A kind of for silicone adhesive tensile test specimen mould
Technical field
The invention belongs to test piece mould technical field, relate to a kind of test piece mould design, be specifically related to a kind of for silicone adhesive tensile test specimen mould.
Background technology
In recent years, China's silicone sealant industry has been stepped into development fast traffic lane, the development of sealing neutral silicone resin series of products is well afoot also, a lot of products are put on market, not only meet the ever-increasing demand of building industry, and promoted double glazing, glass curtain wall, out-hung panel and metal framework adhesive structure etc. to build the development of new product, new construction, new technology.The leading manufacturing enterprise of domestic silicone building sealant, on the basis of pilot scale production technology of introducing national organosilicon engineering center neutral silicone building sealant, has carried out the research and development of series of products, obtains impressive achievement.Although the existing many units of China and enterprise develop silicone adhesive product, part kind has also realized suitability for industrialized production, compares still have larger gap with Foreign Advanced Lerel.
Silicone sealant is called for short silicone adhesive and belongs to silicone based product, to take a kind of encapsulant that hydroxy-end capped polysiloxane makes as base-material, compare with the molecular organic fluid sealant of other high scores, its bonding force is stronger, large and the excellent performance of resistance to outdoor aging of pulling strengrth, moistureproof, anticorona, and there is good high-low temperature resistant, water resistance, be difficult for xanthochromia, oil-tight, can realize and most of building material product between bonding.Therefore, can be used as sealant, adhesive, embedding agent, be widely used in the new high-tech industry fields such as building, automobile, machinery, electronics, weaving.
Silicone adhesive can be divided into one-component and two large class of component two by the component of product, one-component silicone adhesive is a kind of similar ointment, once the moisture in ingress of air will be solidified into a kind of material of tough and tensile rubber-like solid, two component silicone adhesives refer to that silicone adhesive is divided into two groups of A, B, any one group of individualism all can not form curing, but two groups of rubber cements mix by a certain percentage and just can react curing.Common one-component silicone adhesive is divided into de-acetic acid type, dealcoholized type, ketoxime removing type and de amide type etc.At present, ketoxime removing type product accounts for the leading position in market.
Solidifying of one-component silicone adhesive, after being first the moisture in crosslinking chemical contact atmosphere, there is rapidly hydrolysis reaction in the functional group of hydrolyzable, generates silanol.Si-OH base of its silanol and 107 glue
si-OH base is sent out condensation reaction, makes silicone adhesive curing cross-linked, forms tridimensional network, becomes elastic body.
Test about Bond Strength is to check the test that whether can form bonds well between silicone adhesive used and base material, and because base material is of a great variety, its surface treatment form and processing horizontal also vary, and does not also have at present a kind of glue can guarantee all base materials all necessarily to bond.Therefore,, for some concrete engineerings, the fluid sealant that must select it and base material carry out Test about Bond Strength to guarantee that bonding well.The gross data of putting into practice engineering as silicone adhesive supports, and it is particularly important that Test about Bond Strength seems, in the process of making test specimen, must guarantee the deeply-curing that the regular and test specimen of sample dimensions can be good.
At the < < elastic sealants such as Huang Yingchang and adhesive > >, mention, when the surface drying of rubber cement is too fast, after the top layer of glue or shallow-layer district absorb water rapidly and solidify, the surface of glue has just formed a kind of tridimensional network, strand is arranged closely, hindered steam further to rubber cement internal divergence, thereby deeply-curing is slowed down.In the < < silane crosslinkers such as Chen Ping Yao and coupling agent modified silicone sealant research > >, also draw and work as rubber cement surface drying very in short-term, the conclusion that its curing depth reduces on the contrary.In order to raise the efficiency, the silicone adhesive surface drying time of major part is all shorter now, if require surface drying neutral silicone glue silicone adhesive energy large area contact moisture energy fast demoulding in making test specimen process faster, so just can solve the problem that hinders deeply-curing, there is part silicone adhesive surface drying time longer, if the moisture absorption, makes silicone adhesive fully curing with regard to energy fast demoulding preferably.So this patent has been studied a kind of mould of making silicone adhesive test specimen of good permeability, to provide experimental data accurately to carry out the enforcement of propping works.
Through retrieval related documents, there are no the play-by-play about silicone adhesive tensile test specimen Design of Dies.
Summary of the invention
The object of the present invention is to provide a kind of effective and good permeability, be conducive to silicone adhesive test specimen deeply-curing well, little to guarantee silicone adhesive data of mechanical standard deviation, result accuracy is high, and can make the silicone adhesive tensile test specimen mould of silicone adhesive test specimen fast demoulding.
In order to realize the above-mentioned effect of mentioning, the technical solution used in the present invention is:
A silicone adhesive tensile test specimen mould, setting comprises: spacer pad I, spacer pad II, clamping plate I, clamping plate II, securing member and/or holder; Described spacer pad I and spacer pad II are separately positioned on the two ends of test piece mould; Described clamping plate I and clamping plate II are separately positioned on the both sides of spacer pad I and spacer pad II; Described securing member arranges 1-2, and the outside or the two ends that are enclosed within spacer pad I, spacer pad II, clamping plate I and clamping plate II fixedly obtain this silicone adhesive tensile test specimen mould.
Above-described holder is H shape, and upper end is connected with spacer pad I is fixed or movable, and lower end is flexibly connected with spacer pad II.
The material that above-described spacer pad I, spacer pad II and holder adopt comprises: timber, pottery, plastics, metal and stone material.
The material that above-described clamping plate I and clamping plate II adopt comprises: glass, plastics, pottery, metal and stone material.
Above-described metal comprises: aluminium alloy, stainless steel, iron and steel and compound substance thereof.
Above-described securing member adopts and comprises: shrink-ring, contraction bands, locator card.
Metal or plastic bar that above-described locator card is connected with eave tile by spring metal form.
The principle of work of this silicone adhesive tensile test specimen mould is:
To in the concentrated sulphuric acid of clamping plate I, clamping plate II 40 ~ 60%, soak 24 ~ 48h, or the cleaning of general clean solution, then with clear water, clean, then clean with organic solvent, and be dried it.Inner side in spacer pad I and spacer pad II is stained with respectively non-adhesive material, with securing member, be assembled into the silicone adhesive tensile test specimen mould of cavity, then by pretreated silicone adhesive sample pointing in the cavity of test piece mould, pointing sample is the formation that must be noted that to avoid bubble, sample is pushed to the cavity of the full test piece mould of pointing, the sample of the cavity mouth of equating test piece mould, specimen surface is flushed, again test specimen is sidelong, remove as early as possible clamping plate I, clamping plate II, spacer pad I and spacer pad II, obtain silicone adhesive tensile test specimen.
Advantage of the present invention and good effect:
1, Bian is with the test specimen of silicone adhesive tensile test specimen of the present invention Mold Making without bubble, and specimen surface flushes, and set time is short, and deeply-curing guarantees that silicone adhesive data of mechanical standard deviation is little, and result accuracy is high.
2, silicone adhesive tensile test specimen mould of the present invention is simple in structure, and material source is wide, handling ease, and Mold Making cost is low.
Accompanying drawing explanation
Fig. 1 is that this test piece mould is without the structural representation of holder;
Fig. 2 has the structural representation of holder for this test piece mould;
Fig. 3 is the structural representation of this test piece mould spacer pad;
Fig. 4 is the structural representation of this test piece mould clamping plate;
Fig. 5 is the structural representation of this test piece mould concave surface holder;
Fig. 6 is the structural representation of this test piece mould plane holder;
Fig. 7 is the structural representation of this test piece mould holder and spacer pad.
Sign in Fig. 1-6: 1-clamping plate I, 2-spacer pad I, 3-clamping plate II, 4-spacer pad II, 5-securing member, 6-holder.
Specific embodiment
Embodiment 1
This silicone adhesive tensile test specimen mould, setting includes: the spacer pad I 2 of wood quality, spacer pad II 4, the clamping plate I 1 of glass material, clamping plate II 3, rubber shrink-ring securing member 5; Described spacer pad I 2 and spacer pad II 4 are separately positioned on the two ends of test piece mould; Described clamping plate I 1 and clamping plate II 3, be separately positioned on the both sides of spacer pad I 2 and spacer pad II 4; Described securing member 5 arranges 1, and the outside that is enclosed within spacer pad I 2, spacer pad II 4, clamping plate I 1 and clamping plate II 3 fixedly obtains this silicone adhesive tensile test specimen mould.
Embodiment 2
This silicone adhesive tensile test specimen mould, setting includes: the spacer pad I 2 of ceramic material, spacer pad II 4, the clamping plate I 1 of aluminum alloy material, clamping plate II 3, rubber contraction bands securing member 5; Described spacer pad I 2 and spacer pad II 4 are separately positioned on the two ends of test piece mould; Described clamping plate I 1 and clamping plate II 3, be separately positioned on the both sides of spacer pad I 2 and spacer pad II 4; Described securing member 5 arranges 2, twines to tie up in the outside of spacer pad I 2, spacer pad II 4, clamping plate I 1 and clamping plate II 3 fixedly to obtain this silicone adhesive tensile test specimen mould.
Embodiment 3
This silicone adhesive tensile test specimen mould, setting includes: the spacer pad I 2 of aluminum alloy material, spacer pad II 4, the clamping plate I 1 of plastic material, clamping plate II 3, rubber shrink-ring securing member 5; Described spacer pad I 2 and spacer pad II 4 are separately positioned on the two ends of test piece mould; Described clamping plate I 1 and clamping plate II 3, be separately positioned on the both sides of spacer pad I 2 and spacer pad II 4; Described securing member 5 arranges 2, and the outside that is enclosed within spacer pad I 2, spacer pad II 4, clamping plate I 1 and clamping plate II 3 fixedly obtains this silicone adhesive tensile test specimen mould.
Embodiment 4
This silicone adhesive tensile test specimen mould, setting includes: the spacer pad I 2 of glass material, spacer pad II 4, the clamping plate I 1 of plastic-aluminum alloy material, clamping plate II 3, rubber shrink-ring securing member 5; Described spacer pad I 2 and spacer pad II 4 are separately positioned on the two ends of test piece mould; Described clamping plate I 1 and clamping plate II 3, be separately positioned on the both sides of spacer pad I 2 and spacer pad II 4; Described securing member 5 arranges 1, and the outside that is enclosed within spacer pad I 2, spacer pad II 4, clamping plate I 1 and clamping plate II 3 fixedly obtains this silicone adhesive tensile test specimen mould.
Embodiment 5
This silicone adhesive tensile test specimen mould, setting includes: the spacer pad I 2 of wood quality, spacer pad II 4, the clamping plate I 1 of glass material, clamping plate II 3, spring metal is connected with the securing member 5 of the Metallic rod formation locator card of eave tile, the holder 6 of wood quality; Described holder 6 is H shape, and one end and spacer pad I 2 use carpenter's glues are adhesively fixed, and the other end is flexibly connected with spacer pad II 4; Described clamping plate I 1 and clamping plate II 3, be separately positioned on the both sides of spacer pad I 2 and spacer pad II 4; Described securing member 5 arranges 1, and the upper end that is enclosed within clamping plate I 1 and clamping plate II 3 fixedly obtains this silicone adhesive tensile test specimen mould.
Embodiment 6
This silicone adhesive tensile test specimen mould, setting includes: the spacer pad I 2 of plastic material, spacer pad II 4, the clamping plate I 1 of stainless steel, clamping plate II 3, rubber shrink-ring securing member 5, the holder 6 of plastic material; Described holder 6 is H shape, and one end and spacer pad I 2 use bonding agents are fixed, and the other end is flexibly connected with spacer pad II 4; Described clamping plate I 1 and clamping plate II 3, be separately positioned on the both sides of spacer pad I 2 and spacer pad II 4; Described securing member 5 arranges 2, and the middle-end outside that is enclosed within spacer pad I 2, spacer pad II 4, clamping plate I 1 and clamping plate II 3 fixedly obtains this silicone adhesive tensile test specimen mould.