CN103710867A - High-hygroscopicity sound absorbing cotton and preparation method thereof - Google Patents

High-hygroscopicity sound absorbing cotton and preparation method thereof Download PDF

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Publication number
CN103710867A
CN103710867A CN201310601292.XA CN201310601292A CN103710867A CN 103710867 A CN103710867 A CN 103710867A CN 201310601292 A CN201310601292 A CN 201310601292A CN 103710867 A CN103710867 A CN 103710867A
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China
Prior art keywords
parts
powder
hygroscopicity
sound absorbing
back layer
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Pending
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CN201310601292.XA
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Chinese (zh)
Inventor
王黎明
孙益民
章云
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WUHU YUEFEI NEW ACOUSTIC MATERIAL CO Ltd
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WUHU YUEFEI NEW ACOUSTIC MATERIAL CO Ltd
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Priority to CN201310601292.XA priority Critical patent/CN103710867A/en
Publication of CN103710867A publication Critical patent/CN103710867A/en
Pending legal-status Critical Current

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  • Soundproofing, Sound Blocking, And Sound Damping (AREA)
  • Nonwoven Fabrics (AREA)

Abstract

The invention discloses high-hygroscopicity sound absorbing cotton and a preparation method thereof. The high-hygroscopicity sound absorbing cotton is composed of a top face layer, a back layer and a fiber cotton layer clamped between the top face layer and the back layer, the top face layer and the back layer are made of nonwoven cloth, and the high-hygroscopicity sound absorbing cotton is characterized in that the nonwoven cloth is formed by, by weight, 100 parts of isotactic polypropylene, 2-3 parts of polyethylene glycol, 1-2 parts of magnesium acetate, 1-2 parts of tetraethylammonium bromide, 3-4 parts of zinc borate, 8-10 parts of paraffin oil, 7-9 parts of dioctyl phthalate, 12-14 parts of reed, 2-3 parts of purslane, 3-4 parts of frost mulberry leaf, 2-3 parts of dandelion, 1-2 parts of moutan bark and 4-5 parts of auxiliary through a melt-blowing method. The high-hygroscopicity sound absorbing cotton prepared by the method has the advantages of good wet permeability and heat insulativity, high elasticity, corrosion resistance and the like.

Description

A kind of high-hygroscopicity acoustical cotton and preparation method thereof
 
Technical field
The present invention relates to Nonwovens In Technology, be specifically related to a kind of high-hygroscopicity acoustical cotton and preparation method thereof.
Background technology
Noise directly affects the raising of people's physical and mental health and quality of life, for a long time in noise circumstance, can cause that hearing loss even may bring out some diseases.Will be away from noise, what we can do is exactly sound-absorbing and sound insulation.Acoustical cotton, the high-frequency noises vibrational energy that produces in life can be converted to acoustical cotton inside fine count fiber kinetic energy and lead into heat energy and disappear, reach the function of absorbing sound and lowering noise.
Acoustical cotton can be superimposed with multi-layer nonwoven fabrics, or other material of arranging in pairs or groups, and makes sound-absorbing, acoustic material.Nonwoven fabric is that textile staple or long filament are carried out to orientation or random support row, forms fibre net structure, presents many tiny gaps, this gap can be regarded hole as, has adsorption function, therefore, acoustical cotton can be considered porous material, has good sound-absorbing, heat-insulation warm keeping performance.Acoustical cotton is widely used in the industries such as building, electrical equipment, automobile, machinery as a kind of gasket material, mainly play the effect of sound insulation.But all there is more deficiency in existing acoustical cotton product and manufacture method thereof, main manifestations is: not environmental protection of manufacture craft; Sound-absorbing effect is general; Chemical resistance is low, cannot meet Code in Hazardous Special Locations instructions for use; Temperature resistant grade is low; Do not carry out flame treatment; Product caking ability is inadequate, fugitive, tension intensity is poor; Outward appearance and flatness are inadequate, thickness relatively large deviation etc.
Summary of the invention
Object of the present invention is just to provide a kind of high-hygroscopicity acoustical cotton and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of high-hygroscopicity acoustical cotton, by top coat, back layer, and the cellucotton layer being clipped between top coat and back layer forms, described top coat, back layer adopt nonwoven cloth material, and the nonwoven fabric described in it is characterized in that is made by meltblown by the raw material of following weight portion: isotactic polypropylene 100, polyethylene glycol 2-3, magnesium acetate 1-2, tetraethylammonium bromide 1-2, Firebrake ZB 3-4, paraffin oil 8-10, dioctyl ester 7-9, reed rod 12-14, purslane 2-3, frosted mulberry leaf 3-4, dandelion 2-3, moutan bark 1-2, auxiliary agent 4-5.
Described auxiliary agent is made by following raw materials in part by weight: clay 10-12, nano-sized carbon 1-2, polytetrafluoroethylene powder 3-4, antioxidant NBC 1-2, isopropyl distearyl acyl-oxygen base Aluminate 2-3, zinc dialkyl dithiophosphate 2-3, magnetite 2-3, epoxidized soybean oil 35-40, n-propyl gallate 3-4, coix seed oil 2-3, vanadium diboride 1-2, Tea Polyphenols 2-3; Preparation method sends into clay, magnetite in calcining furnace and calcine 2-3 hour at 720-740 ℃, then, takes out, and sends in the hydrochloric acid solution of 10-15% and soaks 2-3 hour, filters, and obtains filter residue, with clear water, cleans, and dries, grinds to form 400-600 order powder; Gained powder mixes with other residual components, is heated to 60-70 ℃, and stirring reaction 40-50 minute is cooling, grinds to form slurry, obtains.
The preparation method of described a kind of high-hygroscopicity acoustical cotton, is characterized in that comprising the following steps:
(1), purslane, frosted mulberry leaf, dandelion, moutan bark are merged and pulverize 220-270 order powder, then, to the powder air blast of gained, it is seethed, to spray form paraffin oil in the powder seething, the two is fully mixed;
(2), reed rod is sent in retort, at 515-660 ℃, 3-4 hour is processed in charing, takes out, and is ground into powder;
(3), isotactic polypropylene is heated to molten condition, add step (1), (2) material, stir;
(4), in step (3) material, add other residual components, fully stir, mix, by nozzle, spray and thread make nonwoven fabric.
The present invention has following beneficial effect: the present invention adopts meltblown to prepare nonwoven fabric, have that technique is simple, raw material green cheap and easy to get, controllability good, production efficiency is high, and industrializing implementation is strong, can guarantee stable and reliable product quality, the acoustical cotton making has leads the advantages such as moist and warmth retention property is good, elasticity is large, corrosion-resistant.
The specific embodiment
Described a kind of high-hygroscopicity acoustical cotton, by top coat, back layer, and the cellucotton layer being clipped between top coat and back layer forms, described top coat, back layer adopt nonwoven cloth material, and the nonwoven fabric described in it is characterized in that is made by meltblown by the raw material of following weight portion: isotactic polypropylene 100, polyethylene glycol 3, magnesium acetate 2, tetraethylammonium bromide 1, Firebrake ZB 4, paraffin oil 9, dioctyl ester 8, reed rod 13, purslane 2, frosted mulberry leaf 4, dandelion 3, moutan bark 1, auxiliary agent 5.
Described auxiliary agent by following weight portion (kilogram) raw material makes: clay 10, nano-sized carbon 1, polytetrafluoroethylene powder 3, antioxidant NBC 1, isopropyl distearyl acyl-oxygen base Aluminate 2, zinc dialkyl dithiophosphate 2, magnetite 3, epoxidized soybean oil 35, n-propyl gallate 3, coix seed oil 2, vanadium diboride 1, Tea Polyphenols 3; Preparation method sends into clay, magnetite in calcining furnace and calcine 2-3 hour at 720-740 ℃, then, takes out, and sends in the hydrochloric acid solution of 10-15% and soaks 2-3 hour, filters, and obtains filter residue, with clear water, cleans, and dries, grinds to form 400-600 order powder; Gained powder mixes with other residual components, is heated to 60-70 ℃, and stirring reaction 40-50 minute is cooling, grinds to form slurry, obtains.
 
Preparation method comprises the following steps:
(1), purslane, frosted mulberry leaf, dandelion, moutan bark are merged and pulverize 220-270 order powder, then, to the powder air blast of gained, it is seethed, to spray form paraffin oil in the powder seething, the two is fully mixed;
(2), reed rod is sent in retort, at 515-660 ℃, 3-4 hour is processed in charing, takes out, and is ground into powder;
(3), isotactic polypropylene is heated to molten condition, add step (1), (2) material, stir;
(4), in step (3) material, add other residual components, fully stir, mix, by nozzle, spray and thread make nonwoven fabric.
 
After tested, the distribution of fiber diameters of resulting materials is 1.6-1.9 μ m, and tearing strength is 567N/m, and oxygen index (OI) is 33%-50%, and noise reduction coefficient is 0.813-0.867.

Claims (2)

1. a high-hygroscopicity acoustical cotton, by top coat, back layer, and the cellucotton layer being clipped between top coat and back layer forms, described top coat, back layer adopt nonwoven cloth material, and the nonwoven fabric described in it is characterized in that is made by meltblown by the raw material of following weight portion: isotactic polypropylene 100, polyethylene glycol 2-3, magnesium acetate 1-2, tetraethylammonium bromide 1-2, Firebrake ZB 3-4, paraffin oil 8-10, dioctyl ester 7-9, reed rod 12-14, purslane 2-3, frosted mulberry leaf 3-4, dandelion 2-3, moutan bark 1-2, auxiliary agent 4-5; Described auxiliary agent is made by following raw materials in part by weight: clay 10-12, nano-sized carbon 1-2, polytetrafluoroethylene powder 3-4, antioxidant NBC 1-2, isopropyl distearyl acyl-oxygen base Aluminate 2-3, zinc dialkyl dithiophosphate 2-3, magnetite 2-3, epoxidized soybean oil 35-40, n-propyl gallate 3-4, coix seed oil 2-3, vanadium diboride 1-2, Tea Polyphenols 2-3; Preparation method sends into clay, magnetite in calcining furnace and calcine 2-3 hour at 720-740 ℃, then, takes out, and sends in the hydrochloric acid solution of 10-15% and soaks 2-3 hour, filters, and obtains filter residue, with clear water, cleans, and dries, grinds to form 400-600 order powder; Gained powder mixes with other residual components, is heated to 60-70 ℃, and stirring reaction 40-50 minute is cooling, grinds to form slurry, obtains.
2. preparation method according to claim 1, is characterized in that comprising the following steps:
(1), purslane, frosted mulberry leaf, dandelion, moutan bark are merged and pulverize 220-270 order powder, then, to the powder air blast of gained, it is seethed, to spray form paraffin oil in the powder seething, the two is fully mixed;
(2), reed rod is sent in retort, at 515-660 ℃, 3-4 hour is processed in charing, takes out, and is ground into powder;
(3), isotactic polypropylene is heated to molten condition, add step (1), (2) material, stir;
(4), in step (3) material, add other residual components, fully stir, mix, by nozzle, spray and thread make nonwoven fabric.
CN201310601292.XA 2013-11-25 2013-11-25 High-hygroscopicity sound absorbing cotton and preparation method thereof Pending CN103710867A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103966767A (en) * 2014-04-23 2014-08-06 安徽依采妮纤维材料科技有限公司 Antibiosis deodorization sound absorption cotton and preparing method thereof
CN105220265A (en) * 2015-10-20 2016-01-06 湖州博润实业有限公司 A kind of new type natural fiber textile material and preparation method thereof

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CN101029433A (en) * 2007-03-06 2007-09-05 天津工业大学 Production and producer for functional modified microgranular melt-jetting non-woven cloth
CN101067228A (en) * 2007-06-12 2007-11-07 江苏盛虹化纤有限公司 Fiber capable of slowly releasing health care traditional Chinese medicine and fabric thereof
CN102100417A (en) * 2009-12-21 2011-06-22 胡敬军 N95 type negative ion mask
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CN102965847A (en) * 2012-11-22 2013-03-13 芜湖跃飞新型吸音材料股份有限公司 PET (polyethylene glycol terephthalate) fiber/polyacrylonitrile fiber composite sound absorbing cotton and preparation method of PET fiber/polyacrylonitrile fiber composite sound absorbing cotton
CN102965845A (en) * 2012-11-22 2013-03-13 芜湖跃飞新型吸音材料股份有限公司 PET (polyethylene glycol terephthalate) fiber/aluminum silicate fiber composite sound absorbing cotton and preparation method of PET fiber/aluminum silicate fiber composite sound absorbing cotton
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Publication number Priority date Publication date Assignee Title
CN101029433A (en) * 2007-03-06 2007-09-05 天津工业大学 Production and producer for functional modified microgranular melt-jetting non-woven cloth
CN101067228A (en) * 2007-06-12 2007-11-07 江苏盛虹化纤有限公司 Fiber capable of slowly releasing health care traditional Chinese medicine and fabric thereof
CN102100417A (en) * 2009-12-21 2011-06-22 胡敬军 N95 type negative ion mask
CN102836594A (en) * 2012-08-30 2012-12-26 上海兴诺康纶纤维科技股份有限公司 Antibacterial polypropylene melt-blow non-woven filter material and preparation method thereof
CN102965847A (en) * 2012-11-22 2013-03-13 芜湖跃飞新型吸音材料股份有限公司 PET (polyethylene glycol terephthalate) fiber/polyacrylonitrile fiber composite sound absorbing cotton and preparation method of PET fiber/polyacrylonitrile fiber composite sound absorbing cotton
CN102965845A (en) * 2012-11-22 2013-03-13 芜湖跃飞新型吸音材料股份有限公司 PET (polyethylene glycol terephthalate) fiber/aluminum silicate fiber composite sound absorbing cotton and preparation method of PET fiber/aluminum silicate fiber composite sound absorbing cotton
CN102965839A (en) * 2012-11-22 2013-03-13 芜湖跃飞新型吸音材料股份有限公司 PET (polyethylene glycol terephthalate) fiber/aramid fiber composite sound absorbing cotton and preparation method of PET fiber/aramid fiber composite sound absorbing cotton

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103966767A (en) * 2014-04-23 2014-08-06 安徽依采妮纤维材料科技有限公司 Antibiosis deodorization sound absorption cotton and preparing method thereof
CN105220265A (en) * 2015-10-20 2016-01-06 湖州博润实业有限公司 A kind of new type natural fiber textile material and preparation method thereof

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