CN103737194A - Welding material and manufacturing method thereof - Google Patents
Welding material and manufacturing method thereof Download PDFInfo
- Publication number
- CN103737194A CN103737194A CN201310715276.3A CN201310715276A CN103737194A CN 103737194 A CN103737194 A CN 103737194A CN 201310715276 A CN201310715276 A CN 201310715276A CN 103737194 A CN103737194 A CN 103737194A
- Authority
- CN
- China
- Prior art keywords
- welding material
- silver
- melting
- zirconium
- yttrium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/26—Selection of soldering or welding materials proper with the principal constituent melting at less than 400 degrees C
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/02—Making non-ferrous alloys by melting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C30/00—Alloys containing less than 50% by weight of each constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/002—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working by rapid cooling or quenching; cooling agents used therefor
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Arc Welding In General (AREA)
Abstract
Provided are a welding material and a manufacturing method thereof. The welding material comprises, by mass, antimony 15-20%, zirconium 25-35%, silver 10-20% and the balance yttrium. Due to the fact that the multi-component alloy welding material is manufactured by the antimony, the zirconium, the silver and the yttrium, a melting point reaches to 275-300 DEG C, and a wetting angle formed by the welding material and a base plate is 15-25 degrees, and lead applied to the welding material is replaced on the basis that excellent performance is ensured. In addition, gold is replaced by the silver, the cost of the welding material is greatly reduced, and products can be well popularized.
Description
Technical field
The present invention relates to a kind of welding material and preparation method thereof.
Background technology
Welding procedure is one indispensable technique in electron trade, and in real life, a lot of products are not because the performance of itself goes wrong but eliminated by people because pad comes off.Improve solder technology, research and develop the cardinal task that high performance welding material becomes electronics corporation.Welding material is drawn materials wider, as zirconium, antimony, iron, lead etc.Because lead can be to environment, large to people's healthy harm, leady raw materials is replaced gradually.During welding material work, environment temperature is high, and pad will guarantee to weld smooth, can not affect the performance of electronic component, and people transfer to sight on the raw material of the costlinesses such as gold gradually.Although increase in performance, also greatly increased cost, do not meet inexpensive shopping principle.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of welding material and preparation method thereof.
For solving existing issue, the technical scheme that the present invention takes is: a kind of welding material, comprises the constituent of following content by mass percentage: antimony 15-20%, and zirconium 25-35%, silver-colored 10-20%, remaining is yttrium.
The preparation method of described a kind of welding material, comprises the following steps:
The first step, accurately takes above-mentioned antimony, zirconium, silver and four kinds of raw materials of yttrium, and is encapsulated in the quartz ampoule that vacuum is 4-5KPa, is being filled with helium;
Second step, drops into the above-mentioned raw material of handling well in reactor and carries out melting 18-24 hour for the first time, and temperature is 850-1020 ℃, after interval 10-24 hour, carries out melting for the second time, and melting duration is 10-15 hour, and temperature is 650-850 ℃;
The 3rd step, by the raw material ice quenching-in water after melting, then vacuum-pumping density be honored as a queen in baking oven 100-105 ° annealing in process 48-72 hour welding material.
Preferably: described smelting temperature is for the first time 950 ℃.
Preferably: described annealing in process is 60 hours.
Beneficial effect: prepare multicomponent alloy welding material because the present invention adopts antimony, zirconium, silver and yttrium, fusing point reaches 275-300 ℃ at 15-25 °, has substituted plumbous application in welding material with the angle of wetting of substrate on the good basis of guaranteed performance.In addition, silver has replaced gold to reduce widely the cost of welding material, and product can be promoted better.
The specific embodiment
Below by specific embodiment, the present invention is further described in detail.
Embodiment 1
A welding material, comprises the constituent of following content by mass percentage: antimony 15%, and zirconium 25%, silver 10%, remaining is yttrium.
The preparation method of described a kind of welding material, comprises the following steps:
The first step, accurately takes above-mentioned antimony, zirconium, silver and four kinds of raw materials of yttrium, and is encapsulated in the quartz ampoule that vacuum is 4KPa, is being filled with helium;
Second step, drops into the above-mentioned raw material of handling well in reactor and carries out melting for the first time 18 hours, and temperature is 850 ℃, and melting for the second time, after 10 hours, is carried out in interval, and melting duration is 10 hours, and temperature is 650 ℃;
The 3rd step, by the raw material ice quenching-in water after melting, then vacuum-pumping density is honored as a queen, and in baking oven, 100 ° of annealing in process 48 hours must welding material.
Embodiment 2
A welding material, comprises the constituent of following content by mass percentage: antimony 20%, and zirconium 35%, silver 20%, remaining is yttrium.
The preparation method of described a kind of welding material, comprises the following steps:
The first step, accurately takes above-mentioned antimony, zirconium, silver and four kinds of raw materials of yttrium, and is encapsulated in the quartz ampoule that vacuum is 5KPa, is being filled with helium;
Second step, drops into the above-mentioned raw material of handling well in reactor and carries out melting for the first time 24 hours, and temperature is 1020 ℃, and melting for the second time, after 24 hours, is carried out in interval, and melting duration is 15 hours, and temperature is 850 ℃;
The 3rd step, by the raw material ice quenching-in water after melting, then vacuum-pumping density is honored as a queen, and in baking oven, 105 ° of annealing in process 72 hours must welding material.
Embodiment 3
A welding material, comprises the constituent of following content by mass percentage: antimony 18%, and zirconium 30%, silver 15%, remaining is yttrium.
The preparation method of described a kind of welding material, comprises the following steps:
The first step, accurately takes above-mentioned antimony, zirconium, silver and four kinds of raw materials of yttrium, and is encapsulated in the quartz ampoule that vacuum is 4.2KPa, is being filled with helium;
Second step, drops into the above-mentioned raw material of handling well in reactor and carries out melting for the first time 20 hours, and temperature is 950 ℃, and melting for the second time, after 20 hours, is carried out in interval, and melting duration is 12 hours, and temperature is 700 ℃;
The 3rd step, by the raw material ice quenching-in water after melting, then vacuum-pumping density is honored as a queen, and in baking oven, 102 ° of annealing in process 60 hours must welding material.
Welding material of the present invention and conventional welding material, performance comparison result is as shown in the table.
Numeral from table is known, and welding material of the present invention can not only be applied in high-temperature soldering, and forms good wetting power between energy and substrate.
In addition, the invention is not restricted to above-mentioned embodiment, as long as within not exceeding scope of the present invention, can take variety of way to implement the present invention.
Claims (4)
1. a welding material, is characterized in that comprising the constituent of following content by mass percentage: antimony 15-20%, and zirconium 25-35%, silver-colored 10-20%, remaining is yttrium.
2. the preparation method of a kind of welding material claimed in claim 1, is characterized in that comprising the following steps:
The first step, accurately takes above-mentioned antimony, zirconium, silver and four kinds of raw materials of yttrium, and is encapsulated in the quartz ampoule that vacuum is 4-5KPa, is being filled with helium;
Second step, drops into the above-mentioned raw material of handling well in reactor and carries out melting 18-24 hour for the first time, and temperature is 850-1020 ℃, after interval 10-24 hour, carries out melting for the second time, and melting duration is 10-15 hour, and temperature is 650-850 ℃;
The 3rd step, by the raw material ice quenching-in water after melting, then vacuum-pumping density be honored as a queen in baking oven 100-105 ° annealing in process 48-72 hour welding material.
3. the preparation method of a kind of welding material according to claim 2, is characterized in that: described smelting temperature is for the first time 950 ℃.
4. the preparation method of a kind of welding material according to claim 2, is characterized in that: described annealing in process is 60 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310715276.3A CN103737194A (en) | 2013-12-23 | 2013-12-23 | Welding material and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310715276.3A CN103737194A (en) | 2013-12-23 | 2013-12-23 | Welding material and manufacturing method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103737194A true CN103737194A (en) | 2014-04-23 |
Family
ID=50494298
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310715276.3A Withdrawn CN103737194A (en) | 2013-12-23 | 2013-12-23 | Welding material and manufacturing method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103737194A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06182580A (en) * | 1992-12-15 | 1994-07-05 | Mitsubishi Materials Corp | Low alpha-ray pb alloy solder material and solder film |
| WO2001034860A1 (en) * | 1999-11-08 | 2001-05-17 | Euromat Gesellschaft Für Werkstofftechnologie Und Transfer Mbh | Soldering alloy |
| CN101234456A (en) * | 2008-02-27 | 2008-08-06 | 厦门大学 | Tin silver gold leadless welding material and preparation thereof |
| CN101618484A (en) * | 2008-07-02 | 2010-01-06 | 比亚迪股份有限公司 | Lead-free solder and preparation method thereof |
| JP4718369B2 (en) * | 2006-05-08 | 2011-07-06 | 本田技研工業株式会社 | Solder alloy |
-
2013
- 2013-12-23 CN CN201310715276.3A patent/CN103737194A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06182580A (en) * | 1992-12-15 | 1994-07-05 | Mitsubishi Materials Corp | Low alpha-ray pb alloy solder material and solder film |
| WO2001034860A1 (en) * | 1999-11-08 | 2001-05-17 | Euromat Gesellschaft Für Werkstofftechnologie Und Transfer Mbh | Soldering alloy |
| JP4718369B2 (en) * | 2006-05-08 | 2011-07-06 | 本田技研工業株式会社 | Solder alloy |
| CN101234456A (en) * | 2008-02-27 | 2008-08-06 | 厦门大学 | Tin silver gold leadless welding material and preparation thereof |
| CN101618484A (en) * | 2008-07-02 | 2010-01-06 | 比亚迪股份有限公司 | Lead-free solder and preparation method thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| C04 | Withdrawal of patent application after publication (patent law 2001) | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20140423 |