CN103804947A - Formula and production method for preparing plum wheat straw dye - Google Patents

Formula and production method for preparing plum wheat straw dye Download PDF

Info

Publication number
CN103804947A
CN103804947A CN201410062752.0A CN201410062752A CN103804947A CN 103804947 A CN103804947 A CN 103804947A CN 201410062752 A CN201410062752 A CN 201410062752A CN 103804947 A CN103804947 A CN 103804947A
Authority
CN
China
Prior art keywords
wheat straw
plum
raw material
solution
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410062752.0A
Other languages
Chinese (zh)
Inventor
马文侠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Harbin Arts and Crafts Co Ltd
Original Assignee
Harbin Arts and Crafts Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Harbin Arts and Crafts Co Ltd filed Critical Harbin Arts and Crafts Co Ltd
Priority to CN201410062752.0A priority Critical patent/CN103804947A/en
Publication of CN103804947A publication Critical patent/CN103804947A/en
Pending legal-status Critical Current

Links

Landscapes

  • Paper (AREA)
  • Coloring (AREA)

Abstract

The invention relates to a formula and production method for preparing a plum wheat straw dye. The plum wheat straw dye is mainly prepared from dried Flos Hibisci Mutabilis, true indigo, tea tree flower, white alum, stibium ionic compound solution and mineral water. The production method mainly comprises the following steps: material selection, cutting, drying, immersion, hot boiling, mixing, precipitation and dyeing to obtain the finished product. The plum wheat straw dye prepared from purely natural plants is purely natural, green and environment-friendly, and has the advantages of no pollution and no toxic or side effect on the human body.

Description

A kind of formula and production method of preparing plum Wheat Straw dyestuff
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and production method of preparing plum Wheat Straw dyestuff.
background technology:
in prior art, the main raw material Wheat Straw of making straw patchwork is dyed to plum method to be had a variety of, but most dyestuffs are chemical dye, what dye is plum impure, easily fade, not only not environmental protection, part dyestuff even can produce toxic gas in the process of the system of dying, and threatens the health of human body.
thereby, lack a kind of vegetable dye of Wheat Straw being dyed to different colours in straw patchwork making field, particularly Wheat Straw is dyed to plum natural plant dyestuff, not only color is pure for the plum Wheat Straw that it dyes, and the straw patchwork made from its material is bright and new beautiful, is difficult for fading, and environmental protection, works give out plant delicate fragrance for a long time, have easy people's physical and mental health, the solution that degree is different other poisonous and harmful chemical dye dying the harm in process processed, people's health being caused.
summary of the invention:
a kind of formula and the production method of preparing plum Wheat Straw dyestuff being mixed with natural plant that the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, the person is had no side effect.
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, and Flos Hibisci Mutabilis is done 10-30 part, wooden blue 10-30 part, Tea Flower 10-30 part, alum 5-15 part, antimony ion compound solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope of the plum Wheat Straw dyestuff of preparation the present invention is, wherein the weight proportion of various raw materials is, Flos Hibisci Mutabilis is done 10-25 part, wooden blue 10-25 part, Tea Flower 10-25 part, alum 5-10 part, antimony ion compound solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range of the plum Wheat Straw dyestuff of preparation the present invention is that wherein the weight proportion of various raw materials is: dry 15 parts of Flos Hibisci Mutabilis, blue 15 parts of wood, 15 parts of Tea Flowers, 8 parts of alums, 7 parts of antimony ion compound solutions, 60 parts of mineral waters.
above-mentioned each component is made to the production method of the plum Wheat Straw dyestuff of the present invention, technical process is: select materials, blank, oven dry, immersion, heat boil, mix, precipitation, dyeing, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select meet that the Flos Hibisci Mutabilis of national health and quality standard is dry, wood indigo plant, Tea Flower, alum, antimony ion compound solution, mineral water is for subsequent use; B, blank, the raw material of selecting is cut into respectively to bulk except alum, antimony ion compound solution, mineral water; C, oven dry, will be cut into block raw material and be placed in respectively stoving oven mummification, temperature is controlled at 100-120 ℃, 30 minutes time, makes to evaporate raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in to the storage tank that mineral water is housed soaks, temperature is 20 ℃ of chambers, time 2-4 hour; E, heat are boiled, the raw material steeping are pulled out from water, are put into pottery interior heat and boil, and 6 hours time, cook pigment solution; F, mixing, pigment solution is invaded in 20% antimony ion compound solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool mixing solutions to 20 ℃, be settled out pure plum cellulose solution; H, dyeing, the temperature of 100 liters of pure plum cellulose solutions is raised to more than 80 ℃ gradually, to soak wherein through sterilization, desulfurization, boiling Wheat Straw after treatment, constant temperature leaves standstill 12-14 hour, during this time Wheat Straw is stirred up and down, make Wheat Straw fully absorb plum cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution that adds alum powder, soak 3-6 hour, make to pull out after the abundant fixation of Wheat Straw, drench dryly, be slowly dried at room temperature plum Wheat Straw finished product.
production method advantage of the present invention is: 1, select raw material, and scientific formulation, color is pure; 2, in product, do not add sanitas, industrial chemicals, pure natural, to human body, without any injury, the straw patchwork works made from its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add technique circuit short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range of the plum Wheat Straw dyestuff of preparation the present invention is: Flos Hibisci Mutabilis is done 10-30 part, wooden blue 10-30 part, Tea Flower 10-30 part, alum 5-15 part, antimony ion compound solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope of the plum Wheat Straw dyestuff of preparation the present invention is: Flos Hibisci Mutabilis is done 10-25 part, wooden blue 10-25 part, Tea Flower 10-25 part, alum 5-10 part, antimony ion compound solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range of the plum Wheat Straw dyestuff of preparation the present invention is: dry 15 parts of Flos Hibisci Mutabilis, blue 15 parts of wood, 15 parts of Tea Flowers, 8 parts of alums, 7 parts of antimony ion compound solutions, 60 parts of mineral waters.
above-mentioned each component is made to the production method of the plum Wheat Straw dyestuff of the present invention, technical process is: select materials, blank, oven dry, immersion, heat boil, mix, precipitation, dyeing, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select meet that the Flos Hibisci Mutabilis of national health and quality standard is dry, wood indigo plant, Tea Flower, alum, antimony ion compound solution, mineral water is for subsequent use; B, blank, the raw material of selecting is cut into respectively to bulk except alum, antimony ion compound solution, mineral water; C, oven dry, will be cut into block raw material and be placed in respectively stoving oven mummification, temperature is controlled at 100-120 ℃, 30 minutes time, makes to evaporate raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in to the storage tank that mineral water is housed soaks, temperature is 20 ℃ of chambers, time 2-4 hour; E, heat are boiled, the raw material steeping are pulled out from water, are put into pottery interior heat and boil, and 6 hours time, cook pigment solution; F, mixing, pigment solution is invaded in 20% antimony ion compound solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool mixing solutions to 20 ℃, be settled out pure plum cellulose solution; H, dyeing, the temperature of 100 liters of pure plum cellulose solutions is raised to more than 80 ℃ gradually, to soak wherein through sterilization, desulfurization, boiling Wheat Straw after treatment, constant temperature leaves standstill 12-14 hour, during this time Wheat Straw is stirred up and down, make Wheat Straw fully absorb plum cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution that adds alum powder, soak 3-6 hour, make to pull out after the abundant fixation of Wheat Straw, drench dryly, be slowly dried at room temperature plum Wheat Straw finished product.

Claims (4)

1. prepare the formula of plum Wheat Straw dyestuff for one kind, it is characterized in that: it is to be made up of the raw material of following weight proportioning, Flos Hibisci Mutabilis is done 10-30 part, wooden blue 10-30 part, Tea Flower 10-30 part, alum 5-15 part, antimony ion compound solution 5-15 part, mineral water 30-80 part.
2. prepare the formula of plum Wheat Straw dyestuff for one kind, it is characterized in that: wherein the weight proportion of various raw materials is, Flos Hibisci Mutabilis is done 10-25 part, wooden blue 10-25 part, Tea Flower 10-25 part, alum 5-10 part, antimony ion compound solution 5-10 part, mineral water 30-70 part.
3. a formula of preparing plum Wheat Straw dyestuff, is characterized in that: wherein the weight proportion of various raw materials is, dry 15 parts of Flos Hibisci Mutabilis, blue 15 parts of wood, 15 parts of Tea Flowers, 8 parts of alums, 7 parts of antimony ion compound solutions, 60 parts of mineral waters.
4. according to a kind of production method of preparing plum Wheat Straw dye formulation described in claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat boil, mix, precipitation, dyeing, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select meet that the Flos Hibisci Mutabilis of national health and quality standard is dry, wood indigo plant, Tea Flower, alum, antimony ion compound solution, mineral water is for subsequent use; B, blank, the raw material of selecting is cut into respectively to bulk except alum, antimony ion compound solution, mineral water; C, oven dry, will be cut into block raw material and be placed in respectively stoving oven mummification, temperature is controlled at 100-120 ℃, 30 minutes time, makes to evaporate raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in to the storage tank that mineral water is housed soaks, temperature is 20 ℃ of chambers, time 2-4 hour; E, heat are boiled, the raw material steeping are pulled out from water, are put into pottery interior heat and boil, and 6 hours time, cook pigment solution; F, mixing, pigment solution is invaded in 20% antimony ion compound solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool mixing solutions to 20 ℃, be settled out pure plum cellulose solution; H, dyeing, the temperature of 100 liters of pure plum cellulose solutions is raised to more than 80 ℃ gradually, to soak wherein through sterilization, desulfurization, boiling Wheat Straw after treatment, constant temperature leaves standstill 12-14 hour, during this time Wheat Straw is stirred up and down, make Wheat Straw fully absorb plum cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution that adds alum powder, soak 3-6 hour, make to pull out after the abundant fixation of Wheat Straw, drench dryly, be slowly dried at room temperature plum Wheat Straw finished product.
CN201410062752.0A 2014-02-22 2014-02-22 Formula and production method for preparing plum wheat straw dye Pending CN103804947A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410062752.0A CN103804947A (en) 2014-02-22 2014-02-22 Formula and production method for preparing plum wheat straw dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410062752.0A CN103804947A (en) 2014-02-22 2014-02-22 Formula and production method for preparing plum wheat straw dye

Publications (1)

Publication Number Publication Date
CN103804947A true CN103804947A (en) 2014-05-21

Family

ID=50702361

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410062752.0A Pending CN103804947A (en) 2014-02-22 2014-02-22 Formula and production method for preparing plum wheat straw dye

Country Status (1)

Country Link
CN (1) CN103804947A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106634023A (en) * 2015-08-11 2017-05-10 哈尔滨市工艺美术有限责任公司 Celadon green cornstalk dye and production method thereof
CN107033625A (en) * 2015-08-11 2017-08-11 哈尔滨市工艺美术有限责任公司 A kind of soil Red maize straw dyestuff and its production method

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103554967A (en) * 2013-11-08 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing yellow wheat straw dye
CN103554964A (en) * 2013-11-08 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing tawny wheat straw dye
CN103554972A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing deep yellow wheat straw dye
CN103554971A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula for preparing lemon-yellow wheat straw dye and production method of lemon-yellow wheat straw dye
CN103554961A (en) * 2013-11-08 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing brown wheat straw dye
CN103554974A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula for preparing coffee-colored wheat straw dye and production method of coffee-colored wheat straw dye
CN103554970A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing dark olive green wheat straw dye
CN103571224A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing purple wheat straw dye
CN103571223A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing bright yellow wheat straw dye
CN103571225A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing peach wheat straw dye
CN103571227A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing silver red wheat straw dye
CN103589186A (en) * 2013-11-10 2014-02-19 哈尔滨市工艺美术有限责任公司 Formula for preparing violet wheat straw dye and production method thereof

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103554967A (en) * 2013-11-08 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing yellow wheat straw dye
CN103554964A (en) * 2013-11-08 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing tawny wheat straw dye
CN103554961A (en) * 2013-11-08 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing brown wheat straw dye
CN103554972A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing deep yellow wheat straw dye
CN103554971A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula for preparing lemon-yellow wheat straw dye and production method of lemon-yellow wheat straw dye
CN103554974A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula for preparing coffee-colored wheat straw dye and production method of coffee-colored wheat straw dye
CN103554970A (en) * 2013-11-10 2014-02-05 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing dark olive green wheat straw dye
CN103571224A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing purple wheat straw dye
CN103571223A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing bright yellow wheat straw dye
CN103571225A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing peach wheat straw dye
CN103571227A (en) * 2013-11-10 2014-02-12 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing silver red wheat straw dye
CN103589186A (en) * 2013-11-10 2014-02-19 哈尔滨市工艺美术有限责任公司 Formula for preparing violet wheat straw dye and production method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
尹卫平 等: "《精细化工产品及工艺》", 31 August 2009, 华东理工大学出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106634023A (en) * 2015-08-11 2017-05-10 哈尔滨市工艺美术有限责任公司 Celadon green cornstalk dye and production method thereof
CN107033625A (en) * 2015-08-11 2017-08-11 哈尔滨市工艺美术有限责任公司 A kind of soil Red maize straw dyestuff and its production method

Similar Documents

Publication Publication Date Title
CN103554967A (en) Formula and production method for preparing yellow wheat straw dye
CN103571225A (en) Formula and production method for preparing peach wheat straw dye
CN103571227A (en) Formula and production method for preparing silver red wheat straw dye
CN103554972A (en) Formula and production method for preparing deep yellow wheat straw dye
CN103554974A (en) Formula for preparing coffee-colored wheat straw dye and production method of coffee-colored wheat straw dye
CN103819932A (en) Madder-red wheat straw dye and preparation method
CN103804947A (en) Formula and production method for preparing plum wheat straw dye
CN103773065A (en) Formula and production method for preparing dark gold wheat straw dye
CN103773064A (en) Formula and production method for preparing coral red wheat straw dye
CN103804948A (en) Preparation formula and production method of light yellow wheat straw dyes
CN103819930A (en) Formula for preparing plum red wheat straw dye and production method
CN103554960A (en) Formula and production method for preparing red brown wheat straw dye
CN103788693A (en) Method for preparing and producing violet wheat straw dye
CN104629471A (en) Formula for preparing dark reddish purple wheat straw dye and production method thereof
CN103834191A (en) Formula and production method for preparing thistle purple wheat straw dye
CN103788687A (en) Formula for preparing deep-red wheat straw dye and production method of deep-red wheat straw dye
CN103788688A (en) Formula for preparing pale-green wheat straw dye and production method of pale-green wheat straw dye
CN103804949A (en) Dye for preparing bronze wheat straws and production method thereof
CN103554962A (en) Formula and production method for preparing lavender wheat straw dye
CN104629453A (en) Formula for preparing dark blue wheat straw dye and production method thereof
CN104861715A (en) Preparation formula and production method for light ink-color wheat straw dye
CN103804946A (en) Formula and production method for preparing light khaki wheat straw dye
CN103571222A (en) Formula and production method for preparing bright blue wheat straw dye
CN104861700A (en) Formula used for preparing dark slate blue wheat straw dye and production method
CN104861699A (en) Formula used for preparing ultramarine blue wheat straw dye and production method

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20140521