plant growth regulating quick-acting panacea is adjusted to PH4-PH9, is suitable for the plant absorbing utilization most, PH (4 or PH) 9 is because of too acid or alkalescence are brought harmful effect to growth and development of plants too greatly.
Purpose of the present invention can also reach by following measure.
Salicylic acid or salicylic acid and methyl and/or phytocytomine ammonification are water-soluble when separating alkalize solution, pH value preferably is controlled at more than 10, so that salicylic acid, methyl and/or phytocytomine dissolve fully, the pH value of the acid solution after citric acid or citric acid dissolve with the material water that contains trace element preferably is controlled at below 5, can dissolve fully so that contain the material of trace element.Temperature when acid and alkaline solution carries out neutralization reaction is 40-90 ℃.
Phytocytomine is the substituted compounds of the amino hydrogen of adenine.The used phytocytomine of the present invention can be selected 6-furfuryladenine and/or 6-N-Benzamido purine for use.The basic element of cell division is a kind of plant hormone, 6-furfuryladenine and 6-N-Benzamido purine have promote plant cell division, promote plant germination, take root, bloom, effects such as parthenocarpy and releasing apical dominance, by keeping the synthetic of protein and nucleic acid, postpone leaf senile and metabolite is gathered.So, among the present invention to plant establishment strong sprout, promote ear differentiation, the later stage is accelerated substance operation, prevents aging, improves grain and heavily plays an important role.
The plant growth substance methyl can impel plant establishment in the present invention, bloom, improves germination rate, makes crops precocity, fecund, prevents fruit drop.
In the preparation plant growth regulating quick-acting panacea institute to add and contain micro-material be the material of elements such as iron content, copper, zinc, boron, manganese, molybdenum, iodine, as select borax, ferrous sulfate, copper sulphate, zinc sulphate etc. for use, wherein the borax ammonia solvent.Trace elements such as these iron, copper, zinc, boron though the plant aequum is few, are that the plant life is necessary, have special physiological properties, and it can improve crop yield.These trace elements dissolve fully through peracid, alkaline treatment, can be changed into the inorganic elements that is easily directly absorbed by plant.
The present invention preferably adds citric acid in the entry dissolving back and adds ferrous sulfate, copper sulphate, the abundant mixed dissolution 10-100 of zinc sulphate minute (ferrous sulfate, copper sulphate, zinc sulphate etc. that make its citric acid and contain trace element can fully be dissolved, be beneficial to the absorption of plant), when the alkaline solution in the closed container drops to essentially no ammonia below the PH9, slowly add with in the alkaline solution behind ammonia solvent salicylic acid and methyl and/or the phytocytomine, transferring to the solution pH value at last is 4-9 again.
The present invention also can be in acid and alkaline solution carry out and the time, adding modulation solution pH values such as quick-acting chemical fertilizer potassium dihydrogen phosphates, urea, carbonic hydroammonium, ammonium chloride, ammonium nitrate, ammonium sulfate, calcium monohydrogen phosphate, superphosphate, ammonium dihydrogen phosphate (ADP), fused calcium magnesium phosphate is 5.8-7.5.These chemical fertilizer can not only increase plant nutrition, help plant and directly absorb, and promote plant growing, can also play coordinate plant growth and regulate the quick-acting panacea pH value.
The working concentration of plant growth regulating quick-acting panacea is 1/800-1/4000 (with the water dilution).
Preparation technology of the present invention is simple, small investment, and instant effect, but product long preservation are convenient to transportation.The plant growth regulating quick-acting panacea that preparation method of the present invention produced is soluble in water, but the suitable viscosity of tool, the energy good adhesive force is difficult for being fallen by rain drop erosion at plant leaf surface when spraying the blade face, thereby helps plant absorbing, and is effective to plant growth regulating; Can intensify the plant cell activity, promote plant grow fast (see Table one and table two).
Find out from table one, soak with 1/1000 concentration with No. 5 and No. 6 plant growth regulating quick-acting panaceas respectively and give wheat 13 wheat seeds and pull out after 4 hours, be seeded in the beaker that fills sand, cultivate with the water logging kind and compare illumination cultivation under the 21-26 of culturing room ℃ condition, broadcast back investigation in the 15 day, through plant growth regulating quick-acting panacea seed soaking processor, the wheat leaf look dark green, and blade is luxuriant, seedling is sturdy, and it is many especially to give birth to secondary rootlet on the lateral root.After measured, after handling with No. 5 and No. 6 plant growth regulating quick-acting panaceas, second lobus cardiacus comparison of wheat all increases a new root respectively according to increasing by 33.6% and 41.7% respectively, and comparison is according to increasing by 16.13%, and the seedling dry matter also obviously increases.
Table two is that the plant growth regulating quick-acting panacea is tested biennial bundle Na grape growth of cuttage seedlings development impact, select the plant growth regulating quick-acting panacea for use No. 2, concentration with 1/2000 is carried out spray test to biennial bundle Na grape cuttage seeding, measure the number of sheets, height and the blade face beam overall of emerging after handling the same day and 8 days, the result is carried out ANOVA showed significant, sprinkling plant growth regulating quick-acting panacea is not remarkable to the increase influence of blade quantity, and very rapid and remarkable to the increase of height and cuttage seeding leaf area.Because the expansion of leaf area, photosynthesis strengthens, and is beneficial to the formation and the accumulation of nutrient, helps growing of plant.
The plant growth regulating quick-acting panacea also has a significant impact (seeing Table three) to improving the plant percentage of fertile fruit.Citrus is sprayed and the filling root with 1/1000 concentration May 2 with No. 1, No. 5, No. 6 plant growth regulating quick-acting panaceas respectively in the table three, green to young fruit commentaries on classics on May 27 the same year, for the first time the physiological fallen fruit peak checks that its seedling really measures later, each is handled to find all sprinkling plant growth regulating quick-acting panaceas, all comparison has improved percentage of fertile fruit significantly according to remarkable or the utmost point, especially with No. 6 plant growth regulating quick-acting panacea processor best results, compare according to improving percentage of fertile fruit 194.82%.
The plant growth regulating quick-acting panacea also can improve the thousand kernel weight (seeing Table four) of crops greatly.No. 6 plant growth regulating quick-acting panaceas that adopt 1/1000 concentration in the table four are in wheat heading stage and carry out foliage spray flowering stage and handle.
From many evidences of carrying out, the plant growth regulating quick-acting panacea of the inventive method preparation, not only can promote plant germination, take root, branches and leaves and the footpath bar growth, and to bloom, different phase in the setting, process of growth such as solid all can play regulating action, doing seed soaking, seed dressing, foliage-spray, filling root on the using method all can, even also can make cutting flower fresh-keeping liquid (powder) etc. through adjusting prescription, to the person poultry harmless, go back the preventable disease insect pest.The plant growth regulating quick-acting panacea can be widely used in plants such as flowers, vegetables, wheat, corn, cotton, tobacco leaf, fruit tree.
Describe the present invention in detail below in conjunction with embodiment.
Embodiment one.At first citric acid is measured according to a certain ratio and added in the agitator, add entry again and carried out stirring and dissolving 10 minutes, form a kind ofly, pH value is at the acid solution below 7.Other measures salicylic acid according to a certain ratio and adds in the closed container, ammonification is water-soluble separates, form the above alkaline solution of a kind of PH7, be 6.5 under 50 ℃ of temperature condition, carrying out neutralization reaction to solution pH value in this alkaline solution adding acid solution at last, at last this plant growth regulating quick-acting panacea solution carried out can, seals, packs.Its proportioning (in weight %) is:
Citric acid 0.5
Salicylic acid 45
Ammoniacal liquor 20
Water 34.5
Embodiment two.
It is more than 10 that the salicylic alkaline solution of ammonia solvent is controlled to pH value by adjusting ammoniacal liquor addition, acid solution is below 5 by the addition control pH value of regulating citric acid, temperature when alkalescence and acid solution neutralization reaction is 40 ℃, plant growth regulating quick-acting panacea solution pH value is 4.5, and its proportioning (weight %) is:
Citric acid 20
Salicylic acid 35
Ammoniacal liquor 18
Water 27
Embodiment three.
Salicylic acid and methyl are measured in the adding closed container according to a certain ratio, adding ammonia solvent to solution pH value is 10, other measures citric acid and the compound ferrous sulfate, copper sulphate and the zinc sulphate that contain trace elements iron, copper, zinc according to a certain ratio and adds in the agitator, added the water stirring and dissolving again 100 minutes, the pH value of gained acid solution is controlled at 2, is 6.5 being neutralized to the solution pH value in this acid solution adding alkaline solution under 70 ℃ of conditions at last.Its proportioning (weight %) is:
Salicylic acid 0.5
Methyl 20
Citric acid 50
Ferrous sulfate 0.5
Copper sulphate 0.1
Zinc sulphate 0.4
Ammoniacal liquor 7.2
Water 21.3
Embodiment four.
Add salicylic acid, methyl in the closed container according to a certain ratio, adding ammonia solvent to solution pH value again is 13, other adds citric acid and the ferrous sulfate that contains trace elements iron, copper, zinc, copper sulphate and zinc sulphate in the agitator, added the water stirring and dissolving 50 minutes, the formation pH value is 3 acid solution, at last this acid solution is added in alkaline solution and under 80 ℃ of temperature, carries out neutralization reaction, to the solution pH value be 8.Its proportioning (weight %) is:
Salicylic acid 14
Methyl 5.5
Citric acid 20
Ferrous sulfate 0.5
Copper sulphate 0.1
Zinc sulphate 0.2
Ammoniacal liquor 30
Soft water 30
Embodiment five.
In the embodiment four made plant growth regulating quick-acting panacea solution of getting ready, add quick-acting fertilizer such as potassium dihydrogen phosphate, urea, the pH value that is adjusted to the plant growth regulating quick-acting panacea at last is 6.5.
Embodiment six.
Salicylic acid, methyl, borax, basic element of cell division 6-N-Benzamido purine are measured in the adding closed container according to a certain ratio, added ammonia solvent, make the alkaline solution that forms PH14; Go in the agitator adding ferrous sulfate, copper sulphate and zinc sulphate again after the dissolving of citric acid water again, be dissolved in water 30 minutes, the formation pH value is 1 acid solution, again this acid solution is added slowly that to be neutralized to the solution pH value in the alkaline solution under 90 ℃ of temperature be 7.5, add potassium dihydrogen phosphate and urea again, transferring to the solution pH value is 6.5.Its proportioning (weight %) is:
Salicylic acid 17
Methyl 8
Ammoniacal liquor 20
6-N-Benzamido purine 0.02
Citric acid 25
Ferrous sulfate 0.5
Copper sulphate 0.4
Zinc sulphate 0.17
Borax 2
Soft water 25
Potassium dihydrogen phosphate 1
Urea 0.91
The plant growth regulating quick-acting panacea that above embodiment one to six preparation method is produced is respectively the plant growth regulating quick-acting panacea No. 1 to No. 6.
Table one plant growth regulating quick-acting panacea is used for wheat seed soaking result of the test
Remarks: this test data is provided by academy of agricultural sciences, Henan Province wheat institute Hua Pei chamber.Table two plant growth regulating quick-acting panacea is to pricking the test of Na grape growth of cuttage seedlings development impact
Table three plant growth regulating quick-acting panacea different disposal is to the influence test of citrus percentage of fertile fruit
Table two, table three test data provide by Agricultural University Of He'nan's undergraduate's thesis.Table four foliage spray plant growth is regulated the influence test of quick-acting panacea to thousand grain weight of wheat
Annotate: this test data is provided by academy of agricultural sciences, Henan Province wheat institute Hua Pei chamber and Fugou County, Henan Province seeds company.
Claims (2)
1. the preparation method of a plant growth regulating quick-acting panacea, it is characterized in that in closed container with proper ammonia dissolving addition being 0.01～50% salicylic acid alkalize solution, with suitable quantity of water dissolving addition is that 0.01～50% citric acid becomes acid solution, the pH value that more described acidity and alkaline solution is neutralized and transfer to solution is 4～9, more than the addition of each material component all in weight %.
2. preparation method according to claim 1, it is characterized in that being controlled at more than 10 with the salicylic alkaline solution pH value of ammonia solvent, the pH value of the acid solution of water dissolving citric acid is controlled at below 5, and the temperature when acidity and alkaline solution neutralization reaction is 40～90 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN90107639A CN1038096C (en) | 1990-09-11 | 1990-09-11 | Preparation method of quick-acting panacea for adjusting the growth of plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN90107639A CN1038096C (en) | 1990-09-11 | 1990-09-11 | Preparation method of quick-acting panacea for adjusting the growth of plant |
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| Publication Number | Publication Date |
|---|---|
| CN1059634A CN1059634A (en) | 1992-03-25 |
| CN1038096C true CN1038096C (en) | 1998-04-22 |
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|---|---|---|---|
| CN90107639A Expired - Fee Related CN1038096C (en) | 1990-09-11 | 1990-09-11 | Preparation method of quick-acting panacea for adjusting the growth of plant |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1048617C (en) * | 1993-06-30 | 2000-01-26 | 湖北农学院 | Compound synergist for killing fungus and pest |
| CN1057429C (en) * | 1994-03-14 | 2000-10-18 | 北京农业大学 | Plant growing regulating agent for promoting fruit tree sproceting buds and its production technology |
| RU2006145957A (en) * | 2004-05-24 | 2008-06-27 | Вэйлент Байосайенсиз Копэрейшн (US) | COMPOSITION FOR REGULATION OF PLANT GROWTH (OPTIONS), METHOD FOR PRODUCING SOLUBLE LIQUID DRUG, MEDICINE AND METHOD FOR REGULATING PLANT GROWTH |
| CN103210773B (en) * | 2013-05-03 | 2014-06-25 | 李敏 | Method of promoting flowering and fructification of arbor willow in advance |
| CN104488402B (en) * | 2014-12-17 | 2016-12-07 | 长江大学 | The method improving the anti-water logging stress of Semen Tritici aestivi |
| CN109924530A (en) * | 2019-02-15 | 2019-06-25 | 湖北省烟草科学研究院 | Upgrading harm reduction regulator and its application method for tobacco leaf modulation |
| CN113951256B (en) * | 2021-10-27 | 2023-04-04 | 河北农业大学 | Pear flowering phase compound regulator and application thereof |
-
1990
- 1990-09-11 CN CN90107639A patent/CN1038096C/en not_active Expired - Fee Related
Non-Patent Citations (5)
| Title |
|---|
| DERWENT ABSTRAFE 78-22408A 1978.3.1 Rice growth sfimulation using organic acid-specificallg citric acid * |
| DERWENT ABSTRAFE 78-22408A 1978.3.1 Rice growth sfimulation using organic acid-specificallg citric acid;DERWENT ABSTRAFE 81-497490 1981.7.1;DERWENT ABSTRAFE 84-207643 1984.7.1 Plant growth regulafor compsns-comtg,reguafor mixt and sgnergist comprisi;DERWENT ABSTRAFE 88-361266 1988.10.1 * |
| DERWENT ABSTRAFE 81-497490 1981.7.1 * |
| DERWENT ABSTRAFE 84-207643 1984.7.1 Plant growth regulafor compsns-comtg,reguafor mixt and sgnergist comprisi * |
| DERWENT ABSTRAFE 88-361266 1988.10.1 * |
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| CN1059634A (en) | 1992-03-25 |
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