CN103690915A - Yao medicine bath pharmaceutical composition and preparation method thereof - Google Patents
Yao medicine bath pharmaceutical composition and preparation method thereof Download PDFInfo
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- CN103690915A CN103690915A CN201310715249.6A CN201310715249A CN103690915A CN 103690915 A CN103690915 A CN 103690915A CN 201310715249 A CN201310715249 A CN 201310715249A CN 103690915 A CN103690915 A CN 103690915A
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Abstract
The invention discloses a Yao medicine bath pharmaceutical composition and a preparation method thereof and belongs to the field of household chemicals. The composition comprises 10-30 weight parts of semiliquidambar cathayensis, 10-30 weight parts of caulis spatholobi, 10-30 weight parts of lycopodium clavatum and 65-90 weight parts of ginger for preparing a Yao medicine extract. The method for preparing the Yao medicine bath pharmaceutical composition comprises the following steps: weighing 10-30 weight parts of semiliquidambar cathayensis, 10-30 weight parts of caulis spatholobi, 10-30 weight parts of lycopodium clavatum and 65-90 weight parts of ginger, adding the components into 200-1000 weight parts of ethanol solution for soaking, performing ultrasonic-microwave assisted extraction, filtering to obtain the filtrate after extraction, and performing vacuum freeze drying on the filtrate to obtain the Yao medicine extract. The invention provides a Yao medicine body wash which is low in price and can have an effective effect of preventing rheumatism and other diseases through daily use.
Description
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Technical field
The present invention relates to daily health products field, particularly a kind of can relaxing muscles and tendons to promote blood circulation, Yao nationality's dipping pharmaceutical composition of expelling wind and removing dampness and preparation method thereof.
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Background technology
Rheumatic osteopathia is that wind-cold damp pathogen is invaded due to human body, and wind-cold damp pathogen is invaded after human body, causes muscle arteries and veins blocking barrier, and " stagnation of QI and blood may bring about pain " often causes that congestion and swelling pain occurs at the positions such as human synovial, periosteum, muscle thus.The main manifestations of rheumatic osteopathia is arthralgia, numb limbs and tense tendons, and disease that QI and blood is obstructed etc., easily occurs in rainyly, under the environment that there was dampness in the air, to people, brings great misery and inconvenience.At present, that on market, sells mostly is medicine for treatment thing preparation for rheumatismal product, is all generally by pharmaceutical preparation, its rheumatism symptom to be treated after patient is sick.
In realizing process of the present invention, inventor finds that prior art at least exists following problem: the pharmaceutical preparation of selling in the market treatment rheumatism is all generally to carry out symptomatic treatment for existing rheumatism symptom, cannot be by using rheumatism is played to effective prevention continuously in daily life.
Due to some ethnic groups of China, as the Yao nationality of south China, hang up one's hat in mountain area, in overcast and rainy moist living environment, find gradually that some can be for suppressing rheumatic ostalgia, the pharmaceutical composition that loose warp is active, as Chinese patent application 201310080024.8 discloses a kind of Yao nationality dipping pharmaceutical composition and preparation method thereof, its composition, preparation technology is simple, more traditional preparation method is easy, and there is good energy relaxing muscles and tendons to promote blood circulation, expelling wind and removing dampness effect, but because it is to use as bath gel, its action time for skin and joint is short, generally only can clean several minutes lesions position, be difficult to reach lasting medicine, the effect that the efficacy of a drug is penetrating.
Prior art generally obtains by one or several of aforementioned pharmaceutical compositions being brought put into the solution that contains its effective ingredient after water boils, then carries out bathing with solution, and such mode not only wastes time and energy, and is also difficult to carry out industrialized applying.
Summary of the invention
For the dipping compositions drug effect that solves relaxing muscles and tendons to promote blood circulation, expelling wind and removing dampness is lasting not, the technical problem of the effect of the penetrating deficiency of the efficacy of a drug and the technical problem that dipping compositions is carried out suitability for industrialized production, the mode with dipping of the invention provides is to rheumatic ostalgia, the obstructed a kind of Yao nationality dipping pharmaceutical composition for the treatment of of QI and blood and preparation method thereof.Yao nationality's dipping pharmaceutical composition comprises following composition:
Pterospermi Heterophylli 10～30 weight portions, Caulis Spatholobi 10～30 weight portions, Herba Lycopodii 10～30 weight portions, Rhizoma Zingiberis Recens 65～90 weight portions.
Further: described Pterospermi Heterophylli powder is that 30 weight portions, Caulis Spatholobi are that 30 weight portions, Herba Lycopodii are 30 weight portions, and Rhizoma Zingiberis Recens is 80 weight portions.
Further: the present invention also provides the preparation method of Yao nationality's dipping pharmaceutical composition, comprises the following steps:
Step a. takes Pterospermi Heterophylli 10～30 weight portions, Caulis Spatholobi 10～30 weight portions, Herba Lycopodii 10～30 weight portions, Rhizoma Zingiberis Recens 65～90 weight portions, all grinds powder;
After the powder Pterospermi Heterophylli that step b. obtains previous step, Caulis Spatholobi, Herba Lycopodii, Rhizoma Zingiberis Recens powder mix, be added to 200～400 weight portions, percentage by weight is in more than 45% alcoholic solution, to soak 30～60 minutes;
The liquid obtaining after the medicine that step c obtains previous step and alcoholic solution mix carries out ultrasonic-microwave auxiliary extraction, ultrasonic power is 600～800w, microwave power is 500～800w, extraction temperature is 25～60 ℃, extraction time is 15～30 seconds, repeatedly extract 8～10 times, after extraction, filter to get filtrate;
Steps d. filtrate vacuum lyophilization, obtains described Yao nationality dipping pharmaceutical composition.
Further: described Pterospermi Heterophylli powder is that 70 weight portions, Caulis Spatholobi are that 30 weight portions, Herba Lycopodii are that 30 weight portions, Rhizoma Zingiberis Recens are 40 weight portions, in the alcoholic solution that to be added to 300 weight portions, percentage by weight be 75%, soak, then carry out ultrasonic-microwave auxiliary extraction, ultrasonic power is 800w, microwave power is 800w, extraction temperature is 60 ℃, and extraction time is 30 seconds, repeatedly extracts 8 times.
Further: the present invention also provides the using method of Yao nationality's dipping pharmaceutical composition: Yao nationality's dipping pharmaceutical composition of 1 weight portion is evenly mixed with the water of 100～500 parts of 50～100 ° of C.
The beneficial effect that the present invention brings is:
1.Gai Yao nationality dipping pharmaceutical composition provide a kind of from daily health caring field pre-antirheumatic product, raw materials used low price, Pterospermi Heterophylli has wind-damp dispelling, promoting the circulation of QI for relieving swelling, the effects such as anti-inflammatory and antalgic, Rhizoma Zingiberis Recens has warm, the functions such as expelling wind and activating blood circulation, the two same used time, by the gingerol chafe diastole in Rhizoma Zingiberis Recens, blood circulation promoting, thereby promote the absorption of skin to Pterospermi Heterophylli effective ingredient, strengthened the promoting the circulation of QI for relieving swelling of Pterospermi Heterophylli to human body, the functions such as expelling wind and cold, Caulis Spatholobi can be treated the waist gonalgia due to rheumatism, rheumatic arthralgia, numb limbs and tense tendons etc., three is with using preventing and improve rheumatic arthritis, rheumatic arthralgia, numbness of hands and feet, lumbar muscle strain, the symptoms such as traumatic injury, Herba Lycopodii can strengthen drug effect, improve the penetrating power of this pharmaceutical composition.
2. by the method for dipping, can improve the effect of this pharmaceutical composition, compared with bath gel, its directivity is stronger, and focus is fully contacted with the effective ingredient of medicine in bathing process by pharmaceutical composition, while being aided with dipping, the effect of warm water can be played to the persistency of the permeability of the efficacy of a drug, drug effect the effectiveness of Synergistic, thereby can be for arthralgia, numb limbs and tense tendons, disease that QI and blood is obstructed etc. is more effective.
3. adopt the effective ingredient of ultrasonic extraction medicine, can also realize the suitability for industrialized production of this pharmaceutical composition in the drug effect that keeps effective ingredient, consumer is also more convenient, quick in use.
The specific embodiment
For making the object, technical solutions and advantages of the present invention clearer, below embodiment of the present invention is described further in detail.
Further: the present invention also provides the preparation method of Yao nationality's dipping pharmaceutical composition, comprises the following steps:
Step a. takes Pterospermi Heterophylli 10～30 weight portions, Caulis Spatholobi 10～30 weight portions, Herba Lycopodii 10～30 weight portions, Rhizoma Zingiberis Recens 65～90 weight portions, all grinds powder;
After the powder Pterospermi Heterophylli that step b. obtains previous step, Caulis Spatholobi, Herba Lycopodii, Rhizoma Zingiberis Recens powder mix, be added to 200～400 weight portions, percentage by weight is to soak in more than 45% alcoholic solution;
The liquid obtaining after the medicine that step c obtains previous step and alcoholic solution mix carries out ultrasonic-microwave auxiliary extraction, ultrasonic power is 600～800w, microwave power is 500～800w, extraction temperature is 25～60 ℃, extraction time is 15～30 seconds, repeatedly extract 8～10 times, after extraction, filter to get filtrate;
Steps d. filtrate vacuum lyophilization, obtains described Yao nationality dipping pharmaceutical composition.
Further: described Pterospermi Heterophylli powder is that 70 weight portions, Caulis Spatholobi are that 30 weight portions, Herba Lycopodii are that 30 weight portions, Rhizoma Zingiberis Recens are 40 weight portions, in the alcoholic solution that to be added to 300 weight portions, percentage by weight be 75%, soak, then carry out ultrasonic-microwave auxiliary extraction, ultrasonic power is 800w, microwave power is 800w, extraction temperature is 60 ℃, and extraction time is 30 seconds, repeatedly extracts 8 times.
Further: the present invention also provides the using method of Yao nationality's dipping pharmaceutical composition: Yao nationality's dipping pharmaceutical composition of 1 weight portion is evenly mixed with the water of 100～500 parts of 50～100 ° of C.
Beneficial effect of the present invention is:
Cheap, formula is simple;
2. product provided by the invention is easy to industrialization, is applicable to large-scale promotion;
3. compared with bath gel, this product is dissolved in hot water by pharmaceutical composition, in conjunction with soaking, crumple affected part, the better effects if playing, more obvious.
Embodiment 1
Prepare precious jade medicament extract:
Take Pterospermi Heterophylli 20kg, Caulis Spatholobi 20 kg, Herba Lycopodii 20 kg, Rhizoma Zingiberis Recens 90 kg, whole grinds powders, after mixing, be added in the alcoholic solution that percentage by weight is 65%, 400 kg and soak 60 minutes, the temperature of this solution is adjusted to 45 ° of C left and right, then this solution is carried out ultrasonic-microwave auxiliary extraction 10 times, hyperacoustic power is made as to 700w, microblogging power is made as 600w, each 25 seconds, after extraction, filter to get filtrate, filtrate vacuum lyophilization, obtains described Yao nationality dipping pharmaceutical composition.
During use, Yao nationality's dipping pharmaceutical composition of the weight portion of 100 grams is evenly mixed with the water of 20000 grams, 80 ° C left and right.
Embodiment 2
Prepare precious jade medicament extract:
Take Pterospermi Heterophylli 10KG, Caulis Spatholobi 10KG, Herba Lycopodii 20 KG, Rhizoma Zingiberis Recens 65KG, whole grinds powders, are added to percentage by weight and are 45%, soak 30 minutes in the alcoholic solution of 200KG after mixing, the temperature of this solution is adjusted to 25 ° of C left and right, then this solution is carried out ultrasonic-microwave auxiliary extraction 8 times, hyperacoustic power is made as to 600w, microblogging power is made as 500w, each 15 seconds, after extraction, filter to get filtrate, filtrate vacuum lyophilization, obtains described Yao nationality dipping pharmaceutical composition.
During use, Yao nationality's dipping pharmaceutical composition of the weight portion of 100 grams is evenly mixed with the water of 10000 grams, 50 ° C left and right.
Embodiment 3
Prepare precious jade medicament extract:
Take Pterospermi Heterophylli 30KG, Caulis Spatholobi 30KG, Herba Lycopodii 30 KG, Rhizoma Zingiberis Recens 80KG, whole grinds powders, are added to percentage by weight and are 75%, soak 30 minutes in the alcoholic solution of 300KG after mixing, the temperature of this solution is adjusted to 60 ° of C left and right, then this solution is carried out ultrasonic-microwave auxiliary extraction 8 times, hyperacoustic power is made as to 800w, microblogging power is made as 800w, each 30 seconds, after extraction, filter to get filtrate, filtrate vacuum lyophilization, obtains described Yao nationality dipping pharmaceutical composition.
During use, Yao nationality's dipping pharmaceutical composition of the weight portion of 100 grams is evenly mixed with the water of 50000 grams, 100 ° C left and right.
The effect of Yao nationality's dipping pharmaceutical composition that table 1 embodiment of the present invention 1-3 provides
Embodiment of the present invention 1-3 is divided into 3 groups, and in conjunction with 1 group of matched group, Jiang Gai Yao nationality dipping pharmaceutical composition is tested, and suffers from for a long time the arthritic patient of rheumatic ostalgia for 10 every group and observes.(male 15 examples, female's 25 examples, 51.2 years old mean age).The results detailed in Table 1.
Table 1 clinical application effect table
| Embodiment | Recovery from illness (%) | Improve (%) | Invalid (%) |
| Embodiment 1 | 40 | 10 | 50 |
| Embodiment 2 | 40 | 30 | 30 |
| Embodiment 3 | 50 | 20 | 30 |
| Hot water matched group | 0 | 5 | 95 |
Result shows: adopt the Yao nationality of the present invention dipping pharmaceutical composition, use safety, effective, to suffering from for a long time the arthritic patient of rheumatic ostalgia, have good curative effect.Be below several model cases:
Case 1: Wang * *, female, 42 years old, owing to causing lower limb to suffer from rheumatic ostalgia existing more than 10 year at field work for a long time.Use the embodiment of the present invention 1, every day 2 times, 20 minutes, each medication blister foot affected part, aftersensation affected part rheumatic ostalgia phenomenon made moderate progress on 15th, after stopping using, observed, and in 30 days, did not have outbreak sign.
Case 2: what * *, man, 61 years old, because lower limb suffer from rheumatic ostalgia existing more than 30 year.Use the embodiment of the present invention 2, every day 3 times, 15 minutes, each medication blister foot affected part, aftersensation affected part rheumatic ostalgia phenomenon was alleviated to some extent on 30th, after stopping using, observed, and in 45 days, did not have outbreak sign.
Case 3: woods * *, female, 28 years old, because lower limb suffer from rheumatic ostalgia existing more than 3 year, day cold often feel knee twinge, stair activity needs people to assist in maybe can only to hold up balustrade slowly or downstairs upstairs.Use the embodiment of the present invention 3, every day 2 times, 10 minutes, each medication blister foot affected part, feels in 45 days that affected part rheumatic ostalgia phenomenon is alleviated to some extent until transference cure is observed after stopping using, and does not have outbreak sign, recovery from illness in 90 days.
Claims (5)
1.Yi Zhong Yao nationality dipping pharmaceutical composition, is characterized in that, comprises following composition:
Pterospermi Heterophylli 10～30 weight portions, Caulis Spatholobi 10～30 weight portions, Herba Lycopodii 10～30 weight portions, Rhizoma Zingiberis Recens 65～90 weight portions.
2. the Yao nationality as claimed in claim 1 dipping pharmaceutical composition, is characterized in that: described Pterospermi Heterophylli powder is that 30 weight portions, Caulis Spatholobi are that 30 weight portions, Herba Lycopodii are 30 weight portions, and Rhizoma Zingiberis Recens is 80 weight portions.
3. the preparation method of the Yao nationality as claimed in claim 1 dipping pharmaceutical composition, is characterized in that comprising the following steps:
Step a. takes Pterospermi Heterophylli 10～30 weight portions, Caulis Spatholobi 10～30 weight portions, Herba Lycopodii 10～30 weight portions, Rhizoma Zingiberis Recens 65～90 weight portions, all grinds powder;
After the powder Pterospermi Heterophylli that step b. obtains previous step, Caulis Spatholobi, Herba Lycopodii, Rhizoma Zingiberis Recens powder mix, be added to 200～400 weight portions, percentage by weight is in more than 45% alcoholic solution, to soak 30～60 minutes;
The liquid obtaining after the medicine that step c obtains previous step and alcoholic solution mix carries out ultrasonic-microwave auxiliary extraction, ultrasonic power is 600～800w, microwave power is 500～800w, extraction temperature is 25～60 ℃, extraction time is 15～30 seconds, repeatedly extract 8～10 times, after extraction, filter to get filtrate;
Steps d. filtrate vacuum lyophilization, obtains described Yao nationality dipping pharmaceutical composition.
4. the preparation method of the Yao nationality as claimed in claim 1 dipping pharmaceutical composition, it is characterized in that: described Pterospermi Heterophylli powder is that 70 weight portions, Caulis Spatholobi are that 30 weight portions, Herba Lycopodii are that 30 weight portions, Rhizoma Zingiberis Recens are 40 weight portions, in the alcoholic solution that to be added to 300 weight portions, percentage by weight be 75%, soak, then carry out ultrasonic-microwave auxiliary extraction, ultrasonic power is 800w, and microwave power is 800w, and extraction temperature is 60 ℃, extraction time is 30 seconds, repeatedly extracts 8 times.
5. the using method of the Yao nationality as claimed in claim 1 or 2 dipping pharmaceutical composition, is characterized in that: Yao nationality's dipping pharmaceutical composition of 1 weight portion is evenly mixed with the water of 100～500 parts of 50～100 ° of C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201310715249.6A CN103690915A (en) | 2013-12-23 | 2013-12-23 | Yao medicine bath pharmaceutical composition and preparation method thereof |
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| CN201310715249.6A CN103690915A (en) | 2013-12-23 | 2013-12-23 | Yao medicine bath pharmaceutical composition and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104435530A (en) * | 2014-11-04 | 2015-03-25 | 覃芬芬 | Yao nationality bath medicament composition and preparation method thereof |
| CN105106365A (en) * | 2015-08-11 | 2015-12-02 | 东莞俪恒生物科技有限公司 | Medicated bath composition |
| CN105832584A (en) * | 2016-05-24 | 2016-08-10 | 贵州理工学院 | Yao medicine bath essential oil hand cream and preparation method thereof |
| CN106511922A (en) * | 2016-10-25 | 2017-03-22 | 黄赵玲 | Channel and collateral heat generation medicinal oil agent for bucket medicated bath and preparation method thereof |
| CN109330958A (en) * | 2018-11-28 | 2019-02-15 | 柳州两面针股份有限公司 | Chinese medicine composition is preparing the application in bath agent |
| CN110368481A (en) * | 2019-09-05 | 2019-10-25 | 山西中芮椒业有限公司 | A kind of Chinese prickly ash lavipeditum pack and application method |
| CN115337364A (en) * | 2022-09-19 | 2022-11-15 | 广东技术师范大学 | Medicated bath bag and preparation method and application thereof |
| CN116036163A (en) * | 2022-12-31 | 2023-05-02 | 从江福临瑶浴开发有限公司 | Yao nationality nursing medicine for gynecopathy |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104435530A (en) * | 2014-11-04 | 2015-03-25 | 覃芬芬 | Yao nationality bath medicament composition and preparation method thereof |
| CN105106365A (en) * | 2015-08-11 | 2015-12-02 | 东莞俪恒生物科技有限公司 | Medicated bath composition |
| CN105832584A (en) * | 2016-05-24 | 2016-08-10 | 贵州理工学院 | Yao medicine bath essential oil hand cream and preparation method thereof |
| CN106511922A (en) * | 2016-10-25 | 2017-03-22 | 黄赵玲 | Channel and collateral heat generation medicinal oil agent for bucket medicated bath and preparation method thereof |
| CN109330958A (en) * | 2018-11-28 | 2019-02-15 | 柳州两面针股份有限公司 | Chinese medicine composition is preparing the application in bath agent |
| CN109330958B (en) * | 2018-11-28 | 2021-04-20 | 柳州两面针股份有限公司 | Application of traditional Chinese medicine composition in preparation of bath agent |
| CN110368481A (en) * | 2019-09-05 | 2019-10-25 | 山西中芮椒业有限公司 | A kind of Chinese prickly ash lavipeditum pack and application method |
| CN115337364A (en) * | 2022-09-19 | 2022-11-15 | 广东技术师范大学 | Medicated bath bag and preparation method and application thereof |
| CN116036163A (en) * | 2022-12-31 | 2023-05-02 | 从江福临瑶浴开发有限公司 | Yao nationality nursing medicine for gynecopathy |
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