CN103740559A - Production method of lucid ganoderma compound wine - Google Patents
Production method of lucid ganoderma compound wine Download PDFInfo
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- CN103740559A CN103740559A CN201410016815.9A CN201410016815A CN103740559A CN 103740559 A CN103740559 A CN 103740559A CN 201410016815 A CN201410016815 A CN 201410016815A CN 103740559 A CN103740559 A CN 103740559A
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Abstract
The invention provides a production method of lucid ganoderma compound wine, aiming at solving the problems that the lucid ganoderma compound wine is turbid and changed in color after the wine is reduced in degree or stored for a long time. The method is characterized in that the characteristic that the absorption capacity of the grain flour containing high carbohydrate to protein is stronger than that of a tannin compound (polyphenol compound) is utilized, the grain flour is added into the compound wine, so that the problem that the precipitate is produced because large molecules are formed due to the combination of the proteins in the compound wine with the tannin compound in the presence of chemical measuring ratio can be solved, the turbidity and color changing condition of the compound wine can be effectively eliminated by utilizing the measures of utilizing purified basic wine and limiting the water for the compounding, and the defects of turbidity and color changing of the compound wine after the wine is reduced in degree or the wine is stored for a long time can be avoided. The lucid ganoderma compound wine produced through the method is clear and transparent in appearance, pure in color and not turbid and changed in color after being stored for a long time; moreover, the process is simple, the cost is low, and easiness in industrialization production can be realized.
Description
Technical field
The present invention relates to coloured assembled alcoholic drinks, specifically belong to a kind of production method of glossy ganoderma assembled alcoholic drinks, the muddiness, the discoloration problem that when the method has solved glossy ganoderma assembled alcoholic drinks at degree of falling or has been long placed in (shelf-lives), have occurred.
Background technology
At present, glossy ganoderma assembled alcoholic drinks is mainly take glossy ganoderma as raw material or other medicinal material of reasonable compatibility, through pure grain brewing original plasm wine, soaks, filters, and is then joined to the auxiliary materials such as honey filtrate adding and blends and form.Its outward appearance is generally golden yellow color to orange red, as clear as crystal liquid.There is the effect of brain-nourishing intelligence-benefiting, cancer-resisting, strengthening body.But, in this wine liquid, contain the materials such as a certain amount of protein, tannin, pectin, phlegmatic temperament, conventionally at degree of falling or after placing for some time (shelf-lives), wine body becomes muddy, color and luster is dim, and with variable color (brown stain) phenomenon, has a strong impact on quality, outward appearance and the production efficiency of Lucid Ganoderma wine.
This seminar to glossy ganoderma assembled alcoholic drinks muddiness, change color to because conducting in-depth research, result shows: Lucid Ganoderma wine is blending, in degree of falling and storage, from the protein,alcohol-soluble of medicinal material and tannins (polyphenolic compound) in conjunction with and from compounds such as the high-grade aliphatic esters of base wine, to separate out be muddy major cause; Browning phenomenon is mainly to add lustre to due to thing and metallic ion coordination or pH value change.
For Lucid Ganoderma wine, remove in process of production purifying method at present, Chinese patent CN102120951B has reported first coarse filtration, the method that essence is filtered again, and its essence filtration journey often causes absurd creature and is difficult to flocculate, and filters very difficult.Chinese patent CN101024809B has reported cold method, and effect is relatively better, but energy consumption is larger, and single freezing treatment is also difficult to the clarifying effect that reaches desirable.Ordinary method: ultrafiltration process is take pressure reduction as impellent, application microporous membrane is as filtration medium, and cost is higher, and especially to adding, to join the colloidal solution efficiency of honey also lower.Finings flocculence is a kind of method simple and easy to do, with low cost, conventional finings has gelatin, diatomite, wilkinite, chitosan etc., gelatin is to utilize itself positively charged and electronegative material phase-polymerization and suspended particulates absorption in wine is sunk, reach clarifying effect, especially remove tannin, tannin polyphenolic compound effect is better, if and owner's aromatic series pigment that adds lustre to of Lucid Ganoderma wine takes off so use its colourity of gelatin greatly to subtract; Diatomaceous chemical composition is take SiO2 as main, there is special porousness structure, can destroy in wine the colloid or the class colloidal structure that because of gelatinoid and carbohydrate, cause, gelatinoid is precipitated completely as far as possible, but for the turbidity removal of Lucid Ganoderma wine, have a certain amount of metal ion, particularly transition metal ion and enter wine body, and with wine in thing coordination generation variable color (brown stain) phenomenon of adding lustre to; Wilkinite can make Lucid Ganoderma wine reach good clarifying effect equally, but it is also stronger to pigment absorption, has similar diatomaceous problem simultaneously, fades, metachromatism is very obvious; Chitosan is the straight chain saccharan of glucosamine, and its structure is given chitosan polyphenolic compound, protein and the material that shows slightly negative charge are had to good Adsorption and flocculation effect.At aspects such as garden spgarden stuff, drinks, drink, medicines, be widely used.Chinese patent CN1170757A has proposed chitosan and derivative thereof and acid as finings, finds that effect is better than ethanol and tannin-gelatin method, but single chitosan exist the clarification cycle long, produce the floss shortcoming such as not tight of condensing.Chinese patent CN1857124A has proposed chitosan and the xanthan gum coupling method as finings, the method be better than single chitosan can solve the clarification cycle long, process the shortcomings such as clarity is high not.But xanthan gum is poorly soluble, before use, need heating to stir evenly, as stir insufficiently, will there is agglomeration problems.The existing supernatant of system has again precipitation simultaneously, therefore, has both needed screen cloth, filter cloth etc. to filter supernatant, needs again centrifugal removal precipitation, operates comparatively loaded down with trivial details.Chinese patent CN101716011A has proposed the fluent meterial defecation method of chitosan and carrageenin coupling.Solved the problem of length consuming time, complex operation.But all there is the problem of a general character for the turbidity removal of Lucid Ganoderma wine in above-mentioned all methods, that is: fail to solve Lucid Ganoderma wine at degree of falling or be long placed in (shelf-lives) process become turbid, the problem such as variable color.
Summary of the invention
The muddiness, the discoloration problem that when the object of the invention is to for glossy ganoderma assembled alcoholic drinks at degree of falling or being long placed in, occur, a kind of production method of glossy ganoderma assembled alcoholic drinks is provided, the Lucid Ganoderma wine of producing by this method, outward appearance is as clear as crystal, color and luster is pure, be long placed in haze-free, nondiscoloration, and technique is simple, cost is lower, be easy to realize suitability for industrialized production.
For achieving the above object, the production method of a kind of glossy ganoderma assembled alcoholic drinks provided by the invention, comprises the steps:
1) get the magma white wine of pure grain brewing, add the gac of white wine weight 0.5%-1%, every 4h stirs once, stirs 15-60min at every turn, processes continuously after 48-72h, and standing 10-24h, filters, and obtains base wine;
2) get section glossy ganoderma and add base wine immersion 7-30 days in the ratio of feed liquid weight ratio 1 ︰ 9-15, filter, the dregs of a decoction add base wine by above-mentioned solid-liquid ratio again and soak 3-7 days, filter, and merge twice filtrate and obtain steeping in wine liquid;
3) dregs of a decoction after steeping in wine, again in the ratio boiling 0.5-2h of feed liquid weight ratio 1 ︰ 2-15, filter, and under the same conditions, the dregs of a decoction again re-treatment once, merge twice filtrate, obtain decocting liquid;
4) merge steeping in wine liquid and decocting liquid, and add honey by the 1.5-2.5% of liquid gross weight, stir, obtain rough Lucid Ganoderma wine;
5) in rough Lucid Ganoderma wine, add the grain flour containing Hi CHO, its addition is the 1%-5% of rough Lucid Ganoderma wine weight, stirs 15-60min, and standing 10-24h filters, and obtains Lucid Ganoderma wine.
Described glossy ganoderma can be also glossy ganoderma and the medicinal material that mixes of other medicinal material reasonable compatibility.
Described grain flour can be corn flour, millet flour or milled glutinous broomcorn millet flour etc.
Described water must be distilled water or deionized water or softening water.
The present invention produces with existing Lucid Ganoderma wine compared with (turbidity removal, protect look) method, has the following advantages:
1, the present invention is soluble in the feature of white wine and hot water according to effective component of glossy ganoderma, has adopted steeping in wine, decocting method, and its effective constituent is entered in wine as much as possible.
2, the grain flour that the present invention adopts has good absorption, flocculation ability to the albumen in Lucid Ganoderma wine, pectin, has prevented colloid that in wine, gelatinoid and carbohydrate cause or the formation of class colloidal structure.Make normal temperature, common filtration in process of production, obtained wine thereby liquid is as clear as crystal, with ultraviolet spectrometer, measures, and adding lustre to, thing can reach more than 97% without absorption place transmitance.
3, the present invention finds according to Lucid Ganoderma wine muddiness, variable color study on the genesis: when albumen and tannins (polyphenolic compound) exist by stoichiometric ratio in this system, easily form macromole and produce precipitation; Utilize the grain flour of Hi CHO protein adsorption to be better than to the characteristic of tannins (polyphenolic compound), add grain flour to break the stoichiometric ratio that albumen and tannins exist in system, effectively avoided the drawback in shelf-lives muddiness.And colourity is influenced hardly, and color and luster greatly takes on a new look.
4, the thorough elimination of the present invention to base wine Fatty Acids ester compound, makes without lipid-soluble substance, to separate out when degree of falling, and has avoided higher fatty acid ester compound water insoluble and make the phenomenon of wine liquid muddiness.
5, the present invention is mainly thing and metallic ion coordination or the pH value conclusion due to changing of adding lustre to according to the brown stain origin cause of formation, in Lucid Ganoderma wine processing, fall spend journey in regulation water must be distilled water or deionized water or softening water, assurance is provided for Lucid Ganoderma wine color and luster is stable.
6, the still edible of grain flour reclaiming after filtration, has reduced production cost.
Embodiment
Embodiment 1
Get 65 degree magma rice wine 110Kg, be placed in the storage tank with electric stirring, add 0.6Kg active carbon for liquor, within every 4 hours, stir once, stir 30min at every turn.Process continuously 72h, standing 12h, subsequent filtration, obtains base wine standby.
Get section glossy ganoderma 5Kg and be placed in immersion still, add above-mentioned base wine 50Kg, soak 10 days, filtration, the dregs of a decoction add base wine by above-mentioned solid-liquid ratio again and soak 5 days, filter, and merge twice filtrate and obtain steeping in wine liquid;
The dregs of a decoction after steeping in wine add 15Kg deionized water to decoct again 1 hour, leach decocting liquid, and under the same conditions, the dregs of a decoction again re-treatment once, merge twice filtrate, and static 4h gets supernatant liquor and is evaporated to 20Kg and obtains decocting liquid.
Merge steeping in wine liquid and decocting liquid, and add 2.5Kg honey, after stirring, add corn flour 5Kg, continue to stir 45min, hold over night, normal temperature, ceramic sand rod filter, the 53 degree Lucid Ganoderma wine 122.5Kg that gained color and luster is orange red, as clear as crystal.With ultraviolet spectrometer, measure, adding lustre to, thing is 97.8% without absorption place transmitance; This wine normal temperature is placed 1 year without muddy, metachromatism.
Embodiment 2
25Kg deionized water decocts for the dregs of a decoction after steeping in wine, decocting liquid is concentrated into 41Kg, add honeybee close for 3Kg, to add corn flour be that 5.0Kg and the churning time of adding after corn flour are 30min, all the other operations and condition are identical with embodiment 1.The about 144Kg of Lucid Ganoderma wine wine liquid of gained golden yellow color, as clear as crystal 45 degree.With ultraviolet spectrometer, measure, adding lustre to, thing is 98.2% without absorption place transmitance; This wine normal temperature is placed 1 year without muddy, metachromatism.
Embodiment 3
40Kg deionized water decocts for the dregs of a decoction after steeping in wine, decocting liquid is concentrated into 67Kg, add honeybee close for 3.5Kg, to add corn flour be that 5.0Kg and the churning time of adding after corn flour are 30min, all the other operations and condition are identical with embodiment 1.The about 170Kg of Lucid Ganoderma wine wine liquid of gained golden yellow color, as clear as crystal 38 degree.With ultraviolet spectrometer, measure, adding lustre to, thing is 98.8% without absorption place transmitance; This wine normal temperature is placed 1 year without muddy, metachromatism.
Embodiment 4
65Kg deionized water decocts for the dregs of a decoction after steeping in wine, decocting liquid is concentrated into 128Kg, add honeybee close for 4.5Kg, to add corn flour be that 5.0Kg and the churning time of adding after corn flour are 30min, all the other operations and condition are identical with embodiment 1.The about 232Kg of Lucid Ganoderma wine wine liquid of gained golden yellow color, as clear as crystal 28 degree.With ultraviolet spectrometer, measure, adding lustre to, thing is 98.9% without absorption place transmitance; This wine normal temperature is placed 1 year without muddy, metachromatism.
Embodiment 5
Except getting section glossy ganoderma formula, be: the mixing medicinal material of glossy ganoderma 2.6Kg, matrimony vine 0.6Kg, Radix Astragali 0.6Kg, Chinese yam 0.6Kg, shizandra berry 0.6Kg replaces, all the other operations and condition are identical with embodiment 1.The 53 degree Lucid Ganoderma wine 122Kg that gained color and luster is orange red, as clear as crystal.With ultraviolet spectrometer, measure, adding lustre to, thing is 97.2% without absorption place transmitance; This wine normal temperature is placed 1 year without muddy, metachromatism.
Method of the present invention is also applicable to the production of other coloured assembled alcoholic drinkss of similar glossy ganoderma assembled alcoholic drinks.
Claims (4)
1. a production method for glossy ganoderma assembled alcoholic drinks, is characterized in that, comprises the steps:
1) get the magma white wine of pure grain brewing, add the gac of white wine weight 0.5%-1%, every 4h stirs once, stirs 15-60min at every turn, processes continuously after 48-72h, and standing 10-24h, filters, and obtains base wine;
2) get section glossy ganoderma and add base wine immersion 7-30 days in the ratio of feed liquid weight ratio 1 ︰ 9-15, filter, the dregs of a decoction add base wine by above-mentioned solid-liquid ratio again and soak 3-7 days, filter, and merge twice filtrate and obtain steeping in wine liquid;
3) dregs of a decoction after steeping in wine, again in the ratio boiling 0.5-2h of feed liquid weight ratio 1 ︰ 2-15, filter, and under the same conditions, the dregs of a decoction again re-treatment once, merge twice filtrate, obtain decocting liquid;
4) merge steeping in wine liquid and decocting liquid, and add honey by the 1.5-2.5% of liquid gross weight, stir, obtain rough Lucid Ganoderma wine;
5) in rough Lucid Ganoderma wine, add the grain flour containing Hi CHO, its addition is the 1%-5% of rough Lucid Ganoderma wine weight, stirs 15-60min, and standing 10-24h filters, and obtains Lucid Ganoderma wine.
2. the production method of a kind of glossy ganoderma assembled alcoholic drinks as claimed in claim 1, is characterized in that, described glossy ganoderma uses glossy ganoderma to substitute with the medicinal material that mixes of other medicinal material reasonable compatibility.
3. the production method of a kind of glossy ganoderma assembled alcoholic drinks as claimed in claim 1, is characterized in that, described grain flour is corn flour, millet flour or milled glutinous broomcorn millet flour.
4. the production method of a kind of glossy ganoderma assembled alcoholic drinks as claimed in claim 1, is characterized in that, described water is distilled water, deionized water or softening water.
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| CN201410016815.9A CN103740559B (en) | 2014-01-15 | 2014-01-15 | A kind of production method of lucid ganoderma compound wine |
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| CN201410016815.9A CN103740559B (en) | 2014-01-15 | 2014-01-15 | A kind of production method of lucid ganoderma compound wine |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1101287A (en) * | 1993-10-04 | 1995-04-12 | 邓凤翔 | Preparation of lucid ganoderma spirit |
| CN1105590A (en) * | 1994-07-07 | 1995-07-26 | 冯选凹 | Method for producing glossy ganoderma wine |
| CN1408844A (en) * | 2001-09-26 | 2003-04-09 | 滕树材 | Chinese medicinal wine for long life |
| KR20110056113A (en) * | 2009-11-20 | 2011-05-26 | 진도군 | Method of producing aged hong-joo with enriched flavor |
| CN103305382A (en) * | 2013-06-27 | 2013-09-18 | 宁夏红中宁枸杞制品有限公司 | Preparation method of lycium barbarum health wine |
-
2014
- 2014-01-15 CN CN201410016815.9A patent/CN103740559B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1101287A (en) * | 1993-10-04 | 1995-04-12 | 邓凤翔 | Preparation of lucid ganoderma spirit |
| CN1105590A (en) * | 1994-07-07 | 1995-07-26 | 冯选凹 | Method for producing glossy ganoderma wine |
| CN1408844A (en) * | 2001-09-26 | 2003-04-09 | 滕树材 | Chinese medicinal wine for long life |
| KR20110056113A (en) * | 2009-11-20 | 2011-05-26 | 진도군 | Method of producing aged hong-joo with enriched flavor |
| CN103305382A (en) * | 2013-06-27 | 2013-09-18 | 宁夏红中宁枸杞制品有限公司 | Preparation method of lycium barbarum health wine |
Non-Patent Citations (2)
| Title |
|---|
| 徐德华: "一种特制灵芝酒的试制报告", 《怀化师专学报》 * |
| 梁利和，等: "低温-淀粉吸附法生产低度白酒技术", 《江苏食品与发酵》 * |
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Granted publication date: 20150729 Termination date: 20180115 |