CN103783349A - Process for preparing honeycomb polyphenol extractive microcapsule by adopting spray drying method - Google Patents
Process for preparing honeycomb polyphenol extractive microcapsule by adopting spray drying method Download PDFInfo
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- CN103783349A CN103783349A CN201410056041.2A CN201410056041A CN103783349A CN 103783349 A CN103783349 A CN 103783349A CN 201410056041 A CN201410056041 A CN 201410056041A CN 103783349 A CN103783349 A CN 103783349A
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- honeycomb
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- polyphenol
- spray drying
- microcapsule
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- 235000013824 polyphenols Nutrition 0.000 title claims abstract description 27
- 239000003094 microcapsule Substances 0.000 title claims abstract description 26
- 150000008442 polyphenolic compounds Chemical class 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 18
- 238000001694 spray drying Methods 0.000 title claims abstract description 11
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000000284 extract Substances 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 239000007787 solid Substances 0.000 claims abstract description 15
- 230000008569 process Effects 0.000 claims abstract description 14
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 241000241413 Propolis Species 0.000 claims abstract description 9
- 229940069949 propolis Drugs 0.000 claims abstract description 9
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 7
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 7
- 235000010489 acacia gum Nutrition 0.000 claims abstract description 7
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims abstract description 7
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 6
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 6
- 238000005516 engineering process Methods 0.000 claims description 15
- 238000003809 water extraction Methods 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 4
- 241000196324 Embryophyta Species 0.000 claims description 3
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims description 2
- 241000206575 Chondrus crispus Species 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims description 2
- 240000008042 Zea mays Species 0.000 claims description 2
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 2
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims description 2
- 235000014633 carbohydrates Nutrition 0.000 claims description 2
- 150000001720 carbohydrates Chemical class 0.000 claims description 2
- 235000005822 corn Nutrition 0.000 claims description 2
- 235000010987 pectin Nutrition 0.000 claims description 2
- 229920001277 pectin Polymers 0.000 claims description 2
- 239000001814 pectin Substances 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 239000006188 syrup Substances 0.000 claims description 2
- 235000020357 syrup Nutrition 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 6
- 230000002572 peristaltic effect Effects 0.000 abstract description 5
- 238000001914 filtration Methods 0.000 abstract description 2
- 239000011259 mixed solution Substances 0.000 abstract 2
- 238000002156 mixing Methods 0.000 abstract 2
- 239000011344 liquid material Substances 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 7
- 238000011160 research Methods 0.000 description 6
- 238000000605 extraction Methods 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 241000256844 Apis mellifera Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 206010039083 rhinitis Diseases 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 1
- 235000009434 Actinidia chinensis Nutrition 0.000 description 1
- 244000298697 Actinidia deliciosa Species 0.000 description 1
- 235000009436 Actinidia deliciosa Nutrition 0.000 description 1
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
- -1 DPPH free radical Chemical class 0.000 description 1
- 240000000950 Hippophae rhamnoides Species 0.000 description 1
- 235000003145 Hippophae rhamnoides Nutrition 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001452 anthocyanidin derivatives Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 235000013871 bee wax Nutrition 0.000 description 1
- 239000012166 beeswax Substances 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 229940074391 gallic acid Drugs 0.000 description 1
- 235000004515 gallic acid Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
- 231100000283 hepatitis Toxicity 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920006254 polymer film Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 201000003068 rheumatic fever Diseases 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Medicinal Preparation (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The invention discloses a process for preparing a honeycomb polyphenol extractive microcapsule by adopting a spray drying method and belongs to the field of microcapsule preparation. The process comprises the steps: sieving honeycomb powder by a 40-mesh sieve, mixing the honeycomb powder passing through the 40-mesh sieve and deionized water with the liquid-material ratio being 20-40/1(w/v), fully stirring by adopting a magnetic water-bath stirring bar, extracting 6-8min at the temperature being 30-50 DEG C so as to obtain a honeycomb water extract liquid, concentrating the honeycomb water extract liquid to obtain a product of which the content of solid contents is more than 10%, adding 280-350ml of the honeycomb water extract liquid in maltodextrin in which the content of a solid propolis water extractive is within 65-75% and Arabic gum in which the content of a solid propolis water extractive is within 3-5%, blending to obtain a mixed solution, filtering the mixed solution to obtain filter liquor, and carrying out spray drying on the filter liquor under a condition that the feeding amount of a peristaltic pump is 300-400ml/h so as to obtain the honeycomb polyphenol extractive microcapsule. The honeycomb polyphenol extractive microcapsule prepared by adopting the process is spherical, smooth in appearance, free from cracks, capable of increasing the bioavailability of honeycomb polyphenol, and high in heat stability; the embedding rate can be up to 46.6%.
Description
technical field
The present invention relates to a kind of preparation technology field of microcapsules, particularly relate to a kind of preparation technology of honeycomb polyphenol microcapsules.
Background technology
Honeycomb is honeycomb, is honeybee life, raises up seed and the place of storage food, is built and is formed by the secreted beeswax processing of the wax gland of worker bee.Honeycomb is not only nutritious, nontoxic, and has the effects such as antibacterial, anti-inflammatory, inhibition tumour, and therefore honeycomb will have wide practical use in food industry.Honeycomb medical value is also very high, conventional fresh clean honeycomb treatment rhinitis.Old honeycomb has the curative effect of the diseases such as treatment hepatitis, rhinitis and rheumatic arthritis.Research shows, honeycomb preparation has the effect that promotes Immune Function.
Polyphenol is the general name of Polyhydroxy phenol, take phenol as basic framework, comprises the natural phenolics such as tannin, anthocyanidin, catechin, an essence, gallic acid.Research shows: phenolic compound has the functions such as reducing blood lipid, anti arteriosclerosis, reduction cholesterol, antitumor, anti-inflammatory, can suppress autoxidation, remove hydroxyl, DPPH free radical, superoxide anion.
Microcapsules technology is that micro substance is wrapped in the technology in thin polymer film, is the microdisplay package technology of a kind of store solids, liquid, gas, and its effect has: effectively reduce the active material reaction of environmental factor to external world; Reduce diffusion and the evaporation of core to environment; Control the release of core; Shelter the peculiar smell of core; Change physical property, the chemical property etc. of core.For food industry, microcapsules technology can make local flavor batching, the bioactivator of pure natural incorporate food system, and can keep biologically active, and many traditional technical process are simplified, also can make the insurmountable technological problems of many common technological means be resolved simultaneously.
Have at present the research that utilizes ultrasonic auxiliary extraction to extract the polyphenol substance flavones in honeycomb, but polyphenol has phenolic hydroxyl group, easily oxidized, generally contact air non-enzymatic browning has just easily occurred.At present the research of microcapsules is comprised the microencapsulation of Seabuckthorn Oil, folium cortex eucommiae water extract, kiwi polyphenol etc., the also not research to propolis polyphenol microcapsules.In order to prevent the oxidation in storing of honeycomb polyphenol extract, adopt spray drying process herein, research honeycomb polyphenol extract is prepared microcapsules technology, explores the technology of storage and transport of honeycomb polyphenol extract.
Summary of the invention
The invention provides a kind of preparation technology of honeycomb extract polyphenol microcapsules, the polyphenol microcapsules embedding rate obtaining is by this method high, and embedding is effective, and embedding rate reaches 46.6%, and its glass transition temperature is brought up to 86 ℃ from 59.6 ℃, is beneficial to storing.
For achieving the above object, this experiment has adopted following technical scheme: a kind of spray drying process is prepared honeycomb polyphenol extract micro capsule technology, carries out according to following step:
(1) honeycomb powder being crossed to 20 ~ 40 mesh sieves and deionized water liquid ratio (w/v) is 20 ~ 40/1 to mix, and using rotating speed is that 500 ~ 700rpm magnetic force stirring in water bath device fully stirs, and extracts 6 ~ 8min and obtain honeycomb water extraction liquid at 30 ~ 50 ℃.
(2) honeycomb water extraction liquid is concentrated into solid content between mass ratio 10% ~ 15%, the carbohydrate wall materials such as the maltodextrin of interpolation Water extracts of propolis solid content mass ratio 65-75% or starch, corn syrup, trehalose.
And add the plant hydrophilic gels such as the Arabic gum of Water extracts of propolis solid content mass ratio 3-5% or pectin, carragheen and allocate (3).
(4) mixed liquor is sprayed filtrate and is dried after filtering under the condition of peristaltic pump inlet amount 300 ~ 400ml/h, obtains honeycomb polyphenol extract microcapsules.
Spray-dired process conditions are: 160 ~ 200 ℃ of intake air temperatures, air outlet temperature is 70 ~ 100 ℃.Charging rate is according to equipment difference, by air outlet Temperature Setting.
Preparation method of the present invention has following features:
(1) honeycomb particle sieves, and less raw material granularity can reduce the distance of material Transfer on the one hand, has increased on the other hand the contact area of material and solvent, thereby has shortened extraction time, has improved extraction efficiency.
(2) water is better than methyl alcohol, ethanol, acetoneand ethyl acetate as extracting solvent effect.
(3), in whole leaching process, extraction vessel is all the time with aluminium-foil paper parcel, with the Oxidative demage that stops light to cause.After extracting, adopt suction method that extract is separated with solid residue, extract is placed in the brown volumetric flask constant volume of 100 mL.
(4) in spray-drying process, add maltodextrin and Arabic gum and can effectively prevent the glutinous wall phenomenon of the heat of spraying while being dried, significantly improve the effect that spray drying process is prepared honeycomb microcapsules.
(5) this good product quality, microcapsule particle is spherical in shape, and smooth in appearance is flawless, and microcapsule embedded effect is better, compares traditional handicraft, and process is simplified more, and Heat stability is good is beneficial to storing.
The specific embodiment
Embodiment 1
(1) the 4 g honeycomb powder that took 20 mesh sieve mix with 160mL deionized water, and use rotating speed is that the magnetic force stirring in water bath device of 600 rpm fully stirs, and at 50 ℃, extracts 6min.
(2) honeycomb water extraction liquid is concentrated into solid content more than 10%, gets 280mL honeycomb water extraction liquid, add the maltodextrin of 28.56g and the Arabic gum of 2.041g and allocate.
(3) mixed liquor filter after by filtrate 180 ℃ of intake air temperatures, 80 ℃ of air outlet temperature, under the condition of peristaltic pump inlet amount 300ml/h spraying dry, obtain honeycomb polyphenol extract microcapsules.
Embodiment 2
(1) the 3.8g honeycomb powder that took 30 mesh sieve mixes with 120mL deionized water, and use rotating speed is that the magnetic force stirring in water bath device of 650 rpm fully stirs, and at 40 ℃, extracts 7min.
(2) honeycomb water extraction liquid is concentrated into solid content more than 10%, gets 290mL honeycomb water extraction liquid, add the maltodextrin of 27.14g and the Arabic gum of 1.987g and allocate.
(3) mixed liquor filter after by filtrate 160 ℃ of intake air temperatures, air outlet temperature 70 C, under the condition of peristaltic pump inlet amount 350ml/h spraying dry, obtain honeycomb polyphenol extract microcapsules.
Embodiment 3
(1) the 4.5g honeycomb powder that took 40 mesh sieve mixes with 90mL deionized water, and use rotating speed is that the magnetic force stirring in water bath device of 700 rpm fully stirs, and at 30 ℃, extracts 8min.
(2) honeycomb water extraction liquid is concentrated into solid content more than 10%, gets 350mL honeycomb water extraction liquid, the maltodextrin of interpolation 32.64 and the Arabic gum of 2.448g are allocated.
(3) mixed liquor filter after by filtrate 200 ℃ of intake air temperatures, 100 ℃ of air outlet temperature, under the condition of peristaltic pump inlet amount 400ml/h spraying dry, obtain honeycomb polyphenol extract microcapsules.
Claims (3)
1. spray drying process is prepared a honeycomb polyphenol extract micro capsule technology, it is characterized in that carrying out according to following step:
It is 20 ~ 40/1 to mix that honeycomb powder is crossed to 20 ~ 40 mesh sieves and deionized water liquid ratio (w/v), and using rotating speed is that 500 ~ 700rpm magnetic force stirring in water bath device fully stirs, and extracts 6 ~ 8min and obtain honeycomb water extraction liquid at 30 ~ 50 ℃;
Honeycomb water extraction liquid is concentrated into solid content between mass ratio 10% ~ 15%, adds carbohydrate wall material to Water extracts of propolis;
And add plant hydrophilic gel to Water extracts of propolis solid content and allocate.
2. a kind of spray drying process according to claim 1 is prepared honeycomb polyphenol extract micro capsule technology, it is characterized in that adding in step (2) maltodextrin of Water extracts of propolis solid content mass ratio 65-75% or starch, corn syrup, trehalose.
3. a kind of spray drying process according to claim 1 is prepared honeycomb polyphenol extract micro capsule technology, it is characterized in that in step (3) and adds the Arabic gum of Water extracts of propolis solid content mass ratio 3-5% or the plant hydrophilic gel such as pectin, carragheen is allocated.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104739880A (en) * | 2015-03-28 | 2015-07-01 | 郭云胶 | Antiallergic liquid capable of effectively eliminating allergies caused by wasp products, and preparation method and application of the antiallergic liquid |
| CN109170889A (en) * | 2018-09-20 | 2019-01-11 | 浙江大学 | A kind of preparation method of honey pear fruit polyphenol microcapsules |
| WO2020169425A1 (en) | 2019-02-19 | 2020-08-27 | Hedera D.O.O. | Liquid propolis extract, its formulation and use thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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| CN109170889A (en) * | 2018-09-20 | 2019-01-11 | 浙江大学 | A kind of preparation method of honey pear fruit polyphenol microcapsules |
| CN109170889B (en) * | 2018-09-20 | 2021-09-28 | 浙江大学 | Preparation method of honey pear fruit polyphenol microcapsules |
| WO2020169425A1 (en) | 2019-02-19 | 2020-08-27 | Hedera D.O.O. | Liquid propolis extract, its formulation and use thereof |
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