CN103694781B - Micro-effect wallpaper ink that a kind of intaglio printing is special and preparation method thereof - Google Patents
Micro-effect wallpaper ink that a kind of intaglio printing is special and preparation method thereof Download PDFInfo
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- CN103694781B CN103694781B CN201310625296.1A CN201310625296A CN103694781B CN 103694781 B CN103694781 B CN 103694781B CN 201310625296 A CN201310625296 A CN 201310625296A CN 103694781 B CN103694781 B CN 103694781B
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- 238000007639 printing Methods 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 27
- 239000000049 pigment Substances 0.000 claims abstract description 23
- 238000013019 agitation Methods 0.000 claims abstract description 21
- 230000000694 effects Effects 0.000 claims abstract description 19
- 239000003094 microcapsule Substances 0.000 claims abstract description 19
- 239000000839 emulsion Substances 0.000 claims abstract description 18
- 239000000463 material Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 12
- 239000013530 defoamer Substances 0.000 claims abstract description 12
- 239000003595 mist Substances 0.000 claims abstract description 12
- 230000008719 thickening Effects 0.000 claims abstract description 12
- 210000001589 microsome Anatomy 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 239000012153 distilled water Substances 0.000 claims abstract description 7
- 239000001993 wax Substances 0.000 claims description 21
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 5
- 229920001903 high density polyethylene Polymers 0.000 claims description 5
- 239000004700 high-density polyethylene Substances 0.000 claims description 5
- 239000002480 mineral oil Substances 0.000 claims description 5
- 229920000570 polyether Polymers 0.000 claims description 5
- 229920002635 polyurethane Polymers 0.000 claims description 5
- 239000004814 polyurethane Substances 0.000 claims description 5
- 239000002562 thickening agent Substances 0.000 claims description 5
- 230000007704 transition Effects 0.000 claims description 5
- 235000010446 mineral oil Nutrition 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 230000000007 visual effect Effects 0.000 abstract description 9
- 238000003915 air pollution Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 abstract description 2
- 239000003960 organic solvent Substances 0.000 abstract description 2
- 230000035807 sensation Effects 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 description 9
- 206010011732 Cyst Diseases 0.000 description 6
- 208000031513 cyst Diseases 0.000 description 6
- 239000012528 membrane Substances 0.000 description 6
- 239000001055 blue pigment Substances 0.000 description 5
- 239000002932 luster Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 238000009775 high-speed stirring Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- RFAFBXGYHBOUMV-UHFFFAOYSA-N calcium chromate Chemical compound [Ca+2].[O-][Cr]([O-])(=O)=O RFAFBXGYHBOUMV-UHFFFAOYSA-N 0.000 description 2
- 239000001054 red pigment Substances 0.000 description 2
- 239000012463 white pigment Substances 0.000 description 2
- PLXMOAALOJOTIY-FPTXNFDTSA-N Aesculin Natural products OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@H](O)[C@H]1Oc2cc3C=CC(=O)Oc3cc2O PLXMOAALOJOTIY-FPTXNFDTSA-N 0.000 description 1
- 241000533950 Leucojum Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The present invention relates to micro-special effect wallpaper ink of a kind of intaglio printing and working method thereof.Described formula comprises following component and mass fraction: waterborne film-forming emulsion 30 ~ 40%; Distilled water 40 ~ 50%; Moistening flatting agent 0.5 ~ 5%; Defoamer 0.1 ~ 1%; Microcapsule pigment 5 ~ 20%; Thickening material 1 ~ 5%; Micro mist wax 2 ~ 4%.Described waterborne film-forming emulsion, for get raw material according to described parts by weight, adds in agitation vat and stirs by its preparation method, adds in agitation vat successively simultaneously, stir described distilled water, moistening flatting agent, defoamer, thickening material; Then described microcapsule pigment is added in agitation vat, stir; Finally, filter with 200-300 eye mesh screen, obtain micro-some effect ink.This ink adopts water to be solvent, without the volatilization of toxic organic solvents, to free of air pollution; And to be printed on wallpaper to people's one sensation of " far seeing that color closely sees flower ", original in style visual effect can be formed in wallpaper printing.
Description
Technical field
The present invention relates to a kind of formula as special visual effect ink special on wallpaper and preparation method thereof.
Background technology
Along with the development of national economy and the raising of living standards of the people, shiploads of merchandise house and hotel, the emerging in large numbers of exhibition center, the requirement of people to house decorative material improves constantly, and wallpaper is more and more subject to people's attention as the important component part of Modern Interior Decoration material.Because wallpaper has good decorative effect, feature that is convenient and environmental protection of constructing obtains applying more and more widely.From initial in hotel, the public arena such as office building, exhibition hall, be applied to ordinarily resident's house more and more in large quantities by now.But wallpaper ink itself is confined to basic toning effect, as broad as long with the ink effect of other print fields, function ratio is more single.
Summary of the invention
The invention provides formula and the complete processing thereof of a kind of wallpaper gravure micro-some effect water color ink, the original in style visual effect that the wallpaper using this ink to prepare has " far seeing that color closely sees flower ".
The present invention solves the scheme that its technical problem adopts: a kind of wallpaper gravure micro-some effect water color ink, and it comprises the raw material of following parts by weight:
Preferably, described waterborne film-forming emulsion is aqueous acrylic emulsion, solid content 45 ~ 48%, acid number 30 ~ 60mgKOH/g, second-order transition temperature 20 ~ 40 DEG C, pH value about 7.5 ~ 9.5, viscosity 500 ~ 1000mPa.s.
Preferably, described moistening flatting agent is polyether siloxane copolymer, and effective content 100%, viscosity is about 100mPa.s.
Preferably, described defoamer is the mixture of fatty race mineral oil, and effective content 100%, viscosity is about 100mPa.s.
Preferably, described microcapsule pigment is Hayashi chemical company MCPHP series, any one in Japanese woods chemical industrial company MCP series.
Preferably, described thickening material is association type polyurethane thickener, effective content 50 ~ 60%, viscosity 2000 ~ 3000mPa.s.
Preferably, described micro mist wax is high density polyethylene waxes, effective content 100%, particle diameter 3 ~ 5 μm, fusing point 120 DEG C.
A kind of wallpaper gravure preparation method of micro-some effect water color ink, raw material is got according to described parts by weight, described waterborne film-forming emulsion is added in agitation vat and stirs, successively described distilled water, moistening flatting agent, defoamer, thickening material, micro mist wax are added in agitation vat simultaneously, stir; Then described microcapsule pigment is added in agitation vat, stir; Finally, filter with 200-300 eye mesh screen, obtain micro-some effect ink.
The present invention adopts film forming material to form fine particle coated for solid pigment, in printing-ink, the microcapsule pigment of different colours is owing to being subject to the coated of cyst membrane, so can not mutually be mixed into a kind of color and luster, only have after printing, make capsular rupture by drying oven heating, the pigment of shades of colour just discharges, so form micro-some decorative pattern of multiple color unique style.If common yellow mill base and blue mill base to be in harmonious proportion by a certain percentage with traditional wallpaper ink and will to become green mill base in same mill base, still belong to single color printing.If yellow and blue pigments are made microcapsule pigment respectively, also can be in together among a mill base, due to the obstruct by cyst membrane parcel, two kinds of pigment do not come in contact each other, namely can not colour mixture.When only having printing post-heating dry (during printing Heating temperature about 150 ~ 200 DEG C), microcapsules rupture distils, pigment just discharges and makes pattern painted respectively from cyst membrane, result in formation of micro-point of different color and luster, due to visual reason, being far seen as green decorative pattern, closely seeing but is be made up of yellow and blue micro-point.So, to the sensation that people's one " far sees that color closely sees flower ", original in style visual effect can be formed in wallpaper printing.
Beneficial effect of the present invention: (1) adopts water to be solvent, without the volatilization of toxic organic solvents, to free of air pollution; (2) lubrication to scraper when adopting wax powder to realize intaglio printing, avoids scraper to cause its wall film to break in advance to the high-speed friction of microcapsule; (3) the present invention can realize micro-point " snowflake " shape pattern that wallpaper one-step print presents polychrome multiple spot, has unique visual effect.
Embodiment
The present invention is further detailed explanation to use embodiment below, is not practical range of the present invention is confined to this.
Embodiment 1, micro-the effect wallpaper ink that a kind of intaglio printing described in the present embodiment is special, it by the raw material of following parts by weight add in agitation vat through mixing, stirring obtains:
Waterborne film-forming emulsion described in the present embodiment is the aqueous acrylic emulsion that Green spring (Xiamen) environmental protection tech materials company limited produces, solid content 47%, acid number 55, second-order transition temperature 30 DEG C, pH value about 8.5, viscosity 800mPa.s; Moistening flatting agent is
flow425, polyether siloxane copolymer, effective content 100%, viscosity 100mPa.s; Defoamer is
foamex K8, the mixture of Aliphatic mineral oils, effective content 100%, viscosity 100mPa.s; Microcapsule pigment is Hayashi chemical company MCPHP series, and wherein red pigment model is GR4614, and blue pigments is GR5315; Thickening material is
viscoPlus3030, association type polyurethane thickener, effective content 55%, viscosity 2500mPa.s; Micro mist wax is the MPE1205 of Shanghai joule wax industry, high density polyethylene waxes, effective content 100%, particle diameter 4 μm, fusing point 120 DEG C.Preparation method is, raw material is taken according to described parts by weight, described aqueous acrylic emulsion is added agitation vat high-speed stirring (stirring velocity 800rpm), successively described distilled water, moistening flatting agent, defoamer, thickening material, micro mist wax are added in agitation vat simultaneously, stir; Then described microcapsule pigment (red pigment, blue pigments successively) is added agitation vat stirring at low speed (stirring velocity 400rpm), stir; Finally, filter with 260 eye mesh screens, obtain micro-some effect ink.
When printing post-heating is dry (Heating temperature about 160 DEG C), microcapsules rupture distils, and pigment discharges and makes pattern painted respectively from cyst membrane, result in formation of micro-point of different color and luster, due to visual reason, being far seen as purple decorative pattern, closely seeing but is be made up of red and blue micro-point.
Embodiment 2, micro-the effect wallpaper ink that a kind of intaglio printing described in the present embodiment is special, it by the raw material of following parts by weight add in agitation vat through mixing, stirring obtains:
Waterborne film-forming emulsion described in the present embodiment is the aqueous acrylic emulsion that Green spring (Xiamen) environmental protection tech materials company limited produces, solid content 47%, acid number 55, second-order transition temperature 30 DEG C, pH value about 8.5, viscosity 800mPa.s; Moistening flatting agent is
flow425, polyether siloxane copolymer, effective content 100%, viscosity 100mPa.s; Defoamer is
foamex K8, the mixture of Aliphatic mineral oils, effective content 100%, viscosity 100mPa.s; Microcapsule pigment is Hayashi chemical company MCPHP series, and wherein yellow ultramarine model is GY8308, and blue pigments is GR5315; ; Thickening material is
viscoPlus3030, association type polyurethane thickener, effective content 55%, viscosity 2500mPa.s; Micro mist wax is the MPE1205 of Shanghai joule wax industry, high density polyethylene waxes, effective content 100%, particle diameter 4 μm, fusing point 120 DEG C.Preparation method is, raw material is taken according to described parts by weight, described aqueous acrylic emulsion is added agitation vat high-speed stirring (stirring velocity 800rpm), successively described distilled water, moistening flatting agent, defoamer, thickening material, micro mist wax are added in agitation vat simultaneously, stir; Then described microcapsule pigment (yellow ultramarine, blue pigments successively) is added agitation vat stirring at low speed (stirring velocity 400rpm), stir; Finally, filter with 260 eye mesh screens, obtain micro-some effect ink.
When printing post-heating is dry (Heating temperature about 170 DEG C), microcapsules rupture distils, and pigment discharges and makes pattern painted respectively from cyst membrane, result in formation of micro-point of different color and luster, due to visual reason, being far seen as green decorative pattern, closely seeing but is be made up of yellow and blue micro-point.
Embodiment 3, micro-the effect wallpaper ink that a kind of intaglio printing described in the present embodiment is special, it by the raw material of following parts by weight add in agitation vat through mixing, stirring obtains:
(numerical value is originally added and has exceeded 100%, so have modified, the numerical value as amendment is unreasonable, can revise again)
Waterborne film-forming emulsion described in the present embodiment is the aqueous acrylic emulsion that Green spring (Xiamen) environmental protection tech materials company limited produces, solid content 47%, acid number 55, second-order transition temperature 30 DEG C, pH value about 8.5, viscosity 800mPa.s; Moistening flatting agent is
flow425, polyether siloxane copolymer, effective content 100%, viscosity 100mPa.s; Defoamer is
foamex K8, the mixture of Aliphatic mineral oils, effective content 100%, viscosity 100mPa.s; Microcapsule pigment is Hayashi chemical company MCPHP series, and wherein black pigment model is GK1110, and white pigment is GW9965; Thickening material is
viscoPlus3030, association type polyurethane thickener, effective content 55%, viscosity 2500mPa.s; Micro mist wax is the MPE1205 of Shanghai joule wax industry, high density polyethylene waxes, effective content 100%, particle diameter 4 μm, fusing point 120 DEG C.Preparation method is, raw material is taken according to described parts by weight, described aqueous acrylic emulsion is added agitation vat high-speed stirring (stirring velocity 800rpm), successively described distilled water, moistening flatting agent, defoamer, thickening material, micro mist wax are added in agitation vat simultaneously, stir; Then described microcapsule pigment (black pigment, white pigment successively) is added agitation vat stirring at low speed (stirring velocity 400rpm), stir; Finally, filter with 260 eye mesh screens, obtain micro-some effect ink.
When printing post-heating is dry (Heating temperature about 190 DEG C), microcapsules rupture distils, and pigment discharges and makes pattern painted respectively from cyst membrane, result in formation of micro-point of different color and luster, due to visual reason, be far seen as grey color patterned, closely see it is but be made up of white and micro-point of black.
The above is only a preferred embodiment of the present invention, just understands method of the present invention and core concept thereof for helping.It should be pointed out that for those skilled in the art, under the premise of not departing from the present invention, can also carry out some improvement and modification to the present invention, these modifications and modification also fall in the protection domain of the claims in the present invention.
Claims (3)
1. micro-the effect wallpaper ink that intaglio printing is special, is characterized in that: it comprises the raw material of following weight percentage:
Described waterborne film-forming emulsion is aqueous acrylic emulsion, solid content 45 ~ 48%, acid number 30 ~ 60mgKOH/g, second-order transition temperature 20 ~ 40 DEG C, pH value 7.5 ~ 9.5, viscosity 500 ~ 1000mPa.s;
Described moistening flatting agent is polyether siloxane copolymer, effective content 100%, viscosity 50 ~ 300mPa.s;
Described defoamer is the mixture of fatty race mineral oil, effective content 100%, viscosity 50 ~ 300mPa.s;
Described thickening material is association type polyurethane thickener, effective content 50 ~ 60%, viscosity 2000 ~ 3000mPa.s;
Described micro mist wax is high density polyethylene waxes, effective content 100%, particle diameter 3 ~ 5 μm, fusing point 120 DEG C;
Described microcapsule pigment is powder or emulsion form, particle diameter≤10 μm.
2. micro-the effect wallpaper ink that a kind of intaglio printing as claimed in claim 1 is special, is characterized in that: described micro mist wax is the MPE1205 of Shanghai joule wax industry.
3. the wallpaper gravure preparation method of micro-some effect water color ink, first raw material is got according to weight percentage described in claim 1, described waterborne film-forming emulsion is added in agitation vat and stirs, successively described distilled water, moistening flatting agent, defoamer, thickening material, micro mist wax are added in agitation vat simultaneously, stir; Then described microcapsule pigment is added in agitation vat, stir; Finally, filter with 200-300 eye mesh screen, obtain micro-some effect ink.
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| CN201310625296.1A CN103694781B (en) | 2013-11-28 | 2013-11-28 | Micro-effect wallpaper ink that a kind of intaglio printing is special and preparation method thereof |
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| CN201310625296.1A CN103694781B (en) | 2013-11-28 | 2013-11-28 | Micro-effect wallpaper ink that a kind of intaglio printing is special and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109337440A (en) * | 2018-09-26 | 2019-02-15 | 浙江美浓世纪集团有限公司 | A kind of environment-friendly water-based gravure printing ink and preparation method thereof |
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| CN104530870A (en) * | 2014-12-24 | 2015-04-22 | 宁波高佳环保涂料有限公司 | Special water-based printing crack pulp for wallpaper and preparation method and application thereof |
| CN105332318A (en) * | 2015-10-27 | 2016-02-17 | 福建圣莉雅环保壁纸有限公司 | Paste containing wax powder, manufacturing process thereof and application of paste in wallpaper |
| JP7187173B2 (en) * | 2018-05-08 | 2022-12-12 | 日本化薬株式会社 | Ink and inkjet printing method |
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| JP4426378B2 (en) * | 2004-05-24 | 2010-03-03 | パイロットインキ株式会社 | Reversible thermochromic water-based ink composition for ballpoint pen and ballpoint pen using the same |
| JP2013082209A (en) * | 2011-09-29 | 2013-05-09 | Fujifilm Corp | Image forming method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109337440A (en) * | 2018-09-26 | 2019-02-15 | 浙江美浓世纪集团有限公司 | A kind of environment-friendly water-based gravure printing ink and preparation method thereof |
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Effective date of registration: 20150629 Address after: 361000, room 3003, Xuan industrial building, pioneer zone, torch hi tech Zone, Xiamen, Fujian Applicant after: Fujian Green Spring Technology Co.,Ltd. Address before: Tongan District of Xiamen City, Fujian province 361000 District Siming Park Central East Sea industrial plant No. 90 3 floor Green spring (Xiamen) environmental Greenway Technology Materials Co Applicant before: Lin Guoliang |
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Effective date of registration: 20240116 Address after: Room 101, Building G, No. 18 Zhenxing Road, Fugong Town, Longhai District, Zhangzhou City, Fujian Province, 363100 Patentee after: Zhangzhou Green Spring Science and Technology Co.,Ltd. Address before: 361000 South 101A room, Chuang Chuang business park, torch high tech Zone, Xiamen, Fujian Patentee before: FUJIAN GREEN SPRING NEW MATERIAL CO.,LTD. |