CN103697920B - A kind of optical fiber sensor head and based on this sensing head measure the optical fiber sensing system of liquid refractivity and method - Google Patents
A kind of optical fiber sensor head and based on this sensing head measure the optical fiber sensing system of liquid refractivity and method Download PDFInfo
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Abstract
一种光纤传感头和基于该传感头的测量液体折射率的光纤传感系统及方法,属于光纤传感系统领域。它是为了解决现有光纤传感头FP腔距光纤尾端的距离较近,进而对反射率产生影响的问题。本发明所述的一种光纤传感头和基于该传感头的测量液体折射率的光纤传感系统及方法,克服了现有技术中,通过在光纤上开一空气通道,改变了光路的方向,从而将光纤包层作为FP腔,避免了待测液体同时对FP腔的两个界面反射率的影响。当入射到传感头中的光处于S偏振时,测量折射率的最大灵敏度达‑298.3dB/RIU,处于P偏振时,测量折射率的最大灵敏度达‑597.1dB/RIU。本发明适用于对液体的折射率进行测量。
An optical fiber sensing head and an optical fiber sensing system and method for measuring liquid refractive index based on the sensing head belong to the field of optical fiber sensing systems. The purpose of the invention is to solve the problem that the distance between the FP cavity of the existing optical fiber sensing head and the end of the optical fiber is relatively short, thereby affecting the reflectivity. An optical fiber sensing head and an optical fiber sensing system and method based on the sensing head for measuring the refractive index of a liquid described in the present invention overcome the problem of changing the optical path by opening an air channel on the optical fiber in the prior art. direction, so that the fiber cladding is used as an FP cavity, which avoids the influence of the liquid to be measured on the reflectivity of the two interfaces of the FP cavity at the same time. When the light incident into the sensor head is at S-polarization, the maximum sensitivity for measuring the refractive index reaches ‑298.3dB/RIU, and when it is at P-polarization, the maximum sensitivity for measuring the refractive index reaches ‑597.1dB/RIU. The invention is suitable for measuring the refractive index of liquid.
Description
技术领域technical field
本发明属于光纤传感系统领域。The invention belongs to the field of optical fiber sensing system.
背景技术Background technique
由于光纤的低成本、抗腐蚀、高敏感等优良特性,近年来光纤在折射率传感方面得到很大的关注并广泛运用到了生物、化学等领域。光纤折射率传感器按探测光谱主要可分为两类,透射型光纤传感器和反射型光纤传感器。相对于反射型光纤传感器,透射型光纤传感器的传感系统所占空间相对较大,限制了其在生物体内进行直接的折射率探测。对于反射型光纤传感器,通常使用光纤结合着光纤外部Fabry-Perot(FP)腔或光纤内部FP腔来探测折射率的变化;而外部FP腔,同样面临着传感头所占空间相对较大的问题。因而相较而言,基于光纤内部FP腔的传感器在折射率的传感应用方面范围更广。然而传统的基于内部FP腔的光纤传感器尽管尺寸小,距离大,由于FP腔距光纤尾端的距离较近,当测试液体时,液体除了对FP反射面的反射率产生影响外,且对光纤尾端的反射率产生影响,两者影响会发生交叉传感,从而导致光谱仪测得的反射光强对于待测液体折射率无法呈单调变化,只能在很窄的一段折射率范围内呈现单调变化,并且单调区域随着待测液体折射率的变化而发生变化。因而大大限制了基于内部FP腔的光纤传感器在折射率测量方面的应用。Due to the low cost, corrosion resistance, high sensitivity and other excellent characteristics of optical fiber, in recent years, optical fiber has received great attention in refractive index sensing and has been widely used in biology, chemistry and other fields. Optical fiber refractive index sensors can be mainly divided into two types according to the detection spectrum, transmission optical fiber sensors and reflective optical fiber sensors. Compared with reflective optical fiber sensors, the sensing system of transmissive optical fiber sensors occupies a relatively large space, which limits its direct detection of refractive index in vivo. For reflective fiber optic sensors, the optical fiber is usually combined with an external Fabry-Perot (FP) cavity or an internal FP cavity to detect changes in the refractive index; and the external FP cavity also faces the relatively large space occupied by the sensor head. question. Therefore, in comparison, the sensor based on the FP cavity inside the optical fiber has a wider range of sensing applications for the refractive index. However, although the traditional optical fiber sensor based on the internal FP cavity has a small size and a large distance, due to the short distance between the FP cavity and the end of the optical fiber, when testing liquid, the liquid not only affects the reflectivity of the FP reflective surface, but also affects the optical fiber end. Influenced by the reflectivity of the terminal, cross-sensing will occur between the two influences, so that the reflected light intensity measured by the spectrometer cannot monotonically change with respect to the refractive index of the liquid to be measured, but can only present a monotonous change within a narrow range of refractive index. And the monotonic region changes with the change of the refractive index of the liquid to be measured. Therefore, the application of fiber optic sensors based on internal FP cavity in refractive index measurement is greatly limited.
发明内容Contents of the invention
本发明是为了解决现有光纤传感头FP腔距光纤尾端的距离较近,进而对反射率产生影响的问题,现提供一种光纤传感头和基于该传感头的测量液体折射率的光纤传感系统及方法。The present invention aims to solve the problem that the distance between the FP cavity of the existing optical fiber sensing head and the end of the optical fiber is relatively short, thereby affecting the reflectivity. Now, an optical fiber sensing head and a method for measuring the refractive index of liquid based on the sensing head are provided. Optical fiber sensing system and method.
一种光纤传感头,它包括:光纤和反射材料;An optical fiber sensing head, comprising: an optical fiber and a reflective material;
所述光纤包括:光纤包层和光纤纤芯;The optical fiber includes: an optical fiber cladding and an optical fiber core;
光纤包层包裹在光纤纤芯的外侧;在光纤纤芯上开有四棱柱形的空气通道,该空气通道的截面为等腰梯形,且该等腰梯形的腰所在平面与光纤轴的夹角为45度,该等腰梯形的高等于光纤纤芯的直径,该等腰梯形的短底边的长度范围在10μm至20μm之间,空气通道的长度等于光纤的直径,该等腰梯形的短底边所对应的光纤包层外侧固定有反射材料;The fiber cladding is wrapped on the outside of the fiber core; there is a quadrangular air channel on the fiber core, the cross section of the air channel is an isosceles trapezoid, and the angle between the plane where the waist of the isosceles trapezoid is located and the fiber axis is is 45 degrees, the height of the isosceles trapezoid is equal to the diameter of the fiber core, the length of the short base of the isosceles trapezoid is between 10 μm and 20 μm, the length of the air channel is equal to the diameter of the optical fiber, the short of the isosceles trapezoid A reflective material is fixed on the outside of the fiber cladding corresponding to the bottom edge;
所述反射材料的材料与光纤纤芯的材料相同。The material of the reflective material is the same as that of the fiber core.
一种测量液体折射率的光纤传感系统,它包括:光源、3dB耦合器、偏振器、传感头、光谱仪和信号处理模块;An optical fiber sensing system for measuring the refractive index of liquid, which includes: a light source, a 3dB coupler, a polarizer, a sensing head, a spectrometer and a signal processing module;
光源发出的光经3dB耦合器传输至偏振器中,偏振器经该光进行调节并传输至传感头中,传感头将该光反射到偏振器中,偏振器将传感头反射的光传输至3dB耦合器中,3dB耦合器将该光传输至光谱仪中,光谱仪的光谱信号输出端连接信号处理模块的光谱信号输入端;The light emitted by the light source is transmitted to the polarizer through the 3dB coupler. The polarizer is adjusted by the light and transmitted to the sensor head. The sensor head reflects the light into the polarizer. Transmission to the 3dB coupler, the 3dB coupler transmits the light to the spectrometer, and the spectral signal output end of the spectrometer is connected to the spectral signal input end of the signal processing module;
所述信号处理模块包括以下单元:The signal processing module includes the following units:
采集光谱仪中获得的反射谱在1550nm处的反射谱强度的单元;A unit for collecting the intensity of the reflection spectrum obtained in the spectrometer at 1550nm;
获得空气通道与光纤纤芯接触面的反射率R的单元;A unit for obtaining the reflectivity R of the interface between the air channel and the fiber core;
获得待测液体的折射率n2的单元;Obtain the unit of the refractive index n of the liquid to be measured ;
所述传感头包括:光纤和反射材料;The sensing head includes: optical fiber and reflective material;
所述光纤包括:光纤包层和光纤纤芯;The optical fiber includes: an optical fiber cladding and an optical fiber core;
光纤包层包裹在光纤纤芯的外侧;在光纤纤芯上开有四棱柱形的空气通道,该空气通道的截面为等腰梯形,且该等腰梯形的腰所在平面与光纤轴的夹角为45度,该等腰梯形的高等于光纤纤芯的直径,该等腰梯形的短底边的长度范围在10μm至20μm之间,空气通道的长度等于光纤的直径,该等腰梯形的短底边所对应的光纤包层外侧设有反射材料。The fiber cladding is wrapped on the outside of the fiber core; there is a quadrangular air channel on the fiber core, the cross section of the air channel is an isosceles trapezoid, and the angle between the plane where the waist of the isosceles trapezoid is located and the fiber axis is is 45 degrees, the height of the isosceles trapezoid is equal to the diameter of the fiber core, the length of the short base of the isosceles trapezoid is between 10 μm and 20 μm, the length of the air channel is equal to the diameter of the optical fiber, the short of the isosceles trapezoid The outer side of the optical fiber cladding corresponding to the bottom edge is provided with a reflective material.
一种测量液体折射率的方法,该方法是基于下述装置实现的,A method for measuring the refractive index of a liquid, the method is realized based on the following device,
所述装置包括:光源、3dB耦合器、偏振器、传感头和光谱仪;The device includes: a light source, a 3dB coupler, a polarizer, a sensor head and a spectrometer;
光源发出的光经3dB耦合器传输至偏振器中,偏振器经该光进行调节并传输至传感头中,传感头将该光反射到偏振器中,偏振器将传感头反射的光传输至3dB耦合器中,3dB耦合器将该光传输至光谱仪中;The light emitted by the light source is transmitted to the polarizer through the 3dB coupler. The polarizer is adjusted by the light and transmitted to the sensor head. The sensor head reflects the light into the polarizer. Transmission to the 3dB coupler, the 3dB coupler transmits the light to the spectrometer;
所述传感头包括:光纤和反射材料;The sensing head includes: optical fiber and reflective material;
所述光纤包括:光纤包层和光纤纤芯;The optical fiber includes: an optical fiber cladding and an optical fiber core;
光纤包层包裹在光纤纤芯的外侧;在光纤纤芯上开有四棱柱形的空气通道,该空气通道的截面为等腰梯形,且该等腰梯形的腰所在平面与光纤轴的夹角为45度,该等腰梯形的高等于光纤纤芯的直径,该等腰梯形的短底边的长度范围在10μm至20μm之间,空气通道的长度等于光纤的直径,该等腰梯形的短底边所对应的光纤包层外侧设有反射材料;The fiber cladding is wrapped on the outside of the fiber core; there is a quadrangular air channel on the fiber core, the cross section of the air channel is an isosceles trapezoid, and the angle between the plane where the waist of the isosceles trapezoid is located and the fiber axis is is 45 degrees, the height of the isosceles trapezoid is equal to the diameter of the fiber core, the length of the short base of the isosceles trapezoid is between 10 μm and 20 μm, the length of the air channel is equal to the diameter of the optical fiber, the short of the isosceles trapezoid A reflective material is provided on the outside of the fiber cladding corresponding to the bottom edge;
基于上述装置的一种测量液体折射率的方法包括以下步骤:A method for measuring the refractive index of liquid based on the above-mentioned device comprises the following steps:
步骤一:调节偏振器,使入射到传感头中的光为一种偏振态下的光;然后执行步骤二;Step 1: Adjust the polarizer so that the light incident on the sensor head is light in one polarization state; then perform step 2;
步骤二:保持传感头不浸入液体中,利用光谱仪获得反射谱在1550nm处的反射谱强度基准值I0,然后执行步骤三;Step 2: keep the sensing head not immersed in the liquid, use a spectrometer to obtain the reference value I 0 of the reflection spectrum intensity at 1550nm, and then perform step 3;
步骤三:将传感头浸入待测液体中,使待测液体进入空气通道,利用光谱仪获得反射谱在1550nm处的反射谱强度值I1,然后执行步骤四;Step 3: Immerse the sensor head in the liquid to be tested, let the liquid to be tested enter the air channel, use a spectrometer to obtain the reflection spectrum intensity value I 1 at 1550nm, and then perform step 4;
步骤四:利用反射谱强度基准值I0和反射谱强度值I1,获得充有待测液体的空气通道与光纤纤芯接触面的反射率R,然后执行步骤五;Step 4: Using the reflection spectrum intensity reference value I 0 and the reflection spectrum intensity value I 1 to obtain the reflectivity R of the contact surface between the air channel filled with the liquid to be measured and the fiber core of the optical fiber, and then perform step 5;
步骤五:利用充有待测液体的空气通道与光纤纤芯接触面的反射率R,获得待测液体的折射率n2。Step 5: Obtain the refractive index n 2 of the liquid to be measured by using the reflectivity R of the contact surface between the air channel filled with the liquid to be measured and the fiber core of the optical fiber.
本发明所述的一种光纤传感头和基于该传感头的测量液体折射率的光纤传感系统及方法,克服了现有技术中,采用现有光纤传感头在光纤外部设置FP腔的固有思路,而是通过在光纤上开一空气通道,改变了光路的方向,从而将光纤包层作为FP腔,避免了待测液体同时对FP腔的两个界面反射率的影响。当入射到传感头中的光处于S偏振时,测量折射率的最大灵敏度能高达-298.3dB/RIU,处于P偏振时,测量折射率的最大灵敏度能高达-597.1dB/RIU。An optical fiber sensing head of the present invention and an optical fiber sensing system and method based on the sensing head for measuring the refractive index of a liquid overcome the problem of using an existing optical fiber sensing head to set an FP cavity outside the optical fiber in the prior art Instead, by opening an air channel on the optical fiber, the direction of the optical path is changed, so that the optical fiber cladding is used as the FP cavity, which avoids the influence of the liquid to be measured on the reflectivity of the two interfaces of the FP cavity at the same time. When the light incident into the sensor head is at S polarization, the maximum sensitivity for measuring the refractive index can be as high as -298.3dB/RIU, and when it is at P polarization, the maximum sensitivity for measuring the refractive index can be as high as -597.1dB/RIU.
本发明所述的一种光纤传感头和基于该传感头的测量液体折射率的光纤传感系统及方法,适用于对液体的折射率进行测量。The optical fiber sensing head and the optical fiber sensing system and method for measuring the refractive index of liquid based on the sensing head described in the present invention are suitable for measuring the refractive index of liquid.
附图说明Description of drawings
图1为一种光纤传感头的剖面结构示意图;Fig. 1 is a schematic cross-sectional structure diagram of an optical fiber sensing head;
图2为一种测量液体折射率的光纤传感系统的原理示意图;Fig. 2 is a schematic diagram of the principle of an optical fiber sensing system for measuring the refractive index of a liquid;
图3为一种测量液体折射率的光纤传感方法的流程图;Fig. 3 is a flow chart of an optical fiber sensing method for measuring liquid refractive index;
图4为S偏振时传感头反射谱对于折射率的光谱变化图;Fig. 4 is the spectral change diagram of the reflection spectrum of the sensor head for the refractive index during S polarization;
图5为P偏振时传感头反射谱对于折射率的光谱变化图。Fig. 5 is a graph showing the spectral change of the reflectance spectrum of the sensing head with respect to the refractive index in the case of P polarization.
具体实施方式detailed description
具体实施方式一:参照图1具体说明本实施方式,本实施方式所述的一种光纤传感头,它包括:光纤和反射材料4-3;Specific embodiment 1: This embodiment is described in detail with reference to FIG. 1. An optical fiber sensing head described in this embodiment includes: an optical fiber and a reflective material 4-3;
所述光纤包括:光纤包层4-1和光纤纤芯4-2;The optical fiber includes: an optical fiber cladding 4-1 and an optical fiber core 4-2;
光纤包层4-1包裹在光纤纤芯4-2的外侧;在光纤纤芯4-2上开有四棱柱形的空气通道4-4,该空气通道4-5的截面为等腰梯形,且该等腰梯形的腰所在平面与光纤轴的夹角为45度,该等腰梯形的高等于光纤纤芯4-2的直径,该等腰梯形的短底边的长度范围在10μm至20μm之间,空气通道4-5的长度等于光纤的直径,该等腰梯形的短底边所对应的光纤包层4-1外侧固定有反射材料4-3。The optical fiber cladding 4-1 is wrapped on the outside of the optical fiber core 4-2; a quadrangular prism-shaped air channel 4-4 is opened on the optical fiber core 4-2, and the cross section of the air channel 4-5 is isosceles trapezoidal, And the angle between the plane where the waist of the isosceles trapezoid is located and the fiber axis is 45 degrees, the height of the isosceles trapezoid is equal to the diameter of the fiber core 4-2, and the length of the short base of the isosceles trapezoid is in the range of 10 μm to 20 μm Between, the length of the air channel 4-5 is equal to the diameter of the optical fiber, and the outside of the optical fiber cladding 4-1 corresponding to the short base of the isosceles trapezoid is fixed with a reflective material 4-3.
具体实施方式二:本实施方式是对具体实施方式一所述的一种光纤传感头作进一步说明,本实施方式中,所述光纤为单模光纤。Embodiment 2: This embodiment further describes the optical fiber sensing head described in Embodiment 1. In this embodiment, the optical fiber is a single-mode optical fiber.
具体实施方式三:本实施方式是对具体实施方式一所述的一种光纤传感头作进一步说明,本实施方式中,所述光纤为多模光纤。Embodiment 3: This embodiment further describes the optical fiber sensing head described in Embodiment 1. In this embodiment, the optical fiber is a multimode optical fiber.
具体实施方式四:本实施方式是对具体实施方式一所述的一种光纤传感头作进一步说明,本实施方式中,所述反射材料4-3的材料与光纤纤芯4-2的材料相同。Embodiment 4: This embodiment is a further description of the optical fiber sensing head described in Embodiment 1. In this embodiment, the material of the reflective material 4-3 and the material of the optical fiber core 4-2 same.
具体实施方式五:参照图2具体说明本实施方式,本实施方式所述的一种测量液体折射率的光纤传感系统,它包括:光源1、3dB耦合器2、偏振器3、传感头4、光谱仪5和信号处理模块6;Specific embodiment five: this embodiment is described in detail with reference to Fig. 2, a kind of optical fiber sensing system for measuring liquid refractive index described in this embodiment, it comprises: light source 1, 3dB coupler 2, polarizer 3, sensing head 4. Spectrometer 5 and signal processing module 6;
光源1发出的光经3dB耦合器2传输至偏振器3中,偏振器3经该光进行调节并传输至传感头4中,传感头4将该光反射到偏振器3中,偏振器3将传感头4反射的光传输至3dB耦合器2中,3dB耦合器2将该光传输至光谱仪5中,光谱仪5的光谱信号输出端连接信号处理模块6的光谱信号输入端;The light emitted by the light source 1 is transmitted to the polarizer 3 through the 3dB coupler 2, the polarizer 3 is adjusted by the light and transmitted to the sensor head 4, the sensor head 4 reflects the light to the polarizer 3, and the polarizer 3 transmit the light reflected by the sensor head 4 to the 3dB coupler 2, and the 3dB coupler 2 transmits the light to the spectrometer 5, and the spectral signal output end of the spectrometer 5 is connected to the spectral signal input end of the signal processing module 6;
所述信号处理模块6包括以下单元:The signal processing module 6 includes the following units:
采集光谱仪5中获得的反射谱在1550nm处的反射谱强度的单元;A unit for collecting the reflectance spectrum intensity at 1550nm of the reflectance spectrum obtained in the spectrometer 5;
获得空气通道4-5与光纤纤芯4-2接触面的反射率R的单元;A unit for obtaining the reflectivity R of the interface between the air channel 4-5 and the optical fiber core 4-2;
获得待测液体的折射率n2的单元;Obtain the unit of the refractive index n of the liquid to be measured ;
所述传感头4包括:光纤和反射材料4-3;The sensing head 4 includes: an optical fiber and a reflective material 4-3;
所述光纤包括:光纤包层4-1和光纤纤芯4-2;The optical fiber includes: an optical fiber cladding 4-1 and an optical fiber core 4-2;
光纤包层4-1包裹在光纤纤芯4-2的外侧;在光纤纤芯4-2上开有四棱柱形的空气通道4-4,该空气通道4-5的截面为等腰梯形,且该等腰梯形的腰所在平面与光纤轴的夹角为45度,该等腰梯形的高等于光纤纤芯4-2的直径,该等腰梯形的短底边的长度范围在10μm至20μm之间,空气通道4-5的长度等于光纤的直径,该等腰梯形的短底边所对应的光纤包层4-1外侧设有反射材料4-3。The optical fiber cladding 4-1 is wrapped on the outside of the optical fiber core 4-2; a quadrangular prism-shaped air channel 4-4 is opened on the optical fiber core 4-2, and the cross section of the air channel 4-5 is isosceles trapezoidal, And the angle between the plane where the waist of the isosceles trapezoid is located and the fiber axis is 45 degrees, the height of the isosceles trapezoid is equal to the diameter of the fiber core 4-2, and the length of the short base of the isosceles trapezoid is in the range of 10 μm to 20 μm Between, the length of the air channel 4-5 is equal to the diameter of the optical fiber, and the outer side of the optical fiber cladding 4-1 corresponding to the short base of the isosceles trapezoid is provided with a reflective material 4-3.
具体实施方式六:本实施方式是对具体实施方式五所述的一种测量液体折射率的光纤传感系统作进一步说明,本实施方式中,所述光源1为高斯光源。Embodiment 6: This embodiment is a further description of the optical fiber sensing system for measuring the refractive index of liquid described in Embodiment 5. In this embodiment, the light source 1 is a Gaussian light source.
具体实施方式七:参照图3具体说明本实施方式,本实施方式所述的一种测量液体折射率的方法,该方法是基于下述装置实现的,Embodiment 7: This embodiment is specifically described with reference to FIG. 3 , a method for measuring the refractive index of a liquid described in this embodiment, which is implemented based on the following device,
所述装置包括:光源1、3dB耦合器2、偏振器3、传感头4和光谱仪5;The device includes: a light source 1, a 3dB coupler 2, a polarizer 3, a sensing head 4 and a spectrometer 5;
光源1发出的光经3dB耦合器2传输至偏振器3中,偏振器3经该光进行调节并传输至传感头4中,传感头4将该光反射到偏振器3中,偏振器3将传感头4反射的光传输至3dB耦合器2中,3dB耦合器2将该光传输至光谱仪5中;The light emitted by the light source 1 is transmitted to the polarizer 3 through the 3dB coupler 2, the polarizer 3 is adjusted by the light and transmitted to the sensor head 4, the sensor head 4 reflects the light to the polarizer 3, and the polarizer 3 transmit the light reflected by the sensor head 4 to the 3dB coupler 2, and the 3dB coupler 2 transmits the light to the spectrometer 5;
所述传感头4包括:光纤和反射材料4-3;The sensing head 4 includes: an optical fiber and a reflective material 4-3;
所述光纤包括:光纤包层4-1和光纤纤芯4-2;The optical fiber includes: an optical fiber cladding 4-1 and an optical fiber core 4-2;
光纤包层4-1包裹在光纤纤芯4-2的外侧;在光纤纤芯4-2上开有四棱柱形的空气通道4-4,该空气通道4-5的截面为等腰梯形,且该等腰梯形的腰所在平面与光纤轴的夹角为45度,该等腰梯形的高等于光纤纤芯4-2的直径,该等腰梯形的短底边的长度范围在10μm至20μm之间,空气通道4-5的长度等于光纤的直径,该等腰梯形的短底边所对应的光纤包层4-1外侧设有反射材料4-3;The optical fiber cladding 4-1 is wrapped on the outside of the optical fiber core 4-2; a quadrangular prism-shaped air channel 4-4 is opened on the optical fiber core 4-2, and the cross section of the air channel 4-5 is isosceles trapezoidal, And the angle between the plane where the waist of the isosceles trapezoid is located and the fiber axis is 45 degrees, the height of the isosceles trapezoid is equal to the diameter of the fiber core 4-2, and the length of the short base of the isosceles trapezoid is in the range of 10 μm to 20 μm Between, the length of the air channel 4-5 is equal to the diameter of the optical fiber, and the outer side of the optical fiber cladding 4-1 corresponding to the short base of the isosceles trapezoid is provided with a reflective material 4-3;
基于上述装置的一种测量液体折射率的方法包括以下步骤:A method for measuring the refractive index of liquid based on the above-mentioned device comprises the following steps:
步骤一:调节偏振器3,使入射到传感头4中的光为一种偏振态下的光;然后执行步骤二;Step 1: adjust the polarizer 3 so that the light incident on the sensor head 4 is light in one polarization state; then perform step 2;
步骤二:保持传感头4不浸入液体中,利用光谱仪5获得反射谱在1550nm处的反射谱强度基准值I0,然后执行步骤三;Step 2: keep the sensing head 4 not immersed in the liquid, use the spectrometer 5 to obtain the reference value I 0 of the reflection spectrum intensity at 1550nm, and then perform step 3;
步骤三:将传感头4浸入待测液体中,使待测液体进入空气通道(4-5),利用光谱仪5获得反射谱在1550nm处的反射谱强度值I1,然后执行步骤四;Step 3: Immerse the sensor head 4 in the liquid to be tested, make the liquid to be tested enter the air channel (4-5), use the spectrometer 5 to obtain the reflection spectrum intensity value I 1 of the reflection spectrum at 1550nm, and then perform step 4;
步骤四:利用反射谱强度基准值I0和反射谱强度值I1,获得空气通道4-5与光纤纤芯4-2接触面的反射率R,然后执行步骤五;Step 4: Using the reflection spectrum intensity reference value I 0 and the reflection spectrum intensity value I 1 to obtain the reflectance R of the contact surface between the air channel 4-5 and the optical fiber core 4-2, and then perform step 5;
步骤五:利用充有待测液体的空气通道4-5与光纤纤芯4-2接触面的反射率R,获得待测液体的折射率n2。Step 5: Obtain the refractive index n 2 of the liquid to be measured by using the reflectivity R of the interface between the air channel 4-5 filled with the liquid to be measured and the optical fiber core 4-2.
具体实施方式八:本实施方式是对具体实施方式七所述的一种测量液体折射率的方法作进一步说明,本实施方式中,根据如下公式获得充有待测液体的空气通道4-5与光纤纤芯4-2接触面的反射率R,Embodiment 8: This embodiment is a further description of a method for measuring the refractive index of liquid described in Embodiment 7. In this embodiment, the air channel 4-5 filled with the liquid to be measured is obtained according to the following formula: The reflectivity R of the contact surface of the fiber core 4-2,
lg(I1/I0)=lg(R)。lg(I 1 /I 0 )=lg(R).
具体实施方式九:本实施方式是对具体实施方式七所述的一种测量液体折射率的方法作进一步说明,本实施方式中,步骤一中调节偏振器3,使入射到传感头4中的光为S偏振时,根据如下公式获得待测液体的折射率n2,Specific Embodiment Nine: This embodiment is a further description of a method for measuring the refractive index of a liquid described in Embodiment 7. In this embodiment, the polarizer 3 is adjusted in step 1 so that the incident When the light is S-polarized, the refractive index n 2 of the liquid to be measured is obtained according to the following formula,
其中,n1为光纤纤芯4-2的折射率,θ1为入射到传感头4中的光与空气通道4-5与光纤纤芯4-2接触面所在平面的夹角,θ2为入射到传感头4中的光在空气通道4-5与光纤纤芯4-2接触面上发生折射时的折射角。Wherein, n 1 is the refractive index of the optical fiber core 4-2, θ 1 is the angle between the light incident in the sensing head 4 and the plane where the air channel 4-5 and the contact surface of the optical fiber core 4-2 are located, θ 2 is the refraction angle when the light incident on the sensor head 4 is refracted on the interface between the air channel 4-5 and the fiber core 4-2.
具体实施方式十:本实施方式是对具体实施方式七所述的一种测量液体折射率的方法作进一步说明,本实施方式中,步骤一中调节偏振器3,使入射到传感头4中的光为P偏振时,根据如下公式获得待测液体的折射率n2,Embodiment 10: This embodiment is a further description of a method for measuring the refractive index of a liquid described in Embodiment 7. In this embodiment, the polarizer 3 is adjusted in step 1 so that the incident light into the sensor head 4 When the light is P-polarized, the refractive index n 2 of the liquid to be measured is obtained according to the following formula,
其中,n1为光纤纤芯4-2的折射率,θ1为入射到传感头4中的光与空气通道4-5与光纤纤芯4-2接触面所在平面的夹角,θ2为入射到传感头4中的光在空气通道4-5与光纤纤芯4-2接触面上发生折射时的折射角。Wherein, n 1 is the refractive index of the optical fiber core 4-2, θ 1 is the angle between the light incident in the sensing head 4 and the plane where the air channel 4-5 and the contact surface of the optical fiber core 4-2 are located, θ 2 is the refraction angle when the light incident on the sensor head 4 is refracted on the interface between the air channel 4-5 and the fiber core 4-2.
光纤包层4-1从功能上可以被视为Fabry-Perot(FP)腔,信号光会在FP腔中不断的反射,由于光束在FP腔上两面的反射率相等且较低,因而该传感探头的反射谱可以直接简单的用双光束干涉表示。即:The fiber cladding 4-1 can be regarded as a Fabry-Perot (FP) cavity in function, and the signal light will be continuously reflected in the FP cavity. Since the reflectivity of the light beam on both sides of the FP cavity is equal and low, the transmission The reflection spectrum of the sensing probe can be expressed directly and simply by two-beam interference. which is:
其中,R为空气通道4-5斜面的反射率;I1为FP腔一个反射面上反射光的光强,I2为FP腔另一个反射面上反射光的光强;λ为光源1发出的光的光强,n3为光纤包层4-1的折射率;L为FP腔的腔长,即为光纤包层4-1的厚度,为初始相位。Among them, R is the reflectivity of the slope of the air channel 4-5; I 1 is the light intensity of the reflected light on one reflective surface of the FP cavity, and I 2 is the light intensity of the reflected light on the other reflective surface of the FP cavity; λ is the light emitted by the light source 1 The light intensity of the light, n 3 is the refractive index of the fiber cladding 4-1; L is the cavity length of the FP cavity, which is the thickness of the fiber cladding 4-1, is the initial phase.
设定入射光为高斯光源,带宽为200nm,光谱范围为1200nm到1600nm,中心波长为1500nm,待测液体折射率选定普遍常用的1.33(水)-1.44,调节偏振器,让信号光处于S偏振时,从所测得的反射谱中提取通信窗口1550nm的数据结果,处理后得到的测量结果如图4所示,随着折射率不断增大,越来越接近纤芯折射率,透射光不断增大,反射光不断减小,呈单调变化。传感头的折射率灵敏度最少为-73.6dB/RIU,最大灵敏度能高达-298.3dB/RIU,完全有能力进行折射率传感。Set the incident light as a Gaussian light source, with a bandwidth of 200nm, a spectral range of 1200nm to 1600nm, and a central wavelength of 1500nm. The refractive index of the liquid to be measured is generally 1.33 (water)-1.44, and the polarizer is adjusted so that the signal light is at S In the case of polarization, the data results of the communication window 1550nm were extracted from the measured reflection spectrum, and the measured results after processing are shown in Figure 4. increasing, the reflected light decreases, showing a monotonous change. The refractive index sensitivity of the sensor head is at least -73.6dB/RIU, and the maximum sensitivity can be as high as -298.3dB/RIU, which is fully capable of refractive index sensing.
同理,调节偏振器,让信号光处于P偏振时,其他参数设置相同,得到的测量结果如图5所示,随着折射率不断增大,越来越接近纤芯折射率,反射光不断减小,呈单调变化。并且,通过计算发现,该传感头的折射率灵敏度最少为-148.0dB/RIU,最大灵敏度能高达-597.1dB/RIU,完全有能力进行折射率传感。Similarly, when the polarizer is adjusted so that the signal light is in the P polarization, other parameter settings are the same, and the measurement results obtained are shown in Figure 5. As the refractive index increases and gets closer to the core refractive index, the reflected light continues to Decrease, monotonous change. Moreover, it is found through calculation that the refractive index sensitivity of the sensor head is at least -148.0dB/RIU, and the maximum sensitivity can be as high as -597.1dB/RIU, which is fully capable of refractive index sensing.
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