CN103804947A - Formula and production method for preparing plum wheat straw dye - Google Patents

Formula and production method for preparing plum wheat straw dye Download PDF

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Publication number
CN103804947A
CN103804947A CN201410062752.0A CN201410062752A CN103804947A CN 103804947 A CN103804947 A CN 103804947A CN 201410062752 A CN201410062752 A CN 201410062752A CN 103804947 A CN103804947 A CN 103804947A
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China
Prior art keywords
wheat straw
plum
raw material
solution
parts
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CN201410062752.0A
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Chinese (zh)
Inventor
马文侠
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Harbin Arts and Crafts Co Ltd
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Harbin Arts and Crafts Co Ltd
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Priority to CN201410062752.0A priority Critical patent/CN103804947A/en
Publication of CN103804947A publication Critical patent/CN103804947A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a formula and production method for preparing a plum wheat straw dye. The plum wheat straw dye is mainly prepared from dried Flos Hibisci Mutabilis, true indigo, tea tree flower, white alum, stibium ionic compound solution and mineral water. The production method mainly comprises the following steps: material selection, cutting, drying, immersion, hot boiling, mixing, precipitation and dyeing to obtain the finished product. The plum wheat straw dye prepared from purely natural plants is purely natural, green and environment-friendly, and has the advantages of no pollution and no toxic or side effect on the human body.

Description

A kind of formula and production method of preparing plum Wheat Straw dyestuff
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and production method of preparing plum Wheat Straw dyestuff.
background technology:
in prior art, the main raw material Wheat Straw of making straw patchwork is dyed to plum method to be had a variety of, but most dyestuffs are chemical dye, what dye is plum impure, easily fade, not only not environmental protection, part dyestuff even can produce toxic gas in the process of the system of dying, and threatens the health of human body.
thereby, lack a kind of vegetable dye of Wheat Straw being dyed to different colours in straw patchwork making field, particularly Wheat Straw is dyed to plum natural plant dyestuff, not only color is pure for the plum Wheat Straw that it dyes, and the straw patchwork made from its material is bright and new beautiful, is difficult for fading, and environmental protection, works give out plant delicate fragrance for a long time, have easy people's physical and mental health, the solution that degree is different other poisonous and harmful chemical dye dying the harm in process processed, people's health being caused.
summary of the invention:
a kind of formula and the production method of preparing plum Wheat Straw dyestuff being mixed with natural plant that the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, the person is had no side effect.
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, and Flos Hibisci Mutabilis is done 10-30 part, wooden blue 10-30 part, Tea Flower 10-30 part, alum 5-15 part, antimony ion compound solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope of the plum Wheat Straw dyestuff of preparation the present invention is, wherein the weight proportion of various raw materials is, Flos Hibisci Mutabilis is done 10-25 part, wooden blue 10-25 part, Tea Flower 10-25 part, alum 5-10 part, antimony ion compound solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range of the plum Wheat Straw dyestuff of preparation the present invention is that wherein the weight proportion of various raw materials is: dry 15 parts of Flos Hibisci Mutabilis, blue 15 parts of wood, 15 parts of Tea Flowers, 8 parts of alums, 7 parts of antimony ion compound solutions, 60 parts of mineral waters.
above-mentioned each component is made to the production method of the plum Wheat Straw dyestuff of the present invention, technical process is: select materials, blank, oven dry, immersion, heat boil, mix, precipitation, dyeing, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select meet that the Flos Hibisci Mutabilis of national health and quality standard is dry, wood indigo plant, Tea Flower, alum, antimony ion compound solution, mineral water is for subsequent use; B, blank, the raw material of selecting is cut into respectively to bulk except alum, antimony ion compound solution, mineral water; C, oven dry, will be cut into block raw material and be placed in respectively stoving oven mummification, temperature is controlled at 100-120 ℃, 30 minutes time, makes to evaporate raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in to the storage tank that mineral water is housed soaks, temperature is 20 ℃ of chambers, time 2-4 hour; E, heat are boiled, the raw material steeping are pulled out from water, are put into pottery interior heat and boil, and 6 hours time, cook pigment solution; F, mixing, pigment solution is invaded in 20% antimony ion compound solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool mixing solutions to 20 ℃, be settled out pure plum cellulose solution; H, dyeing, the temperature of 100 liters of pure plum cellulose solutions is raised to more than 80 ℃ gradually, to soak wherein through sterilization, desulfurization, boiling Wheat Straw after treatment, constant temperature leaves standstill 12-14 hour, during this time Wheat Straw is stirred up and down, make Wheat Straw fully absorb plum cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution that adds alum powder, soak 3-6 hour, make to pull out after the abundant fixation of Wheat Straw, drench dryly, be slowly dried at room temperature plum Wheat Straw finished product.
production method advantage of the present invention is: 1, select raw material, and scientific formulation, color is pure; 2, in product, do not add sanitas, industrial chemicals, pure natural, to human body, without any injury, the straw patchwork works made from its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add technique circuit short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range of the plum Wheat Straw dyestuff of preparation the present invention is: Flos Hibisci Mutabilis is done 10-30 part, wooden blue 10-30 part, Tea Flower 10-30 part, alum 5-15 part, antimony ion compound solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope of the plum Wheat Straw dyestuff of preparation the present invention is: Flos Hibisci Mutabilis is done 10-25 part, wooden blue 10-25 part, Tea Flower 10-25 part, alum 5-10 part, antimony ion compound solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range of the plum Wheat Straw dyestuff of preparation the present invention is: dry 15 parts of Flos Hibisci Mutabilis, blue 15 parts of wood, 15 parts of Tea Flowers, 8 parts of alums, 7 parts of antimony ion compound solutions, 60 parts of mineral waters.
above-mentioned each component is made to the production method of the plum Wheat Straw dyestuff of the present invention, technical process is: select materials, blank, oven dry, immersion, heat boil, mix, precipitation, dyeing, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select meet that the Flos Hibisci Mutabilis of national health and quality standard is dry, wood indigo plant, Tea Flower, alum, antimony ion compound solution, mineral water is for subsequent use; B, blank, the raw material of selecting is cut into respectively to bulk except alum, antimony ion compound solution, mineral water; C, oven dry, will be cut into block raw material and be placed in respectively stoving oven mummification, temperature is controlled at 100-120 ℃, 30 minutes time, makes to evaporate raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in to the storage tank that mineral water is housed soaks, temperature is 20 ℃ of chambers, time 2-4 hour; E, heat are boiled, the raw material steeping are pulled out from water, are put into pottery interior heat and boil, and 6 hours time, cook pigment solution; F, mixing, pigment solution is invaded in 20% antimony ion compound solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool mixing solutions to 20 ℃, be settled out pure plum cellulose solution; H, dyeing, the temperature of 100 liters of pure plum cellulose solutions is raised to more than 80 ℃ gradually, to soak wherein through sterilization, desulfurization, boiling Wheat Straw after treatment, constant temperature leaves standstill 12-14 hour, during this time Wheat Straw is stirred up and down, make Wheat Straw fully absorb plum cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution that adds alum powder, soak 3-6 hour, make to pull out after the abundant fixation of Wheat Straw, drench dryly, be slowly dried at room temperature plum Wheat Straw finished product.

Claims (4)

1. prepare the formula of plum Wheat Straw dyestuff for one kind, it is characterized in that: it is to be made up of the raw material of following weight proportioning, Flos Hibisci Mutabilis is done 10-30 part, wooden blue 10-30 part, Tea Flower 10-30 part, alum 5-15 part, antimony ion compound solution 5-15 part, mineral water 30-80 part.
2. prepare the formula of plum Wheat Straw dyestuff for one kind, it is characterized in that: wherein the weight proportion of various raw materials is, Flos Hibisci Mutabilis is done 10-25 part, wooden blue 10-25 part, Tea Flower 10-25 part, alum 5-10 part, antimony ion compound solution 5-10 part, mineral water 30-70 part.
3. a formula of preparing plum Wheat Straw dyestuff, is characterized in that: wherein the weight proportion of various raw materials is, dry 15 parts of Flos Hibisci Mutabilis, blue 15 parts of wood, 15 parts of Tea Flowers, 8 parts of alums, 7 parts of antimony ion compound solutions, 60 parts of mineral waters.
4. according to a kind of production method of preparing plum Wheat Straw dye formulation described in claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat boil, mix, precipitation, dyeing, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select meet that the Flos Hibisci Mutabilis of national health and quality standard is dry, wood indigo plant, Tea Flower, alum, antimony ion compound solution, mineral water is for subsequent use; B, blank, the raw material of selecting is cut into respectively to bulk except alum, antimony ion compound solution, mineral water; C, oven dry, will be cut into block raw material and be placed in respectively stoving oven mummification, temperature is controlled at 100-120 ℃, 30 minutes time, makes to evaporate raw material moisture content, sterilizing; D, immersion, the raw material after drying is placed in to the storage tank that mineral water is housed soaks, temperature is 20 ℃ of chambers, time 2-4 hour; E, heat are boiled, the raw material steeping are pulled out from water, are put into pottery interior heat and boil, and 6 hours time, cook pigment solution; F, mixing, pigment solution is invaded in 20% antimony ion compound solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool mixing solutions to 20 ℃, be settled out pure plum cellulose solution; H, dyeing, the temperature of 100 liters of pure plum cellulose solutions is raised to more than 80 ℃ gradually, to soak wherein through sterilization, desulfurization, boiling Wheat Straw after treatment, constant temperature leaves standstill 12-14 hour, during this time Wheat Straw is stirred up and down, make Wheat Straw fully absorb plum cellulose solution, level dyeing; I, fixation, the Wheat Straw after dyeing is put into the solution that adds alum powder, soak 3-6 hour, make to pull out after the abundant fixation of Wheat Straw, drench dryly, be slowly dried at room temperature plum Wheat Straw finished product.
CN201410062752.0A 2014-02-22 2014-02-22 Formula and production method for preparing plum wheat straw dye Pending CN103804947A (en)

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Publication number Priority date Publication date Assignee Title
CN106634023A (en) * 2015-08-11 2017-05-10 哈尔滨市工艺美术有限责任公司 Celadon green cornstalk dye and production method thereof
CN107033625A (en) * 2015-08-11 2017-08-11 哈尔滨市工艺美术有限责任公司 A kind of soil Red maize straw dyestuff and its production method

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Publication number Priority date Publication date Assignee Title
CN106634023A (en) * 2015-08-11 2017-05-10 哈尔滨市工艺美术有限责任公司 Celadon green cornstalk dye and production method thereof
CN107033625A (en) * 2015-08-11 2017-08-11 哈尔滨市工艺美术有限责任公司 A kind of soil Red maize straw dyestuff and its production method

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Application publication date: 20140521