CN103674782B - Rotating cylinder flow graph circulation of fluid collimation distributor - Google Patents

Rotating cylinder flow graph circulation of fluid collimation distributor Download PDF

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CN103674782B
CN103674782B CN201310545975.8A CN201310545975A CN103674782B CN 103674782 B CN103674782 B CN 103674782B CN 201310545975 A CN201310545975 A CN 201310545975A CN 103674782 B CN103674782 B CN 103674782B
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fluid
passage
circulation
ring
collimation
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CN103674782A (en
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丁仕强
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Dalian University
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Dalian University
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Abstract

A kind of circulation of fluid collimation distributor, spiral type influent stream passage with dispensing orifice, dispensing orifice was along EDS maps under spiral type influent stream passage one week, dispensing orifice UNICOM separately below perpendicular passage vertically downward, between continuously arranged perpendicular passage and perpendicular passage, part constitutes Ring-cylindrical, the space UNICOM below perpendicular passage and between flow graph rotor and urceolus.It is equal with flow graph rotor, urceolus interior diameter respectively that perpendicular channel width is preferably equal to the inner and outer diameter of measurement space width, i.e. Ring-cylindrical so that perpendicular channel width is equal to measurement space width.Use " the circulation of fluid collimation distributor " of the present invention, when using drum-type rheometer to measure free settling suspension flow variable element, can make circulation of fluid with vertical direction enter measurement space and enter time equiblibrium mass distribution in ring section, so that flow graph is by original operation principle and computation model running, it is not required to any correction.

Description

Rotating cylinder flow graph circulation of fluid collimation distributor
Technical field
The invention belongs to field of chemical engineering, be specifically related to when a kind of drum-type rheometer measures free settling suspension flow variable element circulation of fluid be collimated and the measuring appliance of distribution.
Background technology
When measuring free settling suspension flow degeneration with drum-type rheometer, for overcoming fluid heterogeneous body problem in the measurement space that the sedimentation of particle causes, allowing measured suspension be circulated through measurement space through exterior line is a kind of effective solution (patent of invention see Xu Ji profit et al.: drum-type rheometer circulating system, patent publication No.: CN101788445A).Drum-type rheometer circulating system, including rotor, urceolus, peristaltic pump and circulation pipe, rotor is placed in urceolus, connects circulation pipe bottom urceolus, and circulation pipe is connected with peristaltic pump, and the other end of circulation pipe is placed between rotor and urceolus.Use this invention and be set for operation according to required technology, can effectively measure the rheological parameter of free settling solid-liquid suspension system.But this drum-type rheometer circulating system, circulation of fluid enters measurement space local location with vertical direction, there is the velocity component of radial direction and direction of rotation at whole measurement space, the fluid of entrance measurement space is difficulty with equiblibrium mass distribution on the whole ring section between inside and outside cylinder.It cannot ensure that flow graph can work according to original principle under conditions of fluid circulates, and computation model to be changed.
Summary of the invention
The present invention is just to provide the drum-type rheometer circulating system that such a rotating cylinder flow graph circulation of fluid collimation distributor is constituted, and makes fluid realize equiblibrium mass distribution when circulating and eliminate radial direction and the fluid velocity of direction of rotation, thus ensures that flow graph normally works.Guarantee that flow graph according to original principle work under conditions of fluid circulates, and can not change computation model.
The rotating cylinder flow graph circulation of fluid collimation distributor of the present invention, spiral type influent stream passage with dispensing orifice, dispensing orifice was along EDS maps under spiral type influent stream passage one week, dispensing orifice UNICOM separately below perpendicular passage vertically downward, between continuously arranged perpendicular passage and perpendicular passage, part constitutes Ring-cylindrical, the space UNICOM below perpendicular passage and between flow graph rotor and urceolus.It is equal with flow graph rotor, urceolus interior diameter respectively that perpendicular channel width is preferably equal to the inner and outer diameter of measurement space width, i.e. Ring-cylindrical so that perpendicular channel width is equal to measurement space width.So rotating cylinder flow graph circulation of fluid collimation distributor of the present invention, by the fluid of circulation before entering measurement space, it is initially formed helical flow, it is evenly distributed to the dispensing orifice of a week again, direct fluid is become fluid vertically downward by dispensing orifice each perpendicular passage vertically below, ensure that the fluid entering measurement space only flows downward, and there is no the shunting in other directions.Different helical angles (tangential direction of spiral and horizontal angle) and equally distributed dispensing orifice can ensure circulation of fluid equiblibrium mass distribution on whole measurement space ring section.With the spiral type influent stream passage of dispensing orifice, at streamwise, at the rectangle dispensing orifice that influent stream channel bottom setting space is equal.
Different helical angles (tangential direction of spiral and horizontal angle) and different passage lengths vertically downward, adapt to different hydrometries, simultaneously erect passage vertically downward in order to what same fluid used different helical angles or different length, realize different mensuration.Devise the series helix shape passage with different helical angle to select for during different fluid circulating load.In order to prevent the sedimentation of particle, suitable different pressures and the mensuration of suspension adapting to different spiral angles, the hypomere of Ring-cylindrical is preferably detachably connectable.The remaining spiral type influent stream passage with dispensing orifice, the epimere that below dispensing orifice, UNICOM vertically downward erects passage, can individually be referred to as spiral type influent stream passage.Detachably connectable Ring-cylindrical hypomere and the connection of epimere can be Flange joint or bonding or screw thread socket or transition socket.Ring-cylindrical hypomere and perpendicular passage can individually be referred to as Ring-cylindrical collimator.The Ring-cylindrical collimator so formed, below spiral type influent stream passage, is a circular cylindrical fluid collimator, and its effect is to eliminate the tangential of circulation of fluid and Radial Flow further.The annular width of Ring-cylindrical collimator is equal with measurement space width, has the perpendicular passage of arranged distribution, each passage to dock completely with each passage below the dispensing orifice of spiral type influent stream passage along annulus.The fluid flowed out in collimator duct only has the speed of vertical direction.Spiral type influent stream passage and perpendicular passage with dispensing orifice are made up of transparent material, and whether the equilibrium assignment effect that can observe spirality channel from outside completes.
Spiral type influent stream passage, Ring-cylindrical collimator, flow graph urceolus arrange from top to bottom, are preferably connected by ring flange between any two.Leaving 1mm gap between Ring-cylindrical collimator inner wall lower edge and flow graph rotor, both ensured that the rotation of rotor was interference-free, and made again the circulation of fluid overwhelming majority enter measurement space, the fluid flowing to rotor upper end on a small quantity from gap will not impact.Theoretical research proves, fluid is when drum-type rheometer interval of internal and external tube internal circulation flow, if meeting following condition:
(1) circulation of fluid enters measurement space with vertical direction, i.e. in addition to axial velocity, there is not the velocity component of radial direction and direction of rotation;
(2) equiblibrium mass distribution on the fluid of the measurement space whole ring section between inside and outside cylinder it is recycled into;
Then can ensure that flow graph according to original principle work under conditions of fluid circulates, and can not change computation model.
Beneficial effects of the present invention: use " the circulation of fluid collimation distributor " of the present invention, when using drum-type rheometer to measure free settling suspension flow variable element, can make circulation of fluid with vertical direction enter measurement space and enter time equiblibrium mass distribution in ring section, so that flow graph is by original operation principle and computation model running, it is not required to any correction.
Accompanying drawing explanation
Fig. 1 is the overall assembling schematic diagram of a kind of drum-type rheometer circulation of fluid collimation distributor of the present invention;Fig. 2 is the schematic diagram of the whole clearing of this drum-type rheometer circulation of fluid collimation distributor;Fig. 3 is the schematic diagram of the transparent spiral shape influent stream passage top half of this drum-type rheometer circulation of fluid collimation distributor;Fig. 4 is transparent spiral shape influent stream passage the latter half and the schematic diagram of perpendicular channel part of this drum-type rheometer circulation of fluid collimation distributor;Fig. 5 is the schematic diagram of the flow graph rotor urceolus of this drum-type rheometer circulation of fluid collimation distributor.Fig. 6 is the overall assembling schematic diagram of the another kind of drum-type rheometer circulation of fluid collimation distributor of the present invention;Fig. 7 is the schematic diagram of the spiral type influent stream passage top half end cap of this drum-type rheometer circulation of fluid collimation distributor;Fig. 8 is spiral type influent stream passage the latter half and the schematic diagram of perpendicular channel part of this drum-type rheometer circulation of fluid collimation distributor;Fig. 9 is the schematic diagram of the flow graph rotor urceolus of this drum-type rheometer circulation of fluid collimation distributor;Figure 10 is the schematic diagram of the Ring-cylindrical collimator segment of this drum-type rheometer circulation of fluid collimation distributor.
Detailed description of the invention
As shown in Figure 1, a kind of rotating cylinder flow graph circulation of fluid collimation distributor of the present invention, it is characterized in that: with the spiral type influent stream passage of dispensing orifice, dispensing orifice was along EDS maps under spiral type influent stream passage one week, dispensing orifice UNICOM separately below perpendicular passage vertically downward, between continuously arranged perpendicular passage and perpendicular passage, part constitutes Ring-cylindrical, the space UNICOM below Ring-cylindrical and between flow graph rotor and urceolus.The hypomere of Ring-cylindrical is that detachably connectable Ring-cylindrical and perpendicular passage, Ring-cylindrical hypomere and perpendicular passage are separately formed Ring-cylindrical collimator.Epimere Ring-cylindrical and perpendicular passage can also be collectively referred to spiral type influent stream passage with spiral type influent stream passage.For the ease of forming the passage of spiral type type, spiral type influent stream passage is segmented into spiral type influent stream passage top half (Fig. 3) and spiral type influent stream passage the latter half (Fig. 4), spiral type influent stream passage is formed, with dispensing orifice and perpendicular passage below the spiral type influent stream passage of spiral type influent stream passage the latter half after two parts combination.Being connected with Ring-cylindrical collimator through flange below spiral type influent stream passage, Ring-cylindrical collimator is connected with flow graph urceolus (Fig. 5) through flange again.Flow graph rotor is placed in urceolus, connects with spiral type influent stream channel entrance through peristaltic pump, circulation pipe bottom urceolus, it is achieved fluid circulates.This specially designed circulation of fluid collimation distributor when measuring free settling suspension flow variable element for drum-type rheometer, the utilization of this collimation distributor, flow graph can be made to work according to its original principle and computation model, and do not circulated by fluid and affected.The circulation of fluid collimation distributor of the present invention is made up of two parts.First spiral type circulation of fluid influent stream passage, the rectangle dispensing orifice being uniformly arranged in channel bottom and the spiral current flowing mode of circulation of fluid, dispensing orifice equiblibrium mass distribution on the annular measurement space cross section of flow graph can be passed the fluid through;It two is Ring-cylindrical fluid collimator, has the vertical channel of certain distance in this collimator, the radial direction of circulation of fluid and tangential flow velocity can be made to be eliminated, and only retain and flow graph work is not had influential axial flowing.For guaranteeing that circulation of fluid flows with vertical speed in collimation distributor and equilibrium assignment is on the ring section in rheometry space, devise the series helix shape feeding-passage of interchangeable different helical angle, and Ring-cylindrical fluid collimator design is made by transparent material, in order to directly observe the flow condition of fluid.See Fig. 2.
As shown in Figure 6, the rotating cylinder flow graph circulation of fluid collimation distributor of the another kind of present invention, it is characterized in that: with the spiral type influent stream passage of dispensing orifice, dispensing orifice was along EDS maps under spiral type influent stream passage one week, dispensing orifice UNICOM separately below perpendicular passage vertically downward, between continuously arranged perpendicular passage and perpendicular passage, part constitutes Ring-cylindrical, the space UNICOM below Ring-cylindrical and between flow graph rotor and urceolus.The hypomere of Ring-cylindrical is that detachably connectable Ring-cylindrical and perpendicular passage, Ring-cylindrical hypomere and perpendicular passage are separately formed Ring-cylindrical collimator.Epimere Ring-cylindrical and perpendicular passage can also be collectively referred to spiral type influent stream passage with spiral type influent stream passage.For the ease of processing the passage of spiral type type, the spiral type influent stream passage with dispensing orifice is divided into spiral type influent stream passage top half end cap (Fig. 7) and spiral type influent stream passage the latter half (Fig. 8), forms spiral type influent stream passage after two parts combination.With dispensing orifice and perpendicular passage below the spiral type influent stream passage of spiral type influent stream passage the latter half.Spiral type influent stream passage is connected with Ring-cylindrical collimator (Figure 10) through flange below the latter half, and Ring-cylindrical collimator is connected with flow graph urceolus (Fig. 9) through flange again.Flow graph rotor is placed in urceolus, connects with spiral type influent stream channel entrance through peristaltic pump, circulation pipe bottom urceolus, it is achieved fluid circulates.The hypomere of Ring-cylindrical be separate connect Ring-cylindrical and perpendicular passage, Ring-cylindrical hypomere and perpendicular passage be separately formed Ring-cylindrical collimator;Below its part above Ring-cylindrical and perpendicular passage and spiral type influent stream passage and dispensing orifice is collectively referred to spiral type influent stream passage the latter half.
Circulation of fluid, after spiral type influent stream passage and Ring-cylindrical collimator, eliminates tangential and radial velocity, and equiblibrium mass distribution on the cross section of annular measurement space.With the spiral type influent stream passage of dispensing orifice, at streamwise, at the rectangle dispensing orifice that channel bottom setting space is equal, the long limit of dispensing orifice is wide with measurement space, and minor face is the half on long limit.When Ring-cylindrical collimator is connected with measurement space above flow graph, between Ring-cylindrical collimator inner wall lower edge and flow graph rotor, leave 1mm gap.Overall and Ring-cylindrical collimator the integral passage of spiral type influent stream passage with dispensing orifice is made up of transparent material.
For investigating impact on measurement result after fluid circulation, with traditional drum-type rheometer and the same flow graph with above-mentioned circulation of fluid collimation distributor, the apparent viscosity of the PAM macromolecular solution that temperature is 20 DEG C is determined respectively, result such as table 1.Table 1 shows, both measurement results are basically identical, it is achieved thereby that general object of the present invention.After this uses " the circulation of fluid collimation distributor " of the present invention with regard to indirect proof, drum-type rheometer can directly measure free settling suspension system, is modified without to instrument itself and measurement result.
Table 1: solution concentration is the measurement result comparison of 60ppm

Claims (6)

1. a circulation of fluid collimation distributor, it is characterized in that: this circulation of fluid collimation distributor comprises the spiral type influent stream passage with dispensing orifice, dispensing orifice was along EDS maps under spiral type influent stream passage one week, dispensing orifice UNICOM separately below perpendicular passage vertically downward, the space UNICOM below perpendicular passage and between flow graph rotor and urceolus.
2. circulation of fluid collimation distributor as claimed in claim 1, it is characterised in that: the part between continuously arranged perpendicular passage and adjacent perpendicular passage constitutes Ring-cylindrical, and the inner and outer diameter of Ring-cylindrical is equal with flow graph rotor, urceolus interior diameter respectively.
3. circulation of fluid collimation distributor as claimed in claim 1, it is characterised in that: spiral type influent stream passage and perpendicular passage with dispensing orifice are made up of transparent material.
4. circulation of fluid collimation distributor as claimed in claim 1, it is characterised in that: with the spiral type influent stream passage of dispensing orifice, at streamwise, at the rectangle dispensing orifice that channel bottom setting space is equal.
5. circulation of fluid collimation distributor as claimed in claim 2, it is characterised in that: described Ring-cylindrical divides upper and lower two sections, and the hypomere of Ring-cylindrical and epimere are detachably connectable, and the perpendicular passage of Ring-cylindrical hypomere constitutes Ring-cylindrical collimator.
6. circulation of fluid collimation distributor as claimed in claim 5, it is characterised in that: when Ring-cylindrical collimator is connected with measurement space above flow graph, between Ring-cylindrical collimator inner wall lower edge and flow graph rotor, leave 1mm gap.
CN201310545975.8A 2013-11-07 2013-11-07 Rotating cylinder flow graph circulation of fluid collimation distributor Active CN103674782B (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101788445A (en) * 2010-02-06 2010-07-28 大连大学 Drum-type rheometer circulating system
CN102095670A (en) * 2010-12-20 2011-06-15 聚合物加工研究所 Improved spiral cylinder rheometer and test method
CN102323184A (en) * 2011-08-12 2012-01-18 哈尔滨理工大学 Visual testing device for liquid metal fluidity and testing method based on it
US8424368B2 (en) * 2010-03-11 2013-04-23 Halliburton Energy Services, Inc. Method for estimating proppant transport and suspendability of viscoelastic liquids

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101788445A (en) * 2010-02-06 2010-07-28 大连大学 Drum-type rheometer circulating system
US8424368B2 (en) * 2010-03-11 2013-04-23 Halliburton Energy Services, Inc. Method for estimating proppant transport and suspendability of viscoelastic liquids
CN102095670A (en) * 2010-12-20 2011-06-15 聚合物加工研究所 Improved spiral cylinder rheometer and test method
CN102323184A (en) * 2011-08-12 2012-01-18 哈尔滨理工大学 Visual testing device for liquid metal fluidity and testing method based on it

Non-Patent Citations (4)

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Title
A new elongational rheometer for polymer melts and other highly viscoelastic liquids;J. Meissner et al.;《Rheologica Acta》;19941231;第33卷(第1期);第1~21页 *
旋转流变仪测定易沉降悬浮液流变性的初步探讨;徐继润等;《过滤与分离》;20081231;第18卷(第2期);第1~3页 *
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