CN103784385B - perfume preparation and preparation method thereof - Google Patents
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- CN103784385B CN103784385B CN201410065651.9A CN201410065651A CN103784385B CN 103784385 B CN103784385 B CN 103784385B CN 201410065651 A CN201410065651 A CN 201410065651A CN 103784385 B CN103784385 B CN 103784385B
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Abstract
The present invention proposes a kind of perfume preparation and preparation method thereof, and by percent mass, this is formulated by following for described perfume preparation: by Semen Maydis be main material fermentation, deodorize prepare ethanol 65%～85%, deionized water 3%～12%, essence 3%～25%, muscone 0.1%～2%, benzoic acid Bian ester 0.1～2%, Moschus 1050.1～3%, salicylic acid Bian ester 0.1～3%, galaxolid 0.1～3%, rest in peace balsam 0.1～1% and isopropyl myristate 0.1～0.3%.Perfume alcohol taste both stabilized by perfume preparation of the present invention and preparation method thereof, improves sweet clear (green grass or young crops) fragrant and quiet and tastefully laid out grade of perfume, substantially increases again the aroma retaining effect of perfume, improve quality and the class of perfume.
Description
Technical field
The present invention relates to cosmetic technical field, particularly to a kind of perfume preparation and preparation method thereof.
Background technology
Perfume is a kind of liquid being mixed with essence, ethanol, deionized water and relevant adjuvant, and human body can be allowed after sprinkling to keep more lasting graceful fragrance.Essence extracts from plant, and the health of animal directly taken from by animal perfume material, for instance Moschus, Ambra Grisea etc., is the main fragrant source of perfume.Perfume adds ethanol, is made by the effect that the volatility of ethanol reaches to suffus an exquisite fragrance all around.
At present, China's existing perfume Technology is comparatively backward, and all this is more low-grade for primary flavor raw material, and quality can not show a candle to American-European product；Particularly solvent for use ethanol not only material quality is low, does not carry out again processing to stabilize vinosity, and the perfume alcohol taste made is obvious；During lasting short, generally also only several hours, what have was even shorter, only has 1-2 hour；Existing perfume preparation is low-grade odor type mostly, both suspenseful, does not also have imaginative power, does not possess the most typical graceful grade of perfume and fashion feature.
Summary of the invention
The purpose of the present invention is to propose to a kind of perfume preparation and preparation method thereof, it had both stabilized perfume alcohol taste, improves sweet clear (green grass or young crops) fragrant and quiet and tastefully laid out grade of perfume, substantially increases again the aroma retaining effect of perfume, improve quality and the class of perfume.
For reaching above-mentioned purpose, the present invention proposes a kind of perfume preparation, and by percent mass, this is formulated by following for it:
By Semen Maydis be main material fermentation, deodorize prepare ethanol 65%～85%, deionized water 3%～12%, essence 3%～25%, muscone 0.1%～2%, benzoic acid Bian ester 0.1～2%, Moschus 1050.1～3%, salicylic acid Bian ester 0.1～3%, galaxolid 0.1～3%, rest in peace balsam 0.1～1% and isopropyl myristate 0.1～0.3%.
Further, in above-mentioned perfume preparation, each composition quality percentage of described perfume preparation this be preferably: by Semen Maydis be main material fermentation, deodorize prepare ethanol 75.6%, deionized water 10%, essence 12%, muscone 0.2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 0.3%, galaxolid 1%, rest in peace balsam 0.2% and isopropyl myristate 0.2%.
Further, in above-mentioned perfume preparation, by Semen Maydis be main material fermentation, deodorize prepare ethanol 70%, deionized water 6%, essence 20%, muscone 2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 0.2%, galaxolid 1%, rest in peace balsam 0.1% and isopropyl myristate 0.2%.
The preparation method that the present invention also provides for a kind of perfume preparation, comprises the following steps:
Ethanol postincubation: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, being sufficiently stirred for after dissolving at-10 DEG C of temperature lucifuge places at least one week；Wherein, the percent mass of described ethanol this be 65%～85%, the mass percent of described muscone be 0.1%～2%, the percent mass of described benzoic acid Bian ester this be 0.1～2%, the percent mass of described Moschus 105 this be 0.1～3%, the mass percent of described salicylic acid Bian ester be 0.1～3%, the percent mass of described galaxolid this be 0.1～3%, described in the rest in peace mass percent of balsam be 0.1～1%；
Preparation perfume: in above-mentioned reaction vessel add mass percent be 3%～12% deionized water, mass percent be 3%～25% essence and percent mass this be the isopropyl myristate of 0.1～0.3%, after stirring at-10 DEG C of temperature miscible 3～5 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 0～18 DEG C of temperature, carries out ageing 15～30 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Further, in above-mentioned perfume formulation preparation method, the described each Ingredient percent of perfume preparation be preferably: by Semen Maydis be main material fermentation, deodorize prepare ethanol 75%, deionized water 10%, essence 10%, muscone 0.2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 2%, galaxolid 2%, rest in peace balsam 0.1% and isopropyl myristate 0.2%.
Further, in above-mentioned perfume formulation preparation method, each composition quality percentage of described perfume preparation this be preferably: by Semen Maydis be main material fermentation, deodorize prepare ethanol 70%, deionized water 6%, essence 20%, muscone 2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 0.2%, galaxolid 1%, rest in peace balsam 0.1% and isopropyl myristate 0.2%.
Perfume alcohol taste both stabilized by perfume preparation of the present invention and preparation method thereof, improves sweet clear (green grass or young crops) fragrant and quiet and tastefully laid out grade of perfume, substantially increases again the aroma retaining effect of perfume, improve quality and the class of perfume.
Detailed description of the invention
Below in conjunction with describing the preferred embodiments of the present invention in detail.
The present invention provides a kind of perfume preparation, and by percent mass, this is formulated by following for it:
By Semen Maydis be main material fermentation, deodorize prepare ethanol 65%～85%, deionized water 3%～12%, essence 3%～25%, muscone 0.1%～2%, benzoic acid Bian ester 0.1～2%, Moschus 105 (i.e. 11-oxahexadecanolide) 0.1～3%, salicylic acid Bian ester 0.1～3%, galaxolid 0.1～3%, rest in peace balsam 0.1～1% and isopropyl myristate 0.1～0.3%.
The each composition quality percentage of above-mentioned perfume preparation this be preferably: by Semen Maydis be main material fermentation, deodorize prepare ethanol 75%, deionized water 10%, essence 10%, muscone 0.2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 2%, galaxolid 2%, rest in peace balsam 0.1% and isopropyl myristate 0.2%.
The above-mentioned each Ingredient percent of perfume preparation be preferably: by Semen Maydis be main material fermentation, deodorize prepare ethanol 70%, deionized water 6%, essence 20%, muscone 2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 0.2%, galaxolid 1%, rest in peace balsam 0.1% and isopropyl myristate 0.2%.
Wherein, the superfine alcohol that it is main fermentation with Semen Maydis that the alcohol raw material in the present invention is chosen, and carry out deodorize process, it is determined that meet prerequisite basic demand during perfume makes.In perfume makes, ethanol is a primary raw material, almost accounts for the consumption of 80% in perfume.The class of the therefore quality of the ethanol quality to perfume, or even perfume is all most important.The high-grade food materials fermented soy such as the preferred Semen Maydis of ethanol in the present invention, to reduce the generation of by-product as far as possible, especially to perfume disadvantageous composition such as fusel, assorted ketone, assorted aldehydes etc., can be removed by deodorize, other by-products such as acids, particularly acetic acid, caproic acid etc. its can there is esterification lentamente with ethanol, the ethyl acetate generated or ethyl hexanoate, it is exactly people's sweet delicate fragrance loved by all, both the vinosity in perfume had been stabilized, promote again the esterification of ethanol, so as to get over Chen Yuexiang, improve sweet clear (green grass or young crops) fragrant and quiet and tastefully laid out grade of perfume.
Described muscone is the natural perfume material of a kind of rare costliness, and the saturated macrocyclic ketone only accounting for about 2% in the key aroma composition of natural Moschus is muscone.1906 from natural Moschus by isolated for this macrocyclic ketone out, nineteen twenty-six determines that its chemical constitution is 3-methylcyclopentadecanone.Later, again natural Moschus's composition is studied further, identify its fragrant composition and also have tens kinds of macrocyclic compound such as 5-cyclopentadecylene ketone, 3-methyl cyclotyidecanone, cyclotetradecanone, 5-ring tetradecene ketone, Moschus pyrans, muscopyridine.And 15 cyclic ketones in Moschus structure have the effect suppressing vapour pressure, thus can making the long-term lasting of fragrance, and the vapour pressure of ethanol is significantly high, is only second to aldehydes, the Moschus of 15 cyclic ketones inhibits the vapour pressure of ethanol just, has just had the effect stabilizing vinosity.It addition, adopt muscone as inorganic agent in aromatic, not only can stabilizing vinosity, perfume lasting is long, moreover it is possible to accelerate the ageing of perfume, makes the perfume can in a short time can be ripe, mellow and full, quiet and tastefully laid out.
The preparation method that the present invention also provides for a kind of above-mentioned perfume preparation, before preparation perfume, advanced person serves a round of liquor to the guests precision processing, then carries out preparation perfume, and it comprises the following steps:
Ethanol postincubation: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, being sufficiently stirred for after dissolving at-10 DEG C of temperature lucifuge places at least one week；Wherein, the percent mass of described ethanol this be 65%～85%, the percent mass of described muscone this be 0.1%～2%, the mass percent of described benzoic acid Bian ester be 0.1～2%, the percent mass of described Moschus 105 this be 0.1～3%, the mass percent of described salicylic acid Bian ester be 0.1～3%, the percent mass of described galaxolid this be 0.1～3%, described in rest in peace balsam percent mass this be 0.1～1%；
Preparation perfume: in above-mentioned reaction vessel add percent mass this be 3%～12% deionized water, percent mass this be 3%～25% essence and percent mass this be the isopropyl myristate of 0.1～0.3%, after stirring at-10 DEG C of temperature miscible 3～5 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 0～18 DEG C of temperature, carries out ageing 15～30 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Generally, perfume produce last procedure be ageing, and just the note of the perfume of output mellow and full not, harmonious, coordinate, namely not mature enough, typically requiring natural ageing half a year more than, this can bring the difficulty of capital turnover undoubtedly to enterprise, and product time of overstocking is long.And the present invention adopts muscone as inorganic agent in aromatic, not only can stabilize vinosity, perfume lasting is long, also use for reference Maotai and get over the fragrant principle of Chen Yue, the ageing of perfume can be accelerated, make perfume can get final product maturation in a short time, mellow and full, quiet and tastefully laid out, because alcohol content reaches 70～80% in perfume, ethanol and acids (the mainly acetic acid in by-product, caproic acid etc.), at low temperature, during the ageing of lucifuge stores, complete ageing subtlely, and this Chen Zuoyong of urging is apparent from, soon how this natural ageing, generally only need first quarter moon to one month, maturation can be made, mellow and full, quiet and tastefully laid out.
Compared to prior art, vinosity both stabilized by perfume preparation of the present invention and preparation method thereof, promotes again the esterification of ethanol, so as to get over Chen Yuexiang, improves sweet clear (green grass or young crops) fragrant and quiet and tastefully laid out grade of perfume；Be greatly reinforced aroma retaining effect, improve quality and the class of perfume, originally the domestic perfume of technique generally can only lasting 1～2 hour, the longest also difficult have lasting kind overnight.This new technology of employing can to lasting more than 4 days now, even lasting more than one month having.Separately, the present invention adopts promoting ageing more to improve grade to perfume quality, is also beneficial to capital turnover, improves utilization of area efficiency.
To sum up, perfume alcohol taste both stabilized by perfume preparation of the present invention and preparation method thereof, improves sweet clear (green grass or young crops) fragrant and quiet and tastefully laid out grade of perfume, substantially increases again the aroma retaining effect of perfume, improve quality and the class of perfume.
Below in conjunction with specific embodiment, perfume formulation preparation method of the present invention is described:
Embodiment 1
Before preparation perfume, advanced person serves a round of liquor to the guests precision processing: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, and after being sufficiently stirred for dissolving, at-10 DEG C of temperature, lucifuge places at least one week；Wherein, the mass percent of described ethanol be 75%, the mass percent of described muscone be 0.2%, the percent mass of described benzoic acid Bian ester this be 0.2%, the percent mass of described Moschus 105 this be 0.3%, the mass percent of described salicylic acid Bian ester be 2%, the percent mass of described galaxolid this be 2%, described in rest in peace balsam percent mass this be 0.1%；
Prepare perfume again: in above-mentioned reaction vessel add percent mass this be 10% deionized water, mass percent be 10% essence and percent mass this be the isopropyl myristate of 0.2%, after stirring at-10 DEG C of temperature miscible 5 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 18 DEG C of temperature, carries out ageing 30 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Embodiment 2
Before preparation perfume, advanced person serves a round of liquor to the guests precision processing: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, and after being sufficiently stirred for dissolving, at-10 DEG C of temperature, lucifuge places at least one week；Wherein, the percent mass of described ethanol this be 70%, the percent mass of described muscone this be 2%, the mass percent of described benzoic acid Bian ester be 0.2%, the percent mass of described Moschus 105 this be 0.3%, the percent mass of described salicylic acid Bian ester this be 0.2%, the percent mass of described galaxolid this be 1%, described in rest in peace balsam percent mass this be 0.1%；
Prepare perfume again: in above-mentioned reaction vessel add percent mass this be 6% deionized water, percent mass this be 20% essence and percent mass this be the isopropyl myristate of 0.2%, after stirring at-10 DEG C of temperature miscible 3 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 12 DEG C of temperature, carries out ageing 20 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Embodiment 3
Before preparation perfume, advanced person serves a round of liquor to the guests precision processing: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, and after being sufficiently stirred for dissolving, at-10 DEG C of temperature, lucifuge places at least one week；Wherein, the percent mass of described ethanol this be 65%, the mass percent of described muscone be 2%, the percent mass of described benzoic acid Bian ester this be 1%, the mass percent of described Moschus 105 be 3%, the percent mass of described salicylic acid Bian ester this be 3%, the percent mass of described galaxolid this be 3%, described in rest in peace balsam percent mass this be 0.9%；
Prepare perfume again: in above-mentioned reaction vessel add mass percent be 12% deionized water, mass percent be 10% essence and mass percent be the isopropyl myristate of 0.1%, after stirring at-10 DEG C of temperature miscible 4 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 0 DEG C of temperature, carries out ageing 30 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Embodiment 4
Before preparation perfume, advanced person serves a round of liquor to the guests precision processing: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, and after being sufficiently stirred for dissolving, at-10 DEG C of temperature, lucifuge places at least one week；Wherein, the percent mass of described ethanol this be 85%, the percent mass of described muscone this be 0.1%, the percent mass of described benzoic acid Bian ester this be 0.1%, the percent mass of described Moschus 105 this be 0.1%, the percent mass of described salicylic acid Bian ester this be 0.1%, the percent mass of described galaxolid this be 0.1%, described in rest in peace balsam percent mass this be 1%；
Prepare perfume again: in above-mentioned reaction vessel add percent mass this be 3% deionized water, percent mass this be 10.2% essence and percent mass this be the isopropyl myristate of 0.3%, after stirring at-10 DEG C of temperature miscible 4 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 16 DEG C of temperature, carries out ageing 15 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Embodiment 5
Before preparation perfume, advanced person serves a round of liquor to the guests precision processing: adding in reaction vessel by Semen Maydis is add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace in the ethanol for preparing of main fermentation, deodorize, and after being sufficiently stirred for dissolving, at-10 DEG C of temperature, lucifuge places at least one week；Wherein, the percent mass of described ethanol this be 77.5%, the mass percent of described muscone be 2%, the percent mass of described benzoic acid Bian ester this be 1%, the percent mass of described Moschus 105 this be 3%, the percent mass of described salicylic acid Bian ester this be 3%, the mass percent of described galaxolid be 3%, described in rest in peace balsam percent mass this be 0.1%；
Prepare perfume again: in above-mentioned reaction vessel add mass percent be 10% deionized water, percent mass this be 3% essence and percent mass this be the isopropyl myristate of 0.3%, after stirring at-10 DEG C of temperature miscible 4 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 18 DEG C of temperature, carries out ageing 20 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
Here description of the invention and application is illustrative, is not wishing to limit the scope of the invention in above-described embodiment.The deformation of embodiments disclosed herein and change are possible, for those skilled in the art embodiment replace and the various parts of equivalence are known.It should be appreciated by the person skilled in the art that when without departing from the spirit of the present invention or substitutive characteristics, the present invention can in other forms, structure, layout, this example, and realize with other assembly, material and parts.When without departing from the scope of the invention and spirit, it is possible to embodiments disclosed herein is carried out other deformation and changes.
Claims (2)
1. a perfume preparation, it is characterised in that it is formulated by mass percentage by following component:
By Semen Maydis be main material fermentation, deodorize prepare ethanol 65%～85%, deionized water 3%～12%, essence 3%～25%, muscone 0.1%～0.2%, benzoic acid Bian ester 0.1～2%, Moschus 1050.1～3%, salicylic acid Bian ester 0.1～3%, galaxolid 0.1～3%, rest in peace balsam 0.1～1% and isopropyl myristate 0.1～0.3%；
The preparation method of described perfume preparation comprises the following steps:
Ethanol postincubation: add in reaction vessel by Semen Maydis and be the ethanol for preparing of main fermentation, deodorize and add muscone, benzoic acid Bian ester, Moschus 105, salicylic acid Bian ester, galaxolid, balsam of resting in peace, being sufficiently stirred for after dissolving at-10 DEG C of temperature lucifuge places at least one week；Wherein, the mass percent of described ethanol be 65%～85%, the mass percent of described muscone be 0.1%～0.2%, the mass percent of described benzoic acid Bian ester be 0.1～2%, the mass percent of described Moschus 105 be 0.1～3%, the mass percent of described salicylic acid Bian ester be 0.1～3%, the mass percent of described galaxolid be 0.1～3%, described in the rest in peace mass percent of balsam be 0.1～1%；
Preparation perfume: in above-mentioned reaction vessel add mass percent be 3%～12% deionized water, mass percent be 3%～25% essence and mass percent be the isopropyl myristate of 0.1～0.3%, after stirring at-10 DEG C of temperature miscible 3～5 hours filter；
Reaction vessel after above-mentioned filtration is positioned between ageing at 0～18 DEG C of temperature, carries out ageing 15～30 days；
Product after above-mentioned ageing is filtered and fills packaging and namely obtain described perfume preparation.
2. perfume preparation according to claim 1, it is characterized in that, the described each Ingredient percent of perfume preparation be preferably: by Semen Maydis be main material fermentation, deodorize prepare ethanol 75%, deionized water 10%, essence 10%, muscone 0.2%, benzoic acid Bian ester 0.2%, Moschus 1050.3%, salicylic acid Bian ester 2%, galaxolid 2%, rest in peace balsam 0.1% and isopropyl myristate 0.2%.
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| CN104922001B (en) * | 2015-06-30 | 2017-08-25 | 陈孟桃 | Longaacting fragrance-aretaining perfume, scented tea and preparation method thereof |
| CN110179705A (en) * | 2019-05-22 | 2019-08-30 | 田丹 | It is a kind of to sterilize peculiar smell perfume and preparation method thereof of dispelling |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1147404A (en) * | 1996-01-15 | 1997-04-16 | 门摩西 | Cold-preventing perfume |
| CN1219195A (en) * | 1996-03-22 | 1999-06-09 | 普罗格特-甘布尔公司 | Detergent compositions containing fragrance precursors and the fragrance precursors themselves |
| CN101991524A (en) * | 2009-08-12 | 2011-03-30 | 韩丽丽 | Refreshing perfume containing natural plants |
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2014
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1147404A (en) * | 1996-01-15 | 1997-04-16 | 门摩西 | Cold-preventing perfume |
| CN1219195A (en) * | 1996-03-22 | 1999-06-09 | 普罗格特-甘布尔公司 | Detergent compositions containing fragrance precursors and the fragrance precursors themselves |
| CN101991524A (en) * | 2009-08-12 | 2011-03-30 | 韩丽丽 | Refreshing perfume containing natural plants |
Non-Patent Citations (1)
| Title |
|---|
| 香水级酒精的制程;佚名;《http://miaroma.shop2000.com.tw/news/148101》;20130130;第1页 * |
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